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Materials

Materials is an international peer-reviewed, open access journal on materials science and engineering published semimonthly online by MDPI.
The Portuguese Materials Society (SPM)Spanish Materials Society (SOCIEMAT), Manufacturing Engineering Society (MES) and Chinese Society of Micro-Nano Technology (CSMNT) are affiliated with Materials and their members receive discounts on the article processing charges.
Indexed in PubMed | Quartile Ranking JCR - Q2 (Metallurgy and Metallurgical Engineering | Physics, Applied | Physics, Condensed Matter)

All Articles (53,346)

Polycrystalline Diamond Compacts (PDC) face thermal damage and insufficient wear resistance in complex strata due to the high thermal expansion coefficient of Co binder and its catalysis on diamond graphitization. Existing studies lack a systematic comparison of HfB2, ZrB2, and Al-Ni (1.5wt.%Al + 1.5wt.%Ni) on PDC performance under a unified process, and their synergistic mechanism with the PDC matrix remains unclear. Herein, 3wt.% of these additives were incorporated into diamond micropowder to prepare PDC via unified high-temperature and high-pressure (HTHP) sintering. XRD/SEM-EDS characterized the phase/microstructure, while thermal expansion and Vertical Turret Lathe (VTL) tests evaluated their properties. Results: (1) ZrB2-modified PDC performed the best, with a thermal failure temperature of 800 °C (8.5% higher than the blank group), VTL wear cycles of 110 Pass (22.2% higher), and ZrC (confirmed by XRD) enhancing interface bonding; (2) HfB2-modified PDC reduced the wear area by 18% (vs. the blank group) via low-expansion HfC (6.5 × 10−6/°C) and maintained a continuous structure; (3) Al-Ni-modified PDC had a wear ratio of 1.945 × 104 (4.5% higher) but only 60 Pass and structural defects. This study confirms ZrB2 as the optimal additive for PDC’s comprehensive properties, supporting high-performance PDC development for complex downhole environments.

9 November 2025

XRD pattern of W15-25 diamond micropowder.

This paper compares three nondestructive methods used to detect and locate defects such as delaminations or voids in externally bonded fiber reinforced polymer (FRP) concrete structures: infrared thermography, ground-penetrating radar, and measurement of acoustic wave velocity. One of the main goals was to check whether it was possible to distinguish overlapping defects. For this purpose, eight concrete samples were made with a bonded carbon fiber reinforced polymer (CFRP) strip with the following dimensions 100 × 100 × 500 mm. Two samples had no defects, four had single defects varying in location (at the edge of the strip or in the centre) simulating delamination or voids in the concrete cover, and the remaining samples had overlapping defects. Both infrared thermography and acoustic wave velocity measurement methods allow the detection of defects/voids in the adhesive layer and a concrete defect (void in the concrete cover). However, ground penetration failed to detect defects in the adhesive layer. Only infrared thermography allows for the differentiation of overlapping defects. On the basis of the conducted research, the methodology, differences, advantages, and limitations of each method were described, along with recommendations based on the authors’ experience.

9 November 2025

Scheme of using thermography to detect defects in building structures.

Corrosion-induced cracking poses a significant threat to the longevity of reinforced concrete (RC) structures, yet precisely forecasting its advancement continues to be a considerable scientific obstacle. The principal shortcoming of current numerical models is their excessive simplification, frequently presuming totally saturated conditions and disregarding the dynamic interplay between environmental (hygro-thermal) variations and developing mesoscale damage. This study presents a thorough hygro-thermo-electro-chemo-mechanical (HTECM) phase-field model to fill this research need. The model uniquely combines dynamic unsaturated hygro-thermal transport with multi-ion reactive electrochemistry and meso-scale fracture mechanics. A rigorous comparison with published experimental data validates the model’s exceptional accuracy. The anticipated progression of fracture width exhibited remarkable concordance with experimental data, indicating a substantial enhancement in precision compared to uncoupled, saturated-state models. A key finding is the quantification of the damage-induced “transport-corrosion” positive feedback loop: initial corrosion-induced microcracks significantly expedite the transport of local moisture and corrosive agents, leading to nonlinear structural degradation. This work presents a high-fidelity numerical platform that enhances the understanding of linked deterioration in materials science and improves the durability design of reinforced concrete structures.

9 November 2025

Corrosion of steel rebars in metro concrete and dock concrete.

As the most commercially developed metal additive process, laser powder bed fusion (LPBF) is vital to advancing several industry sectors, enabling high-precision part production across aerospace, biomedical, and manufacturing industries. Al 7075 alloy offers low density and high-specific strength yet faces LPBF challenges such as hot cracking and porosity due to rapid solidification, thermal gradients, and a wide freezing range. To address these challenges, this study proposes an integrated computational and experimental framework to enhance the LPBF processability of Al 7xxx alloys by compositional modification. Using the Calculation of Phase Diagram approach, printable Al 7xxx compositions were designed by adding grain refiners (V and/or Ti) and a eutectic solidification enhancer (Mg) to Al 7075 alloy to enable grain refinement and eutectic solidification. Subsequent LPBF experiments and characterization tests, such as metallography (scanning electron microscopy), energy-dispersive X-ray spectroscopy, X-ray diffraction, and X-ray micro-computed tomography, confirmed the production of refined microstructures with reduced defects. This study contributes to existing approaches for producing high-quality Al 7xxx alloy parts without significant compositional deviations using an integrated computational and experimental approach. Finally, aligning with the Materials Genome Initiative, this study contributes to the development and industrial adoption of advanced materials.

9 November 2025

T–fS curve of Composition 1 (Al 7075 alloy).

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Materials - ISSN 1996-1944