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Article

Comparison of Different Parameters to Evaluate Delamination in Edge Trimming of Basalt Fiber Reinforced Plastics (BFRP)

by
María Dolores Navarro-Mas
1,*,
María Desamparados Meseguer
1,
Joaquín Lluch-Cerezo
1,2 and
Juan Antonio García-Manrique
1
1
Department of Mechanical Engineering and Materials, Universitat Politècnica de València, Camino de Vera s/n, 46022 Valencia, Spain
2
Engineering Research Team, Florida Universitària, 46470 Catarroja, Spain
*
Author to whom correspondence should be addressed.
Materials 2020, 13(23), 5326; https://doi.org/10.3390/ma13235326
Submission received: 2 November 2020 / Revised: 18 November 2020 / Accepted: 22 November 2020 / Published: 24 November 2020
(This article belongs to the Special Issue Special Issue of Manufacturing Engineering Society-2020 (SIMES-2020))

Abstract

:
Delamination is one of the main problems that occur when machining fiber-reinforced composite materials. In this work, Types I and II of delamination are studied separately in edge trimming of basalt fiber reinforced plastic (BFRP). For this purpose, one-dimensional and area delamination parameters are defined. One-dimensional parameters (Wa and Wb) allow to know average fibers length while the analysis of area delamination parameters (Sd) allow to evaluate delamination density. To study delamination, different tests are carried out modifying cutting parameters (cutting speed, feed per tooth and depth of cut) and material characteristics (fiber volume fraction and fiber orientation). Laminates with a lower fiber volume fraction do not present delamination. Attending to one-dimensional parameters it can be concluded that Type II delamination is more important than Type I and that a high depth of cut generates higher values of delamination parameters. An analysis of variance (ANOVA) is performed to study area parameters. Although delamination has a random nature, for each depth of cut, more influence variables in area delamination are firstly, feed per tooth and secondly, cutting speed.

1. Introduction

In aeronautical, naval and automotive sectors, application of fiber-reinforced polymeric matrix composite materials is increasing, mainly due to their lightness, high mechanical resistance and resistance to corrosion and high temperatures. Manufacturing processes of fiber-reinforced composite materials allow to obtain parts with a geometry close to the desired one. After curing, machining processes are required to eliminate excess of material and to achieve the required shapes and tolerances. However, fiber-reinforced composite materials behave differently in machining than metals, due to their heterogeneous nature and anisotropy [1].
One of the main problems that appear when machining fiber-reinforced composite materials is delamination. Delamination consists of a separation of the fabric layers from the composite material due to the force exerted by the cutting tool during machining process. This defect affects both the dimensional accuracy and the subsequent joining between parts [2]. It can cause reprocess the parts, with the loss of time that this entails, and even to discard the part. Delamination can be classified into three types: I, II and III [3]. Type I appears when the fibers are bent into the machining line, causing surface damage to the part. Type II appears when there are fibers that protrude from the machined edge, while Type III appears when there are fibers parallel to the machined edge. It can also appear simultaneously delaminates of Type I/II.
In the literature, the most studied factors to evaluate delamination produced after milling are cutting parameters, fiber orientation angle and cutting tool characteristics (material, teeth number, etc.) [4,5,6,7,8]. Cutting speed and feed are mainly studied [9,10,11,12], but only a few authors also include depth of cut [13] since most of them think that its influence on delamination is not as relevant as cutting speed and feed. Fiber orientation angle respect to machining direction is as well evaluated, with the aim of determining orientations to avoid or decrease delamination [14,15,16].
In milling process, delamination has been mainly studied in grooving and in edge trimming operations. In grooving, a “delamination factor” is defined, similar to the one used in drilling. Instead of referencing the delamination measurement to the hole diameter, reference is made to the groove width [17]. As in drilling, this measurement parameter is one-dimensional and only take into account Type I delamination, which causes damage to the part. This parameter does not evaluate other types of delamination, which protrude into the groove, and that could be more important than Type I delamination.
To evaluate delamination in milling, in both grooving [18] and edge trimming [19], different types of delamination are identified (Types I, II and III), determining the influence of each one and quantifying their values. In edge trimming, for each type of delamination, fibers length is measured, as well as their frequency of appearance, obtaining the average of the values. In addition to measure the length of the fibers that cause different types of delamination, areas occupied by these fibers can also be evaluated. In this way, in wood machining, there are studies that define a delamination factor as the relationship between the delamination area and the evaluated length [20]. This factor can also be applied to fiber-reinforced polymeric matrix composites. Another work that deals with the measurement of delaminated areas defines an area delamination factor as the ratio between the delaminated area and the initial area [21]. An image comparison method is used to determine the delaminated area, but no distinction between different types of delamination is made.
Generally, delamination occurs mostly in one of the layers of the part, the upper or the lower layer, and most factors defined above only evaluate this effect in one of the layers. However, delamination factors have also been defined to jointly evaluate this defect in both layers [22]. In this proposal, delamination areas in both layers are measured in the machined length, taking images from the top, the bottom and the front of the part.
In this paper different parameters are defined to evaluate the two most important types of delamination, Type I and Type II, in edge trimming of BFRP. Basalt fiber is completely inert, non-toxic and good thermal and electrical insulator, and has properties that make it performs better than glass fiber and slightly worse than carbon fiber [23]. All parameters defined and evaluated in this work can also be applied to carbon or glass fiber reinforced plastics.
Different tests are carried modifying cutting parameters (cutting speed, feed per tooth and depth of cut) and material characteristics (fiber volume fraction and fiber orientation) at different cutting times to evaluate delamination.
Delamination parameters are classified in one-dimensional parameters and area parameters. One-dimensional parameters (Wa and Wb) allow to evaluate the length of the fibers that protrudes or goes inward from the trimming edge, considering free spaces between yarns, and without considering these free spaces. These parameters allow to quantify the delamination in all experiments at different cutting times. Anyway, area parameters are also needed to evaluate density delamination. All these parameters allow to study delamination, but considering that delamination has a random nature. Additionally, an ANOVA study has been performed to quantify the effect of cutting conditions and fiber orientation angle in area parameters.

2. Materials and Methods

2.1. Materials

Parts to be machining are rectangular laminates (420 mm × 260 mm) of fiber-reinforced polymer matrix with a thickness of 3.4 mm manufactured by resin transfer molding (RTM). Reinforcement chosen is a bi-directional long basalt fiber fabric (Figure 1), with step between yarns 3 mm. Matrix is an epoxy low viscosity resin (Prime 20 LV Gurit, Newport Isle of Wight, UK).
Edge trimming operation (down milling) is conducted in a milling machine (Kondia B-500, Elgoibar, Spain), with a Mitsubishi Materials milling tool holder of diameter 25 mm and two exchangeable uncoated carbide cutting inserts [24]. To avoid dust, a film bag involved machining area is used.
Variables used to study delamination parameters are cutting parameters (cutting speed, feed per tooth and depth of cut) and material characteristics (fiber volume fraction and fiber orientation). Design of experiments is based in Taguchi’s method for five variables at two levels (Table 1). An L16 orthogonal array was selected to determine combination of factor levels to use for each experiment (Table 2). Each experiment consumes a large amount of material and an elevated time, therefore a full factorial design has not been considered, in order to reduce the number of experiments.
A cutting tool with new inserts was machining without coolant for 80 min. Stopping times (30, 50, 60, 70 and 80 min) are made to measure delamination parameters. In test 14, due to high cutting conditions, a great flank wear occurred, and it was not possible to reach a cutting time of 80 min.

2.2. Delamination Measurement Method

Delamination measurement has been made capturing wick images of the upper face of laminates (Figure 2) in an evaluated length (L). Although laminates allow to measure 240 mm to evaluate delamination, only a length (L) of 80 mm is evaluated to reduce time and data acquisition cost. This length (L) is selected along of 240 mm of the laminate where delamination values are bigger.
An image is taken of the machined edge of the laminate, and for each wick (i) the following three parameters are captured by means of a cutout and its histogram: surface (Sdi) for each type of delamination; maximum value (hmax i) and invaded edge length (li) (Figure 3).
The values obtained by measuring wick to wick delamination from the captured images of each experiment are recorded in Excel data sheets, for subsequent analysis and calculation of delamination parameters. Table 3 shows data collected for test 12 at all cutting times, area delamination values (Sdi) and the length invaded (li) for Type II delamination on the trimming edge. All data are combined and summarized to obtain delamination parameters.

3. Results and Discussion

Laminates with a low fiber volume (Fv 40%) do not present delamination, so they will not be evaluated. However, in laminates manufactured with high fiber volume (Fv 60%) delamination always appears on the edge, regardless of the cutting time. In all laminates, delamination on the upper face is greater than on the lower face. In order to evaluate delamination only upper face will be measured.
Laminates with 45° and 90° fiber orientation are evaluated. In 45° fiber orientation laminates all warp yarns are over the fill yarn, thereby all wicks present delamination. In 90° fiber orientation, different delamination cases are studied (Figure 4), because delamination can appear only in the warp yarn over the fill yarn or in both, the warp yarns over and under the fill yarn.
To analyze delamination, warp yarns over the fill yarn have been identified with a number. If warp yarns are under the fill yarn they have been identified with a number plus ‘(Figure 5).
In the evaluation of delamination, average length of the fibers that protrudes and goes inward from the laminate are measured. To quantify these values, one-dimensional parameters (Wa and Wb) are defined. Wa parameter allows to classify the tests attending at delamination magnitude, distributing delaminated surface in the evaluated length (L). Wb parameter calculates delamination magnitude, but not considering free space between wicks. On the other hand, in order to compare all experiments, a delamination factor (Fdel) is defined as the ratio between Wb value and the maximum theoretical possible value. This factor allows to classify experiment attending to the maximum possible theoretical delamination value. As this maximum value depends on the selected depth of cut, the effect of this variable is mitigated.
One-dimensional parameters do not define correctly delamination density. Therefore, it is also necessary to define area parameters (Sdi). As happens in one-dimensional parameters, to compare between experiments an area delamination factor (FSdi) is defined as the ratio between the Sdi and the maximum theoretical possible delaminated area for each experiment.

3.1. Length Delamination Parameters

These parameters allow to know the average length of fibers that protrude in Type II delamination and the average length of fibers that are inward from the trimmed edge in Type I delamination.
The “medium delamination” parameter (Wa) is defined as the height of an equivalent rectangle of delaminated area with basis the evaluated length (L) (Figure 6). Studied length is 80 mm, and this length considers delaminated fibers and the free space between fibers, where there is not delamination:
Wa =   Sd i   L  
Medium delamination parameter (Wa) does not allow a real measure of delamination length because all delaminated surface is related to studied length (L). Relating delaminated area to only delaminated fibers length ( l i ) , without considering free space between fibers, gives a more real approximation to average fibers length delamination. For this reason, a second parameter denominated “equivalent delamination” (Wb) is defined (Figure 7).
In Type II delamination, the theoretical maximum value (Wmax) of parameters Wa and Wb is the depth of cut. In Type I delamination, this maximum value is the yarn measure (3 mm) in 90° fiber orientation tests, and the yarn diagonal (4.24 mm) in 45° fiber orientation tests (Figure 8). Delamination parameters are defined as mentioned above in warp yarns over fill yarn, and they are called Wa’ and Wb’ in warp yarns under fill yarn.
Table 4 and Table 5 show Wa, Wa’, Wb and Wb’ parameters and the theoretical maximum delamination (Wmax) values. To compare these values, delamination factors (Fdel and Fdel’) are defined as the ratio of Wb (or Wb’) respectively to Wmax:
Fdel =   Wb   Wmax  
Fdel ' =   Wb '   Wmax  
In each experiment, data are taken at different cutting times. As cutting time increases, tool wear increases and delamination should be greater, increasing values of different parameters and factors. Delamination values present great variation at different cutting times, without an increasing or decreasing trend as tool wear increases. Table 4 and Table 5 show maximum and minimum delamination values for Wa, Wb and Fdel, observing that there is no correlation between delamination and cutting time. This is due to the fact that delamination has a random nature, mainly due to the distance of the warp yarn from the trimmed edge until the next dip below the crossing fill is different at every cutting time. This distance is defined as Xd in the literature [14]. Xd value depends on fiber orientation and the width of the yarn, as well as the inclination angle of the fabric with the cutting path. Xd can take a constant value, it can follow a uniform pattern or it can be totally random (Figure 9). For this reason, the minimum and maximum values of the analyzed delamination parameters and factors are not presented at the same cutting times, concluding that there is almost no dependence of delamination with cutting time.
In almost all experiments, Type I and Type II delamination appear at the same places of the trimming edge. Data from all experiments at all cutting times are analyzing, except for test 14, because in this test tool has reached a rapid flank wear and parameters values are excessive high. Values obtained for Type II delamination are much higher than values for Type I delamination. Table 6 shows average values for Wa, Wb and Fdel for Type I and II delamination and their comparison.
Depth of cut is one important parameter to evaluate delamination. Table 7 shows average delaminate values for parameters Wa, Wb and Fdel for experiments with different depth of cut and their comparison. A high depth of cut provokes a high delamination in the part (Table 7). This effect is not entirely showed in Fdel, because this factor is referenced to depth of cut.
In the test with 90° fiber orientation, Wa value is usually higher than Wa’. Table 4 and Table 5 show only a few cases where Wa and Wa’ present similar values. Therefore, it can be concluded that delamination of the warp yarn below the fill yarn is negligible. When parameters Wb and Wb’ are similar, delamination stands out the same, but delamination can be neglected as long as the length invaded is small. This means that there will only be a few wicks with delamination. If invaded length is not small, Wb and Wb’ should be considered together to evaluate delamination. In these tests, appearance of the machined piece is worst, with more length invaded by delamination.
Due to delamination values present great variation at different cutting times, without an increasing or decreasing trend, a range is established to delamination parameters and factors in each experiment (Figure 10 and Figure 11).

3.2. Area Delamination Parameters

In order to quantify density delamination in every experiment, values obtained for Wb and Wb’ parameters in 90° fiber orientation cannot be added. For this reason, delaminated areas measurement has been carried out. In 90° orientation fiber laminates, these areas are compared in the warp yarn over and under fill yarn.
As in one-dimensional parameters, area delamination factors (FSd) are also defined. In these parameters delaminated area is related to the maximum possible delamination area:
FSdi = Sdi   Sd   max  
FSdi ' = Sdi '   Sd   max  
Table 8 and Table 9 show these values and comparisons. Working with delamination areas allow to add FSdi and FSdi’ in 90° fiber orientation laminates to evaluate the total delaminated area, and comparing with 45° fiber orientation experiments.
A range is established to delamination variation for FSdi and FSdi’ in each experiment for Type I and II delamination (Figure 12 and Figure 13).
An analysis of variance (ANOVA) has been performed to quantify the effect of cutting conditions and fiber orientation angle on the area delamination factors (FSdi + FSdi’). For analyzing the significant effect of the factors on the responses, F test with a level significance of 0.05 has been used. Table 10 shows that feed per tooth has the most significant effect on delamination, following by cutting speed. On the other hand fiber orientation is the least significant factor. It is expected that for a feed per tooth of 0.1 mm, delamination is smaller than for 0.4 mm. At smaller feeds, cutting edges impact on the fabric wick a greater number of times. Applying ANOVA to FSdi + FSdi’ does not allow to evaluate properly the effect of depth of cut, because this factor is referenced to depth of cut.
The influence of each factor can be represented using a Box-whisker diagram (Figure 14). The mean plot shows the change in the response when variables varies from level 1 to level 2.

4. Conclusions

This paper defines and evaluates different delamination parameters for Type I and II delamination in edge trimming of basalt fiber reinforced plastics (BFRP). All parameters defined and evaluated in this work can also be applied to carbon or glass fiber reinforced plastics. For this purpose, different tests are carried out modifying cutting parameters (cutting speed, feed per tooth and depth of cut) and material characteristics (fiber volume fraction and fiber orientation). Delamination values have been obtained at different cutting times in order to find a relationship between delamination and cutting time, although most authors do not take delamination values at different cutting times.
Delamination parameters are classified in parameters that evaluate lengths and parameters that evaluate areas. Parameters that evaluate lengths give an average of protrude fibers length (for Type II delamination) and an average of inward fibers length (for Type I delamination). Two parameters are defined in this category (Wa and Wb). Wa considers free spaces between yarns, but Wb does not consider these free spaces. A delamination factor (Fdel) is also defined in order to compare delamination of each experiment with the maximum possible delamination value. On the other hand, parameters evaluating areas (Sd) are needed to quantify density delamination in the machining edge. Additionally, as in one-dimensional parameters, a factor (Fsd) is defined to compare area delamination.
Delamination at the top layer of the laminate only appears with a 60% fiber volume fraction. BFRP consists of a bi-directional long basalt fiber fabric, therefore delamination has been measured in warp yarns over and under fill yarn in 90° fiber orientation laminates. In most of 90° fiber orientation measurements, delamination measured in warp yarns over fill yarn is bigger than one measured in warp yarn under fill yarn, it can be concluded that delamination of the warp yarn below the fill yarn is negligible.
Delamination parameters and factors are calculated at different cutting times. Delamination values present great variation at different cutting times, without an increasing or decreasing trend as tool wear is increasing. It is due to the random nature of delamination. At every cutting time, the distance of the warp yarn from the trimmed edge until next dip below the crossing fill yarn (Xd) is changing, observing a uniform or sine wave delamination.
Analyzing one-dimensional parameters, it can be concluded that Type II delamination is more important than Type I and that a high depth of cut generates higher values of delamination parameters. Fdel factor can be used to compare between experiments with the same depth of cut, but not with different values of depth of cut, as maximum possible area depends on the selected depth of cut.
An analysis of variance (ANOVA) is performed to study area parameters. Although delamination has a random nature, for each depth of cut, more influence variables in area delamination are firstly, feed per tooth and secondly, cutting speed. It is expected that for a feed per tooth of 0.1 mm, delamination is smaller than for 0.4 mm, because at smaller feeds cutting edges impact on the fabric wick a greater number of times.

Author Contributions

Conceptualization, M.D.N.-M. and M.D.M.; methodology, M.D.N.-M. and M.D.M.; software, M.D.N.-M. and J.L.-C.; validation, M.D.N.-M. and M.D.M.; formal analysis, M.D.N.-M. and J.L.-C.; investigation, M.D.N.-M. and M.D.M.; resources, J.A.G.-M.; data curation, M.D.N.-M. and J.L.-C.; writing—Original draft preparation, M.D.N.-M., M.D.M. and J.L.-C.; writing—Review and editing, M.D.N.-M., M.D.M., J.L.-C. and J.A.G.-M.; visualization, M.D.N.-M., M.D.M., J.L.-C. and J.A.G.-M.; supervision, J.A.G.-M.; project administration, J.A.G.-M.; funding acquisition, J.A.G.-M. All authors have read and agreed to the published version of the manuscript.

Funding

This research was funded by Government of Spain, grant number PID2019-108807RB-I00.

Conflicts of Interest

The authors declare no conflict of interest. The funders had no role in the design of the study; in the collection, analyses, or interpretation of data; in the writing of the manuscript, or in the decision to publish the results.

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Figure 1. Bi-directional long basalt fiber fabric.
Figure 1. Bi-directional long basalt fiber fabric.
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Figure 2. Evaluated laminate length (L).
Figure 2. Evaluated laminate length (L).
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Figure 3. Example Wick number 4—parameters delamination measurement: (a) Type I delamination; (b) Type II delamination; (c) histogram with number of yellow pixels (Sdi, delaminated area).
Figure 3. Example Wick number 4—parameters delamination measurement: (a) Type I delamination; (b) Type II delamination; (c) histogram with number of yellow pixels (Sdi, delaminated area).
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Figure 4. Delamination areas in 90° fiber orientation laminates. (a) Delamination in warp yarns over fill yarn (b,c) Delamination in warp yarns over and under the fill yarn.
Figure 4. Delamination areas in 90° fiber orientation laminates. (a) Delamination in warp yarns over fill yarn (b,c) Delamination in warp yarns over and under the fill yarn.
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Figure 5. Warp yarns identification.
Figure 5. Warp yarns identification.
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Figure 6. Medium delamination parameter (Wa) for Type II delamination.
Figure 6. Medium delamination parameter (Wa) for Type II delamination.
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Figure 7. Equivalent delamination parameter (Wb) for Type II delamination.
Figure 7. Equivalent delamination parameter (Wb) for Type II delamination.
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Figure 8. Theoretical maximum value of Wb in 45° fiber orientation tests.
Figure 8. Theoretical maximum value of Wb in 45° fiber orientation tests.
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Figure 9. Xd variation.
Figure 9. Xd variation.
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Figure 10. Wa and Wb delamination parameters.
Figure 10. Wa and Wb delamination parameters.
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Figure 11. Fdel delamination factor.
Figure 11. Fdel delamination factor.
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Figure 12. Area delamination factor range Type I (FSdi + FSdi’).
Figure 12. Area delamination factor range Type I (FSdi + FSdi’).
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Figure 13. Area delamination factor range Type II (FSdi + FSdi’).
Figure 13. Area delamination factor range Type II (FSdi + FSdi’).
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Figure 14. Box-whisker diagram.
Figure 14. Box-whisker diagram.
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Table 1. Variables and levels.
Table 1. Variables and levels.
LevelCutting Speed vc (m/Min)Feed Per Tooth fz (mm)Depth of Cut ap (mm)Fiber Volume Fv (%)Fiber Orientation Fo (°)
13000.10.54045
24700.41.56090
Table 2. Experimental parameters.
Table 2. Experimental parameters.
TestCutting Speed vc (m/Min)Feed Per Tooth fz (mm)Depth of Cut ap (mm)Fiber Volume Fv (%)Fiber Orientation Fo (°)
014700.11.54090
023000.11.54045
033000.40.54045
043000.41.56045
054700.10.56090
064700.40.54090
073000.10.56045
084700.40.56045
094700.10.54045
103000.10.54090
113000.11.56090
123000.40.56090
134700.41.54045
144700.41.56090
153000.41.54090
164700.11.56045
Table 3. Example of Type II delamination data sheets for test 12.
Table 3. Example of Type II delamination data sheets for test 12.
TcE12 Wicks
(min)Type II1234567891011121314Total
30Sdi(mm2)1.120.861.061.051.290.901.311.220.930.540.570.800.450.2212.33
li(mm)2.002.133.482.573.162.932.822.512.531.961.712.172.800.7233.47
50Sdi(mm2)0.410.380.320.310.400.420.450.320.270.310.160.480.350.785.35
li(mm)2.442.782.752.592.962.382.572.002.042.141.142.612.101.8932.38
60Sdi(mm2)0.410.380.320.310.400.420.450.320.270.310.160.480.350.785.35
li(mm)2.422.752.732.572.942.352.541.982.022.121.112.592.081.8732.08
70Sdi(mm2)0.420.270.200.640.320.350.361.010.390.970.390.075.39
li(mm)1.452.091.122.211.963.242.912.742.512.0201.9005.3131.07
80Sdi(mm2)0.870.900.880.900.720.600.640.530.610.660.360.370.480.489.03
li(mm)2.602.201.992.182.092.432.031.732.512.772.032.152.322.7231.74
Table 4. Parameter values in Type I delamination.
Table 4. Parameter values in Type I delamination.
Test TcWaWa’WbWb’ Wmax FdelFdel’
(min)(mm)(mm)(mm)(mm)(mm)
E05Vc 470300.0220.0030.0690.05130.0231 0.0171
Fz 0.1500.0310.0080.0800.08430.0265 0.0281
ap 0.5600.0330.0130.0980.09830.0326 0.0327
Fo 90°700.0250.0230.0640.05830.0215 0.0192
800.0340.0120.1050.05130.0348 0.0169
E12Vc 300300.0650.0050.1740.04930.0579 0.0164
Fz 0.4500.04800.118030.0394 0
ap 0.5600.05300.131030.0437 0
Fo 90°700.0620.0040.1600.09130.0534 0.0303
800.0580.0070.1450.02930.0485 0.0097
E11Vc 300300.08100.178030.0592 0
Fz 0.1500.09300.215030.0718 0
ap 1.5600.0730.0260.1620.07930.0539 0.0264
Fo 90°700.0490.0250.1310.08030.0438 0.0267
800.0630.0540.1330.10230.0445 0.0340
E14Vc 4701.10.1830.0110.3920.07130.1308 0.0235
Fz 0.450.1470.1240.3090.27230.1029 0.0905
ap 1.5100.2220.1540.4980.27830.1661 0.0928
Fo 90°200.3510.0940.8520.16130.2839 0.0535
310.3310.0540.8560.09830.2852 0.0326
37.50.1610.0120.4300.07030.1433 0.0232
400.0770.3180.1710.65630.0571 0.2187
E07Vc 300300.007 0.139 4.240.0327
Fz 0.1500.005 0.086 4.240.0202
ap 0.5600.017 0.085 4.240.0201
Fo 45°700 0 4.240
800.025 0.126 4.240.0296
E08Vc 470300.126 0.266 4.240.0626
Fz 0.4500.121 0.206 4.240.0486
ap 0.5600.098 0.185 4.240.0436
Fo 45°700.122 0.305 4.240.0719
800.032 0.081 4.240.0190
E04Vc 300300.164 0.308 4.240.0726
Fz 0.4500.105 0.225 4.240.0531
ap 1.5600.137 0.238 4.240.0562
Fo 45°700.104 0.183 4.240.0430
800.153 0.252 4.240.0593
E16Vc 470300.039 0.098 4.240.0231
Fz 0.1500.121 0.249 4.240.0587
ap 1.5600.063 0.098 4.240.0231
Fo 45°700.034 0.093 4.240.0219
800.086 0.180 4.240.0424
maximum value Materials 13 05326 i001minimum value Materials 13 05326 i002 Wa Wa ' Materials 13 05326 i003
Table 5. Parameter values in Type II delamination.
Table 5. Parameter values in Type II delamination.
Test TcWaWa’WbWb’ Wmax FdelFdel’
(min)(mm)(mm)(mm)(mm)(mm)
E05Vc 470300.0650.0150.2010.1700.50.4015 0.3404
Fz 0.1500.0660.0070.1700.0980.50.3402 0.1951
ap 0.5600.0570.0620.1690.1310.50.3386 0.2354
Fo 90°700.1050.0910.2760.1780.50.5522 0.3558
800.0520.0620.1570.1640.50.3137 0.2730
E12Vc 300300.1540.0750.3690.2350.50.7371 0.4690
Fz 0.4500.0670.0220.1650.1360.50.3306 0.2722
ap 0.5600.0670.0090.1670.1270.50.3336 0.2549
Fo 90°700.0670.0100.1730.1750.50.3467 0.3498
800.1130.1170.2840.2490.50.5688 0.4783
E11Vc 300300.1090.0250.2390.0931.50.1591 0.0618
Fz 0.1500.2920.0160.6780.0801.50.4520 0.0533
ap 1.5600.5300.1021.1760.2151.50.7839 0.1432
Fo 90°700.2750.1030.7430.1961.50.4952 0.1306
800.2760.0700.5810.1331.50.3875 0.0886
E14Vc 4701.10.2930.0990.6270.2661.50.4180 0.1772
Fz 0.450.6430.1791.3520.3411.50.9012 0.2270
ap 1.5100.5380.3681.2070.6631.50.8045 0.4422
Fo 90°200.4640.2011.1250.3421.50.7502 0.2282
310.5150.2221.3330.4011.50.8884 0.2674
37.50.4840.1661.2930.3621.50.8623 0.2410
400.8410.3081.8750.6341.51.2502 0.4226
E07Vc 300300.028 0.208 0.50.4160
Fz 0.1500.021 0.120 0.50.2400
ap 0.5600.009 0.056 0.50.1112
Fo 45°700.030 0.182 0.50.3646
800.039 0.149 0.50.2971
E08Vc 470300.189 0.397 0.50.7932
Fz 0.4500.165 0.283 0.50.5654
ap 0.5600.136 0.256 0.50.5115
Fo 45°700.168 0.417 0.50.8349
800.128 0.213 0.50.4250
E04Vc 300300.372 0.745 1.50.4967
Fz 0.4500.498 1.072 1.50.7148
ap 1.5600.596 1.038 1.50.6921
Fo 45°700.293 0.512 1.50.3412
800.597 0.983 1.50.6551
E16Vc 470300.387 0.848 1.50.5652
Fz 0.1500.248 0.513 1.50.3420
ap 1.5600.641 1.004 1.50.6693
Fo 45°700.230 0.683 1.50.4552
800.245 0.445 1.50.2969
maximum value Materials 13 05326 i004minimum value Materials 13 05326 i005 Wa Wa ' Materials 13 05326 i006
Table 6. Type I and II delamination comparison.
Table 6. Type I and II delamination comparison.
W a ¯ (mm) W b ¯     mm F d e l ¯
Type I0.0670.1530.042
Type II0.2090.4480.467
W a ¯   Type   II W a ¯   Type   I   = 3.12 W b ¯   Type   II W b ¯   Type   I   = 2.93 F del ¯   Type   II F del ¯   Type   I   = 11.12
Table 7. Comparison of experiments with different depth of cut.
Table 7. Comparison of experiments with different depth of cut.
ap (mm) W a ¯ (mm) W b ¯     m m F d e l ¯
0.50.0860.2210.441
1.50.3730.7510.500
W a ¯   ap 1.5 W a ¯   ap 0.5 = 4.32 W b ¯   ap 1.5 W b ¯   ap 0.5 = 3.40 F del ¯   ap 1.5 F del ¯   ap 0.5 = 1.13
Table 8. Area parameters in Type I delamination.
Table 8. Area parameters in Type I delamination.
Test TcSdi Sdi‘Sdmax FSdiFSdi’FSdi + FSdi’
(min)(mm2)(mm2)(mm2)
E05Vc 470301.790.212400.00750.00090.0084
Fz 0.1502.480.632400.01030.00260.0130
ap 0.5602.641.012400.01100.00420.0152
Fo 90°701.971.832400.00820.00760.0158
802.750.942400.01140.00390.0153
E12Vc 300305.200.372400.02170.00150.0232
Fz 0.4503.8202400.015900.0159
ap 0.5604.2102400.017500.0175
Fo 90°704.980.312400.02070.00130.0220
804.610.542400.01920.00220.0215
E11Vc 300306.4602400.026900.0269
Fz 0.1507.4202400.030900.0309
ap 1.5605.832.102400.02430.00880.0331
Fo 90°703.891.962400.01620.00820.0244
805.074.292400.02110.01790.0390
E14Vc 4701.114.650.842400.06110.00350.0646
Fz 0.4511.749.942400.04890.04140.0903
ap 1.51017.7712.342400.07400.05140.1254
Fo 90°2028.087.552400.11700.03150.1485
3126.464.332400.11020.01800.1283
37.512.870.942400.05360.00390.0575
406.1525.462400.02560.10610.1317
E07Vc 300300.59 169.710.0035 0.0035
Fz 0.1500.43 169.710.0025 0.0025
ap 0.5601.35 169.710.0079 0.0079
Fo 45°700 169.710 0
802.01 169.710.0118 0.0118
E08Vc 4703010.1 169.710.0595 0.0595
Fz 0.4509.65 169.710.0569 0.0569
ap 0.5607.86 169.710.0463 0.0463
Fo 45°709.79 169.710.0577 0.0577
802.58 169.710.0152 0.0152
E04Vc 3003013.09 169.710.0772 0.0772
Fz 0.4508.37 169.710.0493 0.0493
ap 1.56010.96 169.710.0646 0.0646
Fo 45°708.35 169.710.0492 0.0492
8012.23 169.710.0721 0.0721
E16Vc 470303.12 169.710.0184 0.0184
Fz 0.1509.64 169.710.0568 0.0568
ap 1.5605.02 169.710.0296 0.0296
Fo 45°702.75 169.710.0162 0.0162
806.85 169.710.0403 0.0403
Table 9. Area parameters in Type II delamination.
Table 9. Area parameters in Type II delamination.
Test TcSdi Sdi‘Sdmax FSdiFSdi’FSdi + FSdi’
(min)(mm2)(mm2)(mm2)
E05Vc 470305.191.17400.12970.02920.1588
Fz 0.1505.300.56400.13240.01390.1464
ap 0.5604.564.99400.11410.11250.2266
Fo 90°708.427.27400.21050.18180.3922
804.124.94400.10300.10250.2055
E12Vc 3003012.336.03400.30840.15070.4590
Fz 0.4505.351.76400.13380.04410.1779
ap 0.5605.350.70400.13380.01750.1513
Fo 90°705.390.79400.13460.01980.1544
809.039.37400.22570.22500.4507
E11Vc 300308.681.961200.07240.01630.0887
Fz 0.15023.351.241200.19460.01040.2050
ap 1.56042.408.181200.35330.06820.4215
Fo 90°7021.998.271200.18320.06900.2522
8022.085.581200.18400.04650.2305
E14Vc 4701.123.417.951200.19510.06620.2614
Fz 0.4551.4214.291200.42850.11910.5476
ap 1.51043.0429.411200.35860.24510.6037
Fo 90°2037.1016.101200.30910.13410.4433
3141.2117.771200.34340.14810.4915
37.538.7313.281200.32280.11060.4334
4067.2924.601200.56080.20500.7658
E07Vc 300302.23 400.0558 0.0558
Fz 0.1501.68 400.0420 0.0420
ap 0.5600.68 400.0171 0.0171
Fo 45°702.37 400.0593 0.0593
803.12 400.0780 0.0780
E08Vc 4703015.15 400.3788 0.3788
Fz 0.45013.23 400.3308 0.3308
ap 0.56010.87 400.2718 0.2718
Fo 45°7013.4 400.3350 0.3350
8010.2 400.2550 0.2550
E04Vc 3003029.77 1200.2481 0.2481
Fz 0.45039.85 1200.3320 0.3320
ap 1.56047.71 1200.3976 0.3976
Fo 45°7023.42 1200.1951 0.1951
8047.73 1200.3978 0.3978
E16Vc 4703030.93 1200.2578 0.2578
Fz 0.15019.87 1200.1656 0.1656
ap 1.56051.29 1200.4274 0.4274
Fo 45°7018.41 1200.1534 0.1534
8019.57 1200.1631 0.1631
Table 10. Analysis of variance (ANOVA).
Table 10. Analysis of variance (ANOVA).
FactorDfSum SqMean Sq F ValuePr (>F)
Fz10.33950.339527.8765.93 × 106
Vc10.12280.122810.0840.00301
ap 10.12710.127110.4320.00260
Fo 10.07580.07586.2210.01722
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Navarro-Mas, M.D.; Meseguer, M.D.; Lluch-Cerezo, J.; García-Manrique, J.A. Comparison of Different Parameters to Evaluate Delamination in Edge Trimming of Basalt Fiber Reinforced Plastics (BFRP). Materials 2020, 13, 5326. https://doi.org/10.3390/ma13235326

AMA Style

Navarro-Mas MD, Meseguer MD, Lluch-Cerezo J, García-Manrique JA. Comparison of Different Parameters to Evaluate Delamination in Edge Trimming of Basalt Fiber Reinforced Plastics (BFRP). Materials. 2020; 13(23):5326. https://doi.org/10.3390/ma13235326

Chicago/Turabian Style

Navarro-Mas, María Dolores, María Desamparados Meseguer, Joaquín Lluch-Cerezo, and Juan Antonio García-Manrique. 2020. "Comparison of Different Parameters to Evaluate Delamination in Edge Trimming of Basalt Fiber Reinforced Plastics (BFRP)" Materials 13, no. 23: 5326. https://doi.org/10.3390/ma13235326

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