Biopolymer Electrolyte Based on Derivatives of Cellulose from Kenaf Bast Fiber
Abstract
:1. Introduction
2. Experimental Section
2.1. Synthesis of Cellulose
2.2. Synthesis of Carboxymethyl Cellulose from Cellulose Fiber
2.3. Preparation of CMC-Based Biopolymer Electrolytes
2.4. Characterization
2.4.1. Degree of Substitution (DS) Determination
2.4.2. Fourier Transform Infrared Spectroscopy (FTIR)
2.4.3. Thermogravimetric Analysis
2.4.4. Dynamic Mechanical Analyzer (DMA)
2.4.5. Impedance Spectroscopic Study
2.4.6. Scanning Electron Microscope (SEM)
2.4.7. Linear Sweep Voltammetry
3. Results and Discussion
3.1. Carboxymethyl Cellulose
3.2. Carboxymethyl Cellulose-Based Polymer Electrolyte
3.3. Impedance Study
3.4. Morphological Studies
3.5. Electrochemical Stability Determination
4. Conclusions
Acknowledgments
Author Contributions
Conflicts of Interest
References
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Rani, M.S.A.; Rudhziah, S.; Ahmad, A.; Mohamed, N.S. Biopolymer Electrolyte Based on Derivatives of Cellulose from Kenaf Bast Fiber. Polymers 2014, 6, 2371-2385. https://doi.org/10.3390/polym6092371
Rani MSA, Rudhziah S, Ahmad A, Mohamed NS. Biopolymer Electrolyte Based on Derivatives of Cellulose from Kenaf Bast Fiber. Polymers. 2014; 6(9):2371-2385. https://doi.org/10.3390/polym6092371
Chicago/Turabian StyleRani, Mohd Saiful Asmal, Siti Rudhziah, Azizan Ahmad, and Nor Sabirin Mohamed. 2014. "Biopolymer Electrolyte Based on Derivatives of Cellulose from Kenaf Bast Fiber" Polymers 6, no. 9: 2371-2385. https://doi.org/10.3390/polym6092371