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Nanomaterials 2013, 3(1), 117-125; doi:10.3390/nano3010117

A Novel Fluoride Route for the Synthesis of Aluminosilicate Nanotubes

Equipe Matériaux à Porosité Controlée (MPC), Institut de Science des Matériaux de Mulhouse (IS2M), CNRS UMR 7361, Université de Haute Alsace (UHA), ENSCMu, 3b rue Alfred Werner, 68093 Mulhouse Cedex, France
Author to whom correspondence should be addressed.
Received: 8 November 2012 / Revised: 28 January 2013 / Accepted: 29 January 2013 / Published: 6 February 2013
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In this work we present a novel method for synthesis of aluminosilicate nanotubes: the fluoride route. F-containing imogolite (F-IMO) exhibits an improved crystallization rate and improved yield. The structure of F-IMO was investigated and compared with F-free imogolite (IMO) by means of X-ray diffraction (XRD) and Fourier transformed infrared spectroscopy (FTIR) confirming imogolite structure. Solid state nuclear magnetic resonance (NMR) analyses show an increased crystallization rate for F-IMO and confirm the incorporation of fluorine ion in the structure.
Keywords: aluminosilicate nanotube; imogolite; fluoride route; synthesis aluminosilicate nanotube; imogolite; fluoride route; synthesis

This is an open access article distributed under the Creative Commons Attribution License (CC BY 3.0).

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MDPI and ACS Style

Chemmi, A.; Brendlé, J.; Marichal, C.; Lebeau, B. A Novel Fluoride Route for the Synthesis of Aluminosilicate Nanotubes. Nanomaterials 2013, 3, 117-125.

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