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Article

The Measurement Uncertainty in Determining of Electrical Resistance Value by Applying Direct-Comparison Method

Faculty of Science, University of Split, Ruđera Boškovića 33, 21000 Split, Croatia
*
Author to whom correspondence should be addressed.
Energies 2022, 15(6), 2115; https://doi.org/10.3390/en15062115
Submission received: 20 February 2022 / Revised: 9 March 2022 / Accepted: 12 March 2022 / Published: 14 March 2022
(This article belongs to the Topic Advanced Systems Engineering: Theory and Applications)

Abstract

:
This paper considers the unknown electrical resistance (measurand) as the numerical result of the measurement that was carried out by means of the well-known direct comparison measurement method using an appropriate standard resistor and voltmeter. In the literature, this measurement method is also referred to as a series comparison method. This method of measurement is one of the indirect methods and is suitable for measuring low resistance. This paper presents two approaches for evaluating the unknown electrical resistance and its associated combined standard uncertainty. The entire process of evaluating the combined standard uncertainty that is associated with the measurand and the standard uncertainties that are associated with the analyzed input quantities has been entirely performed in accordance with the applicable international recommendations and guidelines for the uncertainty of measurement. The analyzed approaches for evaluating the combined standard uncertainty are designed to be universal and valid both for the mutually non-correlated input quantities and for the mutually correlated input quantities, which can be obtained from a single observation, or repeated observations or by other means. This paper can substantially contribute to the measurements in electrical engineering and education.

1. Introduction

When the result of a quantity measurement is reported, it requires the estimated value of the measurand (the quantity to be measured) and the uncertainty that is associated with that value. The uncertainty of measurement as an attribute for expressing the quality of a measurement result is relatively new in the history of measurement. The acceptance of uncertainty of measurement as a unique numerical expression of the measurement result quality ensued from many years of discussions resulting in international agreements that are outlined in the guidelines [1]. That authoritative document is popularly known as the GUM, (which stands for guide to the expression of uncertainty in measurement). The GUM indicates that the formal definition of “uncertainty of measurement” refers to a parameter that is associated with the measurement result characterizing the dispersion of values that are reasonably attributable to the measurand. Correspondingly, other standards and guides, such as [2,3], are strictly based on the guide.
For many years, the determination and expression of uncertainty in measurement has been subject to debate in several global metrological organizations (IEC, BIMP, ISO, etc.) around the world for many years. Several recommendations, guidelines, and instructions have been generated therefrom. The latest internationally accepted document for the expression of uncertainty in measurement is [2], which was adopted by the European Cooperation for Accreditation (EA).
For many purposes, unknown resistors are compared to standard resistors by a comparison circuit. One such measurement method is the direct comparison measurement method using a standard resistor and a voltmeter. There are other similar methods, such as the substitution method and the direct comparison method using a standard resistor and potentiometer, to which the same procedure for evaluating and expressing uncertainty in measurement may apply as the procedure that is described in this scientific paper. Thus far, the literature has reported only the numerical value of the unknown resistance that is obtained by means of the direct comparison method, rarely considering the internal resistance of the voltmeter [4,5,6,7,8,9,10,11].
In general, every value that is obtained through measurement has some uncertainty, and even though uncertainty may be reduced by thorough planning, a prudent selection of a measuring instrument, and a careful execution of the experiment, it cannot be eliminated entirely. Therefore, the main goal of this paper is to calculate the value of the unknown electrical resistance using this direct comparison method, as well as to evaluate the associated uncertainty of measurement according to [1,2].
In the proposed model, a measurand (output quantity) RX is not measured directly, but it is determined from four quantities (input quantities: resistance of a standard resistor RN, input resistance of used voltmeter RV, the voltage drop UN across resistor RN, and the voltage drop UX across resistor RX) through a functional relationship f(∙), also referred to as the measurement model function. This functional relationship f(∙) is based on the theory of a voltage divider. This paper provides a detailed description of the determination of the measurand RX and its combined standard uncertainty uC(RX). Generally, the determination of the combined standard uncertainty of a non-directly measured measurand (output quantity) is described in many textbooks [12,13,14,15,16,17,18]. Ref. [19] provides a simplified form of the output quantity RX evaluation when it is determined from only three input quantities, RN, UN, and UX, by applying the direct comparison measurement method using a standard resistor and voltmeter, in addition to the evaluation of the combined standard uncertainty that is associated with this RX. Unlike the aforementioned research, the model that is proposed in this paper is more comprehensive and analyzed in more detail. The output quantity RX in this model is determined from either four mutually non-correlated or four mutually independent input quantities, which can be obtained from a single observation, repeated observations, or by other means.
According to [1,2], the steps for evaluating and expressing uncertainty in the measurement of the unknown electrical resistance that is determined according to the proposed method may be summarized as follows:
  • Determination of the functional relationship f(∙) (measurement model function) between the unknown electrical resistance RX (output quantity) and the input quantities, on which it depends. This functional relationship should contain every quantity, including all corrections and correction factors, that can add a significant component of uncertainty to the measurement result.
  • Determination of the estimated value of each input quantity in the relationship, which can be obtained from a single observation, repeated observations, or by other means.
  • Evaluation of the standard uncertainty of each input-estimated quantity. Type A evaluation of the standard uncertainty will be evaluated for an input estimate that is obtained from the statistical analysis of a series of observations, and Type B evaluation of standard uncertainty will be evaluated for an input estimate that is obtained from a single observation or by other means.
  • Evaluation of the covariances that are associated with any correlated input estimates.
  • Calculation of the measurement result.
  • Determination of the combined standard uncertainty of the measurement result from the standard uncertainties and covariances that are associated with the input-estimated quantities that were obtained in step 2.
  • If necessary, the determination of an expanded uncertainty.
  • Presentation of the measurement result.
An illustrative example that is presented at the end of this paper describes the practical application of the proposed measurement method.
The main contributions and originality of the proposed model include:
  • the new and the original form of the mathematical expression for the calculation of the electrical resistance value, which is extremely suitable for conducting higher-order partial derivatives which can be of great importance when the model of measurement functions has a nonlinear character,
  • the complete the measurement model function,
  • the method that is proposed in this paper allows the elimination of the influence of thermo-electrical voltages, if any,
  • the proposed model includes the cases where the input quantities are correlated and mutually independent,
  • the proposed model can be used in the determination of the electrical resistance value by means of the direct comparison method using a standard resistor and potentiometer, and in case when the unknown resistors are compared to standard resistors by a comparison circuit (comparators).

2. Direct Comparison Method Using a Standard Resistor and Voltmeter

In this method, the unknown resistor RX, the standard resistor RN and a current source are connected in series, as shown in Figure 1, and a voltmeter is used to measure the voltage drop across each resistor.

2.1. Formulation of the Functional Relationship (Measurement Equation)

This measurement method is based on the principle of a voltage resistive divider. In this case, a simple example of a voltage resistive divider is presented by two resistors that are connected in a series with the input DC voltage applied across the resistor pair, Figure 2. One of them has the unknown electrical resistance RX and the second one is a standard resistor with the known electrical resistance RN. According to the principle of a voltage resistive divider, the well-known equation applies:
I = U X R X = U N R N U X U N = R X R N
Deriving from (1), the value of the unknown resistance RX is:
R X = R N U X U N
If the unknown resistance RX is to be determined by measuring the voltage UN and UX using a voltmeter according to Figure 1, then (2) would be valid only if the measurement is performed by using an ideal voltmeter (voltmeter with an infinitely large internal resistance). However, although the voltmeters typically have a large internal resistance RV, they introduce systematic effects in the measurement of electrical voltage, which in some circumstances may be neglected, and considered in others.
Due to this internal resistance of the voltmeter, a systematic effect occurs in the above voltage measurement, so the measured voltage values UX and UN will also contain this systematic effect.
In order to minimize and ignore the systematic effect, the following conditions must be met:
(a)
During the measurement of voltages UX and UN, the current I in the circuit shown in Figure 1 must remain unchanged, respectively
U 0 R N + R X R V = U 0 R X + R N R V = I = constant
which is achieved by using a highly stabilized DC power source or by adjusting the variable resistor Rp (see Figure 3).
(b)
During the measurement of voltages UX and UN, the value of the internal resistance of the voltmeter RV should remain unchanged, which is achieved if both the measurements are performed within the same voltmeter measuring range.
(c)
The resistance values of RX and RN should be approximately in the same order of magnitude and significantly lower (102 to 104 times less) than the voltmeter resistance value RV. Therefore, this measurement method is commonly used when measuring the low resistance values RX (up to a few kΩ only).
If voltages UX and UN are measured simultaneously using the same high-resolution voltmeter while maintaining the same measuring range and without changing the current intensity during the measurement, the systematic effects in measuring these voltages can be neglected (Figure 1). In this case, no correction of the calculated value of the unknown resistance RX is required, which can be derived from (2), as corroborated by the following observation.
The voltage UN can be derived from Figure 1 by the following expression:
U N = U 0 ( R N R V ) R X + ( R N R V ) = I R N R V R N + R V
Analogously, the voltage UX can be derived from Figure 2 by the expression:
U X = U 0 ( R X R V ) R N + ( R X R V ) = I R X R V R X + R V
Dividing (5) by (4), with the fulfilled conditions (a), (b) and (c) and by using (1), the following equation is obtained:
U X U N = R X R N R X + R V R N + R V = R X R N R X / R V 0 + 1 R N / R V 0 + 1 = R X R N
It is evident from Equations (2) and (6) that the value of the unknown resistance RX is independent of the connected voltage U0, the current I, or the internal resistance of the voltmeter RV. That means that this method of comparing the voltage with the fulfilled conditions (a), (b), and (c) is exempt from the systematic voltage deviation. Hence, we obtain the following simplified measurement model function:
R X = f ( R N , U N , U X )
In practice, the following circuit diagrams are commonly used to measure small resistances using the direct comparison method (Figure 3a). The variable resistor Rp adjusts the current intensity I so that it remains unaltered during voltages measurement and lower than the continuous allowed current intensity through the RX and RN resistors. That is controlled by means of an ammeter.
The method of four-terminal (four-wire) connections for electrical resistance measurement (according to Figure 3b) is used for precise measurement and for measuring low electrical resistances. The four-terminal (four-wire) connection of both the measured resistor and the standard resistor is the most accurate method when measuring circuits below 10 ohms, as this method eliminates the influence of the terminal resistances and the resistances of connecting wires.
If conditions (a) and (b) are met, but condition (c) is not, the internal resistance of the RV voltmeter must be considered when determining the unknown resistance RX. Hence, dividing (5) by (4) we obtain:
R X = R N U X U N R V R V + R N ( 1 U X U N ) = [ U N U X ( 1 R N + 1 R V ) 1 R V ] 1
According to (8), the measurand (output quantity) RX is not measured directly, but it is determined from four other quantities (input quantities), RN, RV, UN, and UX, through a functional relationship f(∙) (measurement model function):
R X = f ( R N , R V , U N , U X )
The complete model function (9) is an algorithm that must be evaluated numerically.
The input quantities RN, RV, UN, and UX upon which the output quantity RX depends may be viewed as the measurands themselves and depend on other quantities, including corrections and correction factors for systematic effects, thereby leading to a complicated functional relationship f(∙) that may never be explicitly noted. No further dependence of the input quantities RN, RV, UN, and UX on other quantities will be considered in this paper.

2.2. Evaluation of the Input Quantities and Their Standard Uncertainties

In order to obtain the numerical value of the unknown resistance RX, according to (8), the measurements of voltage drops UN and UX are required, as well as the appropriate value of standard resistor RN.
Each of the input quantities in the model function (9) indicates not only their estimated value, but also their standard uncertainty. With the model function (9), both the output estimated value and the standard uncertainty are then calculated considering the GUM rules.
An estimate of the measurand RX, denoted by R1X, is obtained from (9) by using input estimates R1N, R1V, U1N, and U1X for the values of the four input quantities RN, RV, UN, and UX. Hence, the output estimate R1X, which is the numerical result of the measurement, is given by
R 1 X = f ( R 1 N , R 1 V , U 1 N , U 1 X )
Since the input estimates R1N, R1V, U1N, and U1X in (10) refer to the measurement results, each of them has an associated standard uncertainty u(R1N), u(R1V), u(U1N), and u(U1X), which may contribute to the standard uncertainty of the final measurement result R1X. The sets of input quantities R1N, R1V, U1N, and U1X are categorized as quantities whose values and uncertainties are directly determined in the current measurement. These values and uncertainties are obtained from a single observation, repeated observations, or by other means, and may involve the determination of corrections of instrument readings and corrections of influence quantities, such as ambient temperature, barometric pressure, and humidity.
In general, the uncertainty of the measurement comprises many components. Some of these components may be evaluated from the statistical distribution of the results of a series of measurements and characterised by experimental standard deviations. The other components, which can also be characterized by standard deviations, are evaluated from the assumed probability distributions based on experience or other information.
In the following section, we will consider the evaluation of the input estimates U1N and U1X and their associated standard uncertainties u(U1N) and u(U1X), which can be obtained either from the statistical analysis of a series of individual measurements under identical experimental conditions (repeatability conditions)—repeated observations, or from a single observation.
The mean estimate of the supposed distribution of the values is taken as the value of the input quantity, and the estimation of the standard deviation of the mean estimate is taken as the standard uncertainty.
Hence, for the input quantity U1N that is estimated from n independent repeated observations U1N,k (k = 1, , n), the arithmetic mean U ¯ 1 N is obtained from equation
U ¯ 1 N = 1 n k = 1 n U 1 N , k
is used as the input estimate U1N in (10) to determine the measurement result R1X; i.e.,
U 1 N = U ¯ 1 N
Analogously, for the input quantity U1X that is estimated from n independent repeated observations U1X,k (k = 1, , n), the arithmetic mean U ¯ 1 X is obtained from equation:
U ¯ 1 X = 1 n k = 1 n U 1 X , k
is used as the input estimate U1X in (10) to determine the measurement result R1X; i.e.,
U 1 X = U ¯ 1 X
If the input estimates U1N and U1X are obtained from the repeated observations, their associated standard uncertainties are evaluated as Type A evaluation of standard uncertainties uA(U1N) and uA(U1X), respectively. Standard uncertainty uA(U1N) is defined as an estimate of the standard deviation of the distribution of values, termed the experimental standard deviation s(U1N). The experimental standard deviation provided a quantitative estimate of the dispersion of the possible measured values U1N,k (k = 1, , n), about their mean value U ¯ 1 N , and it is given by
u A ( U 1 N ) s ( U 1 N ) = 1 n 1 k = 1 n ( U 1 N , k U ¯ 1 N ) 2
Analogously, the standard uncertainty uA(U1X) is defined as an estimate of the standard deviation s(U1X) and is given by
u A ( U 1 X ) s ( U 1 X ) = 1 n 1 k = 1 n ( U 1 X , k U ¯ 1 X ) 2
The best estimate for the standard uncertainty uA(U1N) to be associated with U1N is the experimental standard deviation of the mean and is given by
u A ( U 1 N ) = u A ( U ¯ 1 N ) = s ( U ¯ 1 N ) = = 1 n ( n 1 ) k = 1 n ( U 1 N , k U ¯ 1 N ) 2    ( n 10 )
The best estimate for the standard uncertainty uA(U1X) to be associated with U1X is the experimental standard deviation of the mean and is given by
u A ( U 1 X ) = u A ( U ¯ 1 X ) = s ( U ¯ 1 X ) = = 1 n ( n 1 ) k = 1 n ( U 1 X , k U ¯ 1 X ) 2    ( n 10 )
Those input estimates which are not evaluated from the repeated observations must be obtained by other methods, such as those that are indicated in the second category of 4.1.3 in [1].
If the input estimates U1N and U1X are obtained by means of the same voltmeter from a single observation, their standard uncertainties are evaluated as Type B evaluation of standard uncertainties. Presuming that the values of the input estimates U1N and U1X are estimated from an assumed rectangular probability distribution of a lower limit a and an upper limit a+, the input estimate U1N is usually the expectation of the rectangular probability distribution
U 1 N = a + + a 2
while the standard uncertainty uB(U1N) to be associated with U1N is the positive square root of the distribution variance
u B ( U 1 N ) = a + a 2 3 ( V )
If a + = a = a then
U 1 N = a
and
u B ( U 1 N ) = σ = a 3 ( V )
The input estimate U1X can also be obtained by means of (19). Type B evaluation of standard uncertainty uB(U1X) to be associated with U1X can also be derived from (22).
Let us also suppose that the manufacturer accuracy specifications are available for the used voltmeter and that, for the considered range, they provide an interval of possible values, whose half-amplitude a is provided for:
- an analogous voltmeter (such as PMMC voltmeter) by means of:
a = C M 100 ( V )
where C refers to the accuracy class of the analogous voltmeter (%), and M to the maximum value of the voltmeter (V) measuring range;
- a digital voltmeter by means of any combination of two or three terms on the right side of the following expression:
a = p 1 100 X D V + p 2 100 M D V + N D ( V )
where
p1—percentage of the voltmeter reading (%),
p2—percentage of the voltmeter range (%),
XDV—reading value of the used digital voltmeter (V). In our proposed model XDV = U1N or XDV = U1X,
MDV—selected measurement range of the digital voltmeter (V), and
ND—number of digits, where the lexeme digit, sometimes confused with the lexeme count due to its similar meaning, indicates the value of the less significant digit for the range in use. The number of digits represents the resolution of the instrument for that range.
Sometimes these combinations also include the absolute value of the measured quantity (volt, ohms, ampere…).
According to the manufacturer of the voltmeter, the interval U1N ± a encompasses all the values that are reasonably attributable to the estimate U1N, hence its coverage probability is, therefore, 100%. In addition, the interval U1X ± a encompasses all the values that are reasonably attributable to the estimate U1X, hence its coverage probability is 100%.
Let us also suppose that the manufacturer’s specification is available for the used standard resistor RN. The nominal value of standard resistor RN, that is selected from the manufacturer’s specification, will be taken as the input estimate R1N. Usually, the nominal values of standard resistors are given with the tolerance band ± Δ R N , max or with the standard resistor tolerance δ R N , max (%).
For the input estimate R1N, the standard uncertainty is also considered as Type B evaluation of standard uncertainty. Type B evaluation is founded on the assumption of rectangular (uniform) probability distribution and the manufacturer’s specification for the selected standard resistor R1N. The standard uncertainty uB(R1N) to be associated with R1N is given by
u B ( R 1 N ) = σ = Δ R N , max 3 = δ R N , max / 100 3 R N [ Ω ]
where
RN—nominal value of standard resistor (Ω)
δ R N , max —tolerance of the standard resistor RN (%).
Presuming that the manufacturer’s specification of the used voltmeter provides the data for the internal resistance of the used voltmeter RV, the nominal value of the input resistance RV will be taken as the input estimate R1V. Since the manufacturer does not provide any additional information about the tolerance (%) of this resistance, apart from the internal resistance of the voltmeter RV, we can ignore the standard uncertainty uB(R1V) to be associated with R1V.
This is also permitted in [1], where it has been indicated that in some cases the uncertainty of a correction of a systematic effect does not need to be included in the evaluation of the uncertainty of a measurement result. Although the uncertainty has been evaluated, it may be ignored if its contribution to the combined standard uncertainty of the measurement result is insignificant, since the internal resistance of the voltmeters is very large in relation to the measured resistance.

2.3. Evaluation of Output Quantity and Its Uncertainty

In view of the above, the output estimate R1X is the numerical result of the measurement, and it can be calculated by means of (10), which is obtained from (9) when the unknown input quantities RN, RV, UN, and UX are replaced by the corresponding estimates R1N, R1V, U1N, and U1X that are obtained from the measurements. According to [1], the output estimate R1X may be obtained by means of the two following approaches:
The output estimate R1X is taken as the functional relationship f(∙) from the arithmetic means U ¯ 1 N and U ¯ 1 X , the nominal values of the standard resistor R1N and the internal resistance of voltmeter R1V, i.e.,
R 1 X = f ( R 1 N , R 1 V , U ¯ 1 N , U ¯ 1 X )
where U ¯ 1 N and U ¯ 1 X are obtained by means of (11) and (13), respectively.
The output estimate R1X is taken as the arithmetic mean or average of n independent determinations R1X,k (k = 1, , n) of RX, each determination having the same uncertainty and each being based on a complete set of observed values of the four input estimates R1N, R1V, U1N, and U1X that are obtained simultaneously, i.e.,
R 1 X = R ¯ X = 1 n k = 1 n R X , k = 1 n k = 1 n f ( R N , k , R V , k , U N , k , U X , k )
The output estimate R1X is obtained by means of (27) may be preferable when the measurement model function f(∙) is a nonlinear function, but the two approaches are identical if f(∙) is a linear function of the input quantities (provided that the experimentally observed correlation coefficients are taken into account when implementing the first approach). In the measurement practice, the value of the uncertainty of the measurement is generally low with respect to the measured value, hence it determines small variations of the measurand. This means that the linearity condition of f(∙) is almost always locally verified, near the measurement point.
Presuming that the function f(∙) in (10) is fairly linear, about the measured value R1X, at least for small deviations of each of the four input quantities RN, RV, UN, and UX, about their estimates R1N, R1V, U1N, and U1X, respectively. When the input quantities U1N,k and U1X,k (k = 1, , n) are correlated in the repeated observations assuming that that function f() in (10) is fairly linear, about the measured value R1X, then the determination of the output estimate R1X by means of (26) will be more convenient for further analysis.
The standard uncertainty of the result of the measurement R1X, which is obtained from the values of the four input quantities RN, RV, UN, and UX, is termed a combined standard uncertainty and denoted by uC(R1X). In the general case, with the correlated estimates of the input values and assuming that the measurement model function f(∙) is a linear function, the combined standard uncertainty uC(R1X) of the measurement result R1X is the estimated standard deviation that is associated with the result R1X and is equal to the positive square root of the combined variance u C 2 ( R 1 X ) that is obtained from the following variance and covariance components
u C 2 ( R 1 X ) = ( f R 1 N ) 2 u B 2 ( R 1 N ) + ( f R 1 V ) 2 u B 2 ( R 1 V ) + ( f U ¯ 1 X ) 2 u 2 ( U ¯ 1 X ) + ( f U ¯ 1 N ) 2 u 2 ( U ¯ 1 N ) + + 2 f U ¯ 1 N f U ¯ 1 X u ( U ¯ 1 N , U ¯ 1 X ) + 2 f R 1 N f R 1 V u ( R 1 N , R 1 V ) + + 2 f U ¯ 1 N f R 1 N u ( U ¯ 1 N , R 1 N ) + 2 f U ¯ 1 N f R 1 V u ( U ¯ 1 N , R 1 V ) + + 2 f U ¯ 1 X f R 1 N u ( U ¯ 1 X , R 1 N ) + 2 f U ¯ 1 X f R 1 V u ( U ¯ 1 X , R 1 V )
where
u B ( R 1 N ) —Type B evaluation of standard uncertainty that is associated with the input estimate R1N, which can be obtained by means of (22),
u B ( R 1 V ) —Type B evaluation of standard uncertainty that is associated with the input estimate R1V, which can be obtained by means of (22),
u ( U ¯ 1 N ) —may be Type A or either Type B evaluation of standard uncertainty that is associated with the input estimate U1N. Type A evaluation can be obtained by means of (17) and Type B evaluation can be obtained by means of (22),
u ( U ¯ 1 X ) —may be Type A or either Type B evaluation of standard uncertainty that is associated with the input estimate U1X. Type A evaluation can be obtained by means of (18) and Type B evaluation can be obtained by means of (22),
u ( U ¯ 1 N , U ¯ 1 X ) —estimate of the covariance of input means U ¯ 1 N and U ¯ 1 X ,
u(R1N, R1V)—estimate of the covariance of input estimates R1N and R1V,
u ( U ¯ 1 N , R 1 N ) —estimate of the covariance of input mean U ¯ 1 N and input estimate R1N,
u ( U ¯ 1 N , R 1 V ) —estimate of the covariance of input mean U ¯ 1 N and input estimate R1V,
u ( U ¯ 1 X , R 1 N ) —estimate of the covariance of input mean U ¯ 1 X and input estimate R1N,
u ( U ¯ 1 X , R 1 V ) —estimate of the covariance of input mean U ¯ 1 X and input estimate R1V.
The partial derivatives f R 1 N , f R 1 V , f U ¯ 1 N and f U ¯ 1 X (often referred to as sensitivity coefficients) are equal to f R N , f R V , f U N and f U X evaluated at RN = R1N, RV = R1V, U N = U ¯ 1 N , and U X = U ¯ 1 X , respectively.
Equation (28) is based on the first-order Taylor series approximation of the model function of the measurement R X = f ( R N , R V , U N , U X ) and it expresses what is termed in the Guide [1] as the law of propagation of uncertainty.
It is noted in [1] that the covariance that is associated with the estimates of two input quantities may be taken to be zero or treated as insignificant if
  • these input quantities are uncorrelated,
  • either of these two input quantities can be treated as a constant, or if
  • there is insufficient information to evaluate the covariance that is associated with the estimates of these two input quantities.
Hence, considering that the estimates R1N and R1V are constant during the measurement by the proposed method, then the estimated covariances u(R1N, R1V), u ( U ¯ 1 N , R 1 N ) , u ( U ¯ 1 N , R 1 V ) , u ( U ¯ 1 X , R 1 N ) , and u ( U ¯ 1 X , R 1 V ) may be ignored in (28). Since it frequently occurs that no associated uncertainty uB(R1V) is stated in the manufacturer’s specification of the voltmeter, it can also be ignored in (28).
In accordance with this explanation, Equation (28) is reduced and may be rendered as follows
u C 2 ( R 1 X ) = ( f R 1 N ) 2 u B 2 ( R 1 N ) + ( f U ¯ 1 X ) 2 u 2 ( U ¯ 1 X ) + + ( f U ¯ 1 N ) 2 u 2 ( U ¯ 1 N ) + 2 f U ¯ 1 N f U ¯ 1 X u ( U ¯ 1 N , U ¯ 1 X )
The partial derivatives or sensitivity coefficients in (29) are evaluated by means of the following expressions:
f R 1 N = U ¯ 1 N U ¯ 1 X 1 R 1 N 2 [ U ¯ 1 N U ¯ 1 X ( 1 R 1 N + 1 R 1 V ) 1 R 1 V ] 2
f U ¯ 1 X = U ¯ 1 N U ¯ 1 X 2 ( 1 R 1 N + 1 R 1 V ) [ U ¯ 1 N U ¯ 1 X ( 1 R 1 N + 1 R 1 V ) 1 R 1 V ] 2
and
f U ¯ 1 N = 1 U ¯ 1 X ( 1 R 1 N + 1 R 1 V ) [ U ¯ 1 N U ¯ 1 X ( 1 R 1 N + 1 R 1 V ) 1 R 1 V ] 2 .
where U ¯ 1 N and U ¯ 1 X are obtained by means of (11) and (13), respectively.
The terms u ( U ¯ 1 N , U ¯ 1 X ) in (28) represent the estimate of the covariance of input means U ¯ 1 N and U ¯ 1 X , determined from n independent pairs of repeated simultaneous observations U1N,k and U1X,k (k = 1, …., n) of the estimates U1N and U1X. If there are n pairs of measured results of independent repeated measurements of the estimates U1N and U1X, then the covariance u ( U ¯ 1 N , U ¯ 1 X ) as a statistical measurement of the strength of the correlation between these n pairs of the estimates can be calculated by the following equation:
u ( U ¯ 1 N , U ¯ 1 X ) = u ( U ¯ 1 X , U ¯ 1 N ) = 1 N ( N 1 ) k = 1 N ( U 1 N , k U ¯ 1 N ) ( U 1 X , k U ¯ 1 X )
The degree of correlation between u ( U ¯ 1 N ) and u ( U ¯ 1 X ) is characterized by the estimated correlation coefficient of input means U ¯ 1 N and U ¯ 1 X , defined as
r ( U ¯ 1 N , U ¯ 1 X ) = r ( U ¯ 1 X , U ¯ 1 N ) = u ( U ¯ 1 N , U ¯ 1 X ) u ( U ¯ 1 N ) u ( U ¯ 1 X ) 1 r ( U ¯ 1 N , U ¯ 1 X ) 1
In terms of the correlation coefficients, which are more readily interpreted than covariances, and by using (34), Equation (29) may be written as
u C 2 ( R 1 X ) = ( f R 1 N ) 2 u B 2 ( R 1 N ) + ( f U ¯ 1 X ) 2 u 2 ( U ¯ 1 X ) + ( f U ¯ 1 N ) 2 u 2 ( U ¯ 1 N ) + + 2 f U ¯ 1 N f U ¯ 1 X u ( U ¯ 1 N ) u ( U ¯ 1 X ) r ( U ¯ 1 N , U ¯ 1 X )
which is also known as the general formulation of the law of propagation of uncertainty [1].
With the uncorrelated estimates of the input values, r ( U ¯ 1 N , U ¯ 1 X ) = 0 , and consequently
u C 2 ( R 1 X ) = ( f R 1 N ) 2 u B 2 ( R 1 N ) + ( f U ¯ 1 X ) 2 u 2 ( U ¯ 1 X ) + ( f U ¯ 1 N ) 2 u 2 ( U ¯ 1 N )
The uncertainty propagation law (35) (or its simplified version (36) in case of the uncorrelated input quantities) can be used to evaluate the combined standard uncertainty u C ( R 1 X ) of the result of the unknown resistance measurement when the measurand RX is not measured directly, but is determined from the four input quantities RN, RV, UN, and UX according to (8), while the standard uncertainties of their estimates are known. The combined standard uncertainty u C ( R 1 X ) is an estimated standard deviation and it indicates the dispersion of the values that are reasonably attributable to the measurand RX. The resulting combined standard uncertainty can be used to obtain an expanded uncertainty with a provided coverage probability.

2.4. Evaluation of Output Quantity and Its Uncertainty Considering Thermo-Electrical Voltages

Thermoelectric voltages can seriously affect the low resistance measurement accuracy. The current reversal method, the delta method, and the offset-compensated ohms method are three common ways to overcome these unwanted offsets. When the thermoelectric voltages are constant with respect to the measurement cycle, the current-reversal method will successfully compensate for these offsets. However, if the changing thermoelectric voltages are causing inaccurate results, then the delta method should be used. The delta method is similar to the current reversal method in terms of alternating the current source polarity, but it differs in using three voltage measurements to perform each resistance calculation. The current reversal method provides a twice better signal-to-noise ratio and, therefore, better accuracy than the offset-compensated ohms method. Hence, in this paper we will use the current reversal method to cancel the thermoelectric voltage, which is also used in [19].
Thermoelectric voltages can be cancelled by making two measurements with the currents of opposite polarity, as shown in Figure 3b. This can be achieved by measuring the voltages UN and UX for both polarities of the power supply (measuring first the voltage UN for both polarities, and afterwards the voltage UX for both polarities). The averaging of the voltage measurement results by both polarities of the power supply, i.e.,
U 1 N = U 1 N + U 1 N - 2
and
U 1 X = U 1 X + U 1 X - 2 ,
allows the elimination of the influence of thermo-electrical voltages. In the case of several repeated voltage measurements, substituting the voltage results from (37) and (38) into (11) and (13), and then into (8), will provide an estimation of the unknown resistance R1X. In the case of a single observation of the voltages UN and UX, the results from (37) and (38) are immediately substituted in (8). It is noted that the thermoelectric voltages are completely cancelled out by this approach.
Type A evaluation of standard uncertainty u ( U ¯ 1 N ) can be obtained by means of (17), and Type A evaluation of standard uncertainty u ( U ¯ 1 X ) can be obtained by means of (18).
In the case of a single observation of the voltages UN and UX and according to [19], it can be assumed that there is u C ( R 1 X + ) u C ( R 1 X - ) , and it, therefore, suffices to estimate only one of these uncertainties, i.e., the uncertainty of the measured resistance R1X for one power supply polarity only. The resulting combined standard uncertainty of the averaged value R 1 X = ( R 1 X + + R 1 X - ) / 2 can be derived from the equation
u C ( R 1 X ) = ( u C ( R 1 X + ) 2 ) 2 + ( u C ( R 1 X - ) 2 ) 2 = 2 u C 2 ( R 1 X + ) 4 = u C ( R 1 X + ) 2
where u C ( R 1 X + ) and u C ( R 1 X - ) can be obtained by means of (36).

2.5. Determining Expanded Uncertainty

The combined standard uncertainty of the measurement result u C ( R 1 X ) defines an interval R 1 X u C ( R 1 X ) to R 1 X + u C ( R 1 X ) about the measurement result R1X within which the value of the measurand RX estimated by R1X can be confidently asserted to lie to the extent of 68% for the normal (Gaussian) probability distribution or to the extent of approximately 57.7% for the rectangular probability distribution. That is, it is confidently believed that
R 1 X u C ( R 1 X ) R X R 1 X + u C ( R 1 X ) which is commonly written as R X = R 1 X ± u C ( R 1 X ) .
In many areas of the industrial measuring practice, a coverage probability of p = 68.3% is found to be too low. It is the intention of this paper to provide an interval about the result of a measurement R1X that may be expected to encompass a large fraction of the distribution of values that could reasonably be attributed to the measurand RX. Hence, the expanded uncertainty is introduced in this analysis and its value is given by
U = k u C ( R 1 X )
where k is a coverage factor. In terms of the rectangular distribution, the value of the factor k usually ranges from 1.5 to 1.73 and it is based on the coverage probability, or the level of confidence that is required from the interval, Table 1. The relationship between the coverage factor k and the coverage probability p for the rectangular distribution is given by
k = p 3
For the normal (Gaussian) probability distribution, the value of the factor k is usually in the range from one to three and it is based on the coverage probability, or the level of confidence required for the interval, Table 2.
Finally, the value of the measured unknown resistance can be expressed by using the expanded uncertainty by means of the following expression
R X = R 1 X ± k u C ( R 1 X ) = R 1 X ± U

3. Practical Example

This practical example demonstrates both approaches for determining the value of the unknown electrical resistance by applying the direct comparison method using a standard resistor and voltmeter and by evaluating its combined standard uncertainty. The unknown resistor RX, the standard resistor RN and the current source are connected in a series, as shown in Figure 1, and a voltmeter (DMM) is used to measure the voltage drop across each resistor. All the connections according to Figure 1 are made by the same type of conductor and thus the amount of thermoelectric EMF that was added to the voltage measurement will be negligible.
Measuring instruments and devices with the following data were used:
  • Single-channel laboratory linear DC power supply, Model GPS-3030DD (30 V/3 A single output, 90 W), GW Instek,
  • Variable resistor PRN 533 (as the unknown resistor RX) with the rated resistance ranging from 0 to1 kΩ and the continuous permitted current 0.57 A. Resistance tolerance was +10%,
  • Resistance decade MA 2125 (as the standard resistor RN) with the standard resistance ranging from 0 to 9,999999 MΩ. The accuracy class of this resistance decade was ±1% + 0.08 Ω. The maximum current rating ranging from 0 to 999 Ω was 25 mA,
  • TRMS multi-meter, Model EX542, EXTECH (as the voltmeter) with 40,000 count LCD display and input impedance >10 MΩ VDC. The accuracy of this multi-meter for DC voltage was ±(0.06% reading + 4 digits) with resolution of 0.0001 V.
During the measurement that was performed in line with the proposed model, the slider of the variable resistor PRN 533 was set to an arbitrary position. The desired value of the resistance decade MA 2125 was predicted and set to 240 Ω. The current intensity through the resistors RX and RN during the measurement was constantly maintained at 10 mA, which is considerably less than the continuous permissible currents through these resistors, and at the same time this amount of current intensity will not cause a noticeable temperature rise of these resistors, hence their electrical resistances can be considered constant during the measurement.
Since the internal resistance of the voltmeters is very large (>10 MΩ VDC) in relation to the measured electrical resistance, and the conditions (a) and (b) of Chapter 2.1 are also fulfilled, then the measurand (output quantity) RX may be determined from the three input quantities RN, UN, and UX through the functional relationship f(∙) that is given by means of (7). Hence, the combined standard uncertainty uC(R1X) can be obtained in the case of correlated input quantities by means of (35).
Since the conditions (a), (b), and (c) of Chapter 2.1 are fulfilled in this measurement, then the output estimate R1X is calculated by means of (2) according to both proposed approaches.
In this example, we considered eleven independent sets of simultaneous observations of two input quantities UN and UX that were obtained under similar conditions, resulting in the data that is provided in Table 3. The arithmetic means of the observations and the experimental standard deviations of those means that were calculated from Equations (11), (13), (17) and (18) are also given.
According to the first approach, the means are taken as the optimum estimates of the expected input quantity values, and the experimental standard deviations represent the standard uncertainties of those means.
Table 4 shows the measured input data and the analysis results in accordance with the second approach. By comparing the results of the calculations from Table 3 and Table 4, it is noted that the same values for resistance R1X were obtained by using both approaches and that the combined standard uncertainty uC(R1X) that was obtained from the first approach was less than 1.39% compared to the amount of uC(R1X) that was obtained in the second approach. These results justify the introduction of the assumption into the proposed model that the function f(·) given by (7) or by (10) is a linear function.
Both approaches for calculating the output estimate R1X and its associated combined standard uncertainty uC(R1X) are carried out by means of the Microsoft Excel software, while Table 3 and Table 4 represent parts of the corresponding Microsoft Excel worksheet.
Figure 4 presents the results of the analysis that were carried out by means of the GUM Workbench Edu software [20] using the same input data.
Table 5 gives a comparative presentation of the results for R1X and uC(R1X) from Table 3 and Table 4, and from Table in Figure 4.
Table 5 shows good congruence results for R1X and uC(R1X) from Table in Figure 4 with corresponding results given in Table 3 and Table 4.
The uncertainty budget from Figure 4 shows that the standard uncertainty uB(R1N) contributes the most (95.2%) to the combined standard uC(R1X). Hence, it can be concluded that the combined standard uncertainty uC(R1X) is limited by the precision and accuracy of the standard resistor R1N.
It is very important to note that additional measurements were conducted with set values 140 Ω and 940 Ω of the resistance decade MA 2125 and that very similar results were obtained to abovementioned results.

4. Conclusions

In this paper, the mathematical expression (8) consists of the old expression which is modified to represent the new and the original form for the calculation of unknown electrical resistance. This new form is extremely suitable for conducting a partial derivation which can be of great importance if one assumes that the model of measurement functions has a nonlinear character. This paper sets out three conditions that must be met in order to minimize and ignore the systematic measurement deviations. The fulfilment of these three conditions allows the use of the theoretical expression (2) for the calculation of unknown electrical resistance. The complete model function of the measurement that is given by (10), or a simplified model function given by (7) are assumed to have functional linear dependence. The results that were obtained from the illustrative example justify the introduction of such assumption.
In this paper, two approaches for the estimation of unknown resistance RX and its combined standard uncertainty are analyzed. The set of input quantities RN, RV, UN, and UX is categorized in this paper as the quantities whose estimated values and uncertainties are obtained from manufacturer’s specification (RN and RV) and from a single observation or from repeated observations (UN and UX). The results that were obtained in the illustrative example indicate that it is not necessary to perform repeated voltage measurements, i.e., only one measurement suffices because the standard uncertainty uB(R1N) that is associated with the standard resistor contributes the most (95.2%) to the combined standard uC(R1X). It is very important to note that the combined standard uncertainty is limited by the precision and the accuracy of the standard resistance RN. The mathematical apparatus for the statistical analysis of this indirect measurement has been substantially elaborated.
The method that is proposed in this paper allows the elimination of the influence of thermo-electrical voltages, if any.
For many purposes, the unknown resistors are compared to standard resistors by a comparison circuit (comparators). In this method, it is possible to use the proposed approach for the estimation of the combined standard uncertainty that is associated with the measurand too. Analogously, it is also possible to determine the unknown electrical resistance and its associated combined standard uncertainty by the measurement method that is referred to as the direct comparison method using a standard resistor and potentiometer [21].
This paper has practical application and can be used for educational purposes.

Author Contributions

Conceptualization, V.P. and V.B.; methodology, V.P. and V.B.; software, V.P. and V.B.; validation, V.P., V.B. and H.T.; formal analysis, V.P. and V.B.; investigation, V.P., V.B. and H.T.; resources, V.P., V.B. and H.T.; data curation, V.P., V.B. and H.T.; writing—original draft preparation, V.P. and V.B.; writing—review and editing, V.P.; visualization, V.B.; supervision, V.B.; project administration, V.P.; funding acquisition, V.P. All authors have read and agreed to the published version of the manuscript.

Funding

This research received no external funding.

Institutional Review Board Statement

Not applicable.

Informed Consent Statement

Not applicable.

Data Availability Statement

Not applicable.

Conflicts of Interest

The authors declare no conflict of interest.

References

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Figure 1. Direct comparison method using a standard resistor and a voltmeter.
Figure 1. Direct comparison method using a standard resistor and a voltmeter.
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Figure 2. Equivalent circuit of a voltage resistive divider with two resistors.
Figure 2. Equivalent circuit of a voltage resistive divider with two resistors.
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Figure 3. Wiring diagrams that are implemented in practice for the direct comparison method using a standard resistor and voltmeter: (a) two-terminal and (b) four-terminal connection.
Figure 3. Wiring diagrams that are implemented in practice for the direct comparison method using a standard resistor and voltmeter: (a) two-terminal and (b) four-terminal connection.
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Figure 4. Value of the output quantity RX and its combined uncertainty uC that was obtained by using the GUM Workbench Edu from eleven sets of simultaneous observations.
Figure 4. Value of the output quantity RX and its combined uncertainty uC that was obtained by using the GUM Workbench Edu from eleven sets of simultaneous observations.
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Table 1. Values of the coverage factor k that produces an interval with the coverage probability p assuming a rectangular distribution.
Table 1. Values of the coverage factor k that produces an interval with the coverage probability p assuming a rectangular distribution.
Coverage Probability pCoverage Factor k
0.901.559
0.951.645
0.991.715
1.001.732
Table 2. Values of the coverage factor k that produces an interval with the coverage probability p assuming a normal distribution.
Table 2. Values of the coverage factor k that produces an interval with the coverage probability p assuming a normal distribution.
Coverage Probability pCoverage Factor k
0.68271
0.901.645
0.951.96
0.95452
0.992.576
0.99733
Table 3. Value of the output quantity RX and its combined uncertainty uC that were obtained according to the first approach from eleven sets of simultaneous observations.
Table 3. Value of the output quantity RX and its combined uncertainty uC that were obtained according to the first approach from eleven sets of simultaneous observations.
Set Number
k
Input QuantitiesOutput Quantity R1X (Ω)Combined Standard Uncertainty uC(R1X) [Ω]
U1X (V)U1N (V)R1N (Ω)
11.14184.636240
21.14184.635240
31.13134.594240
41.13154.594240
51.1334.601240
61.13314.601240
71.13324.601240
81.13254.598240
91.13254.598240
101.13554.611240
111.13564.611240
Arithmetic mean1.1347094.6072727240
Experimental standard deviation of mean0.0011340.0045369
u B ( R 1 N ) 1.431828668
R 1 X = R ¯ 1 N U ¯ 1 X / U ¯ 1 N 59.10876085
u ( U ¯ 1 N , U ¯ 1 X ) 5.14248 × 10−6
f R 1 N = U ¯ 1 X U ¯ 1 N 0.246286504
f U ¯ 1 X = R 1 N U ¯ 1 N 52.09155485
f U ¯ 1 N = R 1 N U ¯ 1 X U ¯ 1 N 2 −12.82944691
u C ( R 1 X ) [ Ω ] 0.352645412
Table 4. Value of the output quantity RX and the associated combined uncertainty uC that was obtained according to the 2nd approach from eleven sets of simultaneous observations.
Table 4. Value of the output quantity RX and the associated combined uncertainty uC that was obtained according to the 2nd approach from eleven sets of simultaneous observations.
Set Number
k
Input QuantitiesOutput Quantity
R1X (Ω)
ua(U1X)
[V]
uB(U1X)
[V]
ua(U1N)
[V]
uB(U1N)
[V]
uC(R1X)
[Ω]
U1X (V)U1N (V)R1N (Ω)
11.14184.63624059.109577220.00108510.0006264710.00678160.0039153590.357691535
21.14184.63524059.12233010.00108510.0006264710.0067810.0039150120.357690911
31.13134.59424059.101436660.00107880.0006228340.00675640.0039008090.357648132
41.13154.59424059.111885070.00107890.0006229030.00675640.0039008090.357648459
51.1334.60124059.100195610.00107980.0006234230.00676060.0039032340.357655271
61.13314.60124059.105411870.00107990.0006234570.00676060.0039032340.357655434
71.13324.60124059.110628120.00107990.0006234920.00676060.0039032340.357655598
81.13254.59824059.112657680.00107950.000623250.00675880.0039021950.357652585
91.13254.59824059.112657680.00107950.000623250.00675880.0039021950.357652585
101.13554.61124059.102147040.00108130.0006242890.00676660.0039066980.357665595
111.13564.61124059.107351980.00108140.0006243230.00676660.0039066980.357665759
Arithmetic mean1.134714.6072724059.10875264 0.357661988
Table 5. Comparative presentation of the results for R1X and uC(R1X).
Table 5. Comparative presentation of the results for R1X and uC(R1X).
Table 3Table 4Figure 4
R1X (Ω)59.1087608559.1087526459.11
uC(R1X) (Ω)0.3526454120.3576619880.361
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Pleština, V.; Boras, V.; Turić, H. The Measurement Uncertainty in Determining of Electrical Resistance Value by Applying Direct-Comparison Method. Energies 2022, 15, 2115. https://doi.org/10.3390/en15062115

AMA Style

Pleština V, Boras V, Turić H. The Measurement Uncertainty in Determining of Electrical Resistance Value by Applying Direct-Comparison Method. Energies. 2022; 15(6):2115. https://doi.org/10.3390/en15062115

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Pleština, Vladimir, Vedran Boras, and Hrvoje Turić. 2022. "The Measurement Uncertainty in Determining of Electrical Resistance Value by Applying Direct-Comparison Method" Energies 15, no. 6: 2115. https://doi.org/10.3390/en15062115

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