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Article

Synthesis, Characterization, and Properties of High-Energy Fillers Derived from Nitroisobutylglycerol

by
Sergey A. Rzhevskiy
1,
Lidiya I. Minaeva
1,
Maxim A. Topchiy
1,
Igor N. Melnikov
2,
Vitaly G. Kiselev
3,
Alla N. Pivkina
2,
Igor V. Fomenkov
4 and
Andrey F. Asachenko
1,*
1
A.V. Topchiev Institute of Petrochemical Synthesis, Russian Academy of Sciences, Leninsky Prospect 29, 119991 Moscow, Russia
2
Semenov Federal Research Center for Chemical Physics RAS, 4 Kosygina Str., 119991 Moscow, Russia
3
Institute of Chemical Kinetics and Combustion SB RAS, 3 Institutskaya Str., 630090 Novosibirsk, Russia
4
Zelinsky Institute of Organic Chemistry RAS, 47 Leninsky Ave., 119991 Moscow, Russia
*
Author to whom correspondence should be addressed.
Int. J. Mol. Sci. 2023, 24(10), 8541; https://doi.org/10.3390/ijms24108541
Submission received: 3 April 2023 / Revised: 3 May 2023 / Accepted: 8 May 2023 / Published: 10 May 2023
(This article belongs to the Section Macromolecules)
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Abstract

Herein we report a comprehensive laboratory synthesis of a series of energetic azidonitrate derivatives (ANDP, SMX, AMDNNM, NIBTN, NPN, 2-nitro-1,3-dinitro-oxypropane) starting from the readily available nitroisobutylglycerol. This simple protocol allows obtaining the high-energy additives from the available precursor in yields higher than those reported using safe and simple operations not presented in previous works. A detailed characterization of the physical, chemical, and energetic properties including impact sensitivity and thermal behavior of these species was performed for the systematic evaluation and comparison of the corresponding class of energetic compounds.
Keywords: energetic compounds; high-energy additives; nitroisobutylglycerol; comprehensive study; physiochemical and energetic properties energetic compounds; high-energy additives; nitroisobutylglycerol; comprehensive study; physiochemical and energetic properties

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MDPI and ACS Style

Rzhevskiy, S.A.; Minaeva, L.I.; Topchiy, M.A.; Melnikov, I.N.; Kiselev, V.G.; Pivkina, A.N.; Fomenkov, I.V.; Asachenko, A.F. Synthesis, Characterization, and Properties of High-Energy Fillers Derived from Nitroisobutylglycerol. Int. J. Mol. Sci. 2023, 24, 8541. https://doi.org/10.3390/ijms24108541

AMA Style

Rzhevskiy SA, Minaeva LI, Topchiy MA, Melnikov IN, Kiselev VG, Pivkina AN, Fomenkov IV, Asachenko AF. Synthesis, Characterization, and Properties of High-Energy Fillers Derived from Nitroisobutylglycerol. International Journal of Molecular Sciences. 2023; 24(10):8541. https://doi.org/10.3390/ijms24108541

Chicago/Turabian Style

Rzhevskiy, Sergey A., Lidiya I. Minaeva, Maxim A. Topchiy, Igor N. Melnikov, Vitaly G. Kiselev, Alla N. Pivkina, Igor V. Fomenkov, and Andrey F. Asachenko. 2023. "Synthesis, Characterization, and Properties of High-Energy Fillers Derived from Nitroisobutylglycerol" International Journal of Molecular Sciences 24, no. 10: 8541. https://doi.org/10.3390/ijms24108541

APA Style

Rzhevskiy, S. A., Minaeva, L. I., Topchiy, M. A., Melnikov, I. N., Kiselev, V. G., Pivkina, A. N., Fomenkov, I. V., & Asachenko, A. F. (2023). Synthesis, Characterization, and Properties of High-Energy Fillers Derived from Nitroisobutylglycerol. International Journal of Molecular Sciences, 24(10), 8541. https://doi.org/10.3390/ijms24108541

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