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Article
Peer-Review Record

Thermo-Responsive ZnPc-g-TiO2-g-PNIPAM Photocatalysts Sensitized with Phthalocyanines for Water Purification under Visible Light

Molecules 2022, 27(10), 3330; https://doi.org/10.3390/molecules27103330
by Bingxin Mao 1, Cong Liu 1, Xu Cui 1,*, Yanhui Li 1 and Qian Duan 1,2,*
Reviewer 1: Anonymous
Reviewer 2:
Molecules 2022, 27(10), 3330; https://doi.org/10.3390/molecules27103330
Submission received: 26 April 2022 / Revised: 14 May 2022 / Accepted: 20 May 2022 / Published: 22 May 2022
(This article belongs to the Section Photochemistry)

Round 1

Reviewer 1 Report

The artcile concernes interisting topic about TiO2 sensibilization. There are a few points which can be improved:

  1. I think it's worth adding a description of XPS peaks of O and N elements
  2. Please add a scale in Fig. S1. Also, there are not EDS spectrum, which are mentioned in the caption. 
  3. How were the specific surface areas of 64.38 m2/g and 35.55 m2/g defined? When using the BET method, this is too high accuracy. 
  4. Please add label to axis Y in Fig. 5a. Acording 5b: the tangent line for modified TiO2 (blue line) is incorrectly. Actually, I do not think one can define the band gap in this case.
  5. Line 180-181: "the removal efficiency could reach 31.9 % in 75 min under visible light in Fig. S6". But in Fig. S6 one can see the increase in adsorption after 75 min. Please clarify.
  6. I would recommend to add information about errors to the figures presented catalytic results.
  7. Experimental details about reactor for photocatalytic tests are necessary. 

Author Response

Please see the attachment.

Author Response File: Author Response.pdf

Reviewer 2 Report


Comments for author File: Comments.pdf

Author Response

Please see the attachment

Author Response File: Author Response.pdf

Round 2

Reviewer 1 Report

The article can be published

Reviewer 2 Report

The authors responded to the comments  and revised the manuscript and it is ready to be published.

 

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