Selenium-Enriched Brushite: A Novel Biomaterial for Potential Use in Bone Tissue Engineering
Abstract
:1. Introduction
2. Results and Discussion
3. Materials and Methods
3.1. Sample Preparation
3.2. Characterization
4. Conclusions
Author Contributions
Funding
Acknowledgments
Conflicts of Interest
Appendix A
Peak Position-2 Theta (°) | ||
---|---|---|
Peak Index | Bru | Se-Bru |
020 | 11.75 | 11.70 |
12-1 | 21.00 | 20.99 |
040 | 23.50 | 23.47 |
21-1 | 24.56 | 24.53 |
14-1 | 29.35 | 29.33 |
121 | 30.56 | 30.54 |
150 | 34.19 | 34.18 |
200 | 34.45 | 34.45 |
141 | 37.06 | 36.90 |
22-2 | 37.17 | 37.14 |
15-2 | 41.61 | 41.60 |
240 | 42.09 | 42.08 |
170 | 45.30 | 45.27 |
062 | 47.95 | 47.92 |
32-1 | 48.61 | 48.60 |
Appendix B
Wavenumbers (CM−1) | Vibration Modes | |
---|---|---|
Bru | Se-Bru | |
3544-3491 | 3544-3491 | ν3 H2O (lattice water molecules) |
3283-3163 | 3285-3167 | ν1 H2O (lattice water molecules) |
2943 | 2945 | PO-H stretching |
2364 | 2359 | |
1725 | 1727 | Combination (bending) and rotation of residual free water |
1649 | 1650 | H-O-H bending of lattice water molecules |
1222 | 1219 | δ (PO-H) |
1133 | 1134 | νd(P-OH) |
1058 | 1060 | |
985 | 985 | νs(P-OH) |
874 | 873 | ν(P-O(H)) |
790 | 790 | δ(P-O(H)) |
660 | 660 | water libration |
576 | 577 | δ(O-P-O(H)) |
524 | 523 | δ(O-P-O(H)) |
410 | 412 | δ(O-P-O(H)) |
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Parameters | Bru | Se-Bru |
---|---|---|
Phase Composition | 100% DCPD | 100% DCPD |
Unit Cell Parameters | ||
a (Å) | 5.915 | 6.238 |
b (Å) | 15.12 | 15.16 |
c (Å) | 6.242 | 5.806 |
β (˚) | 116.4 | 116.4 |
Volume ((Å)3) | 500.2 | 491.7 |
Se Content (wt%) | -------- | 0.67 ± 0.03% |
Parameters | Bru | Se-Bru |
---|---|---|
T1ρH | 7.09 ± 0.05 | 6.84 ± 0.08 |
λ | 0.51 ± 0.01 | 0.54 ± 0.02 |
Tdf | 0.88 ± 0.03 | 0.56 ± 0.04 |
TCP* | 0.0809 ± 0.001 | 0.101 ± 0.005 |
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Laskus, A.; Zgadzaj, A.; Kolmas, J. Selenium-Enriched Brushite: A Novel Biomaterial for Potential Use in Bone Tissue Engineering. Int. J. Mol. Sci. 2018, 19, 4042. https://doi.org/10.3390/ijms19124042
Laskus A, Zgadzaj A, Kolmas J. Selenium-Enriched Brushite: A Novel Biomaterial for Potential Use in Bone Tissue Engineering. International Journal of Molecular Sciences. 2018; 19(12):4042. https://doi.org/10.3390/ijms19124042
Chicago/Turabian StyleLaskus, Aleksandra, Anna Zgadzaj, and Joanna Kolmas. 2018. "Selenium-Enriched Brushite: A Novel Biomaterial for Potential Use in Bone Tissue Engineering" International Journal of Molecular Sciences 19, no. 12: 4042. https://doi.org/10.3390/ijms19124042