Zinc Ferrite Nanoparticle Coatings on Austenitic Alloy Steel
Abstract
:1. Introduction
2. Materials and Methods
2.1. Zinc Ferrite Nanoparticles
2.2. Austenitic Stainless Steel CL20ES
2.3. CL20ES and ZnFe2O4 Mixture
2.4. Fabrication of ZnFe2O4 Covering Layer
2.5. X-ray Powder Diffraction
2.6. 57Fe Mössbauer Spectroscopy
2.7. Scanning Electron Microscopy
2.8. Ultrasonic Hardness Tester
2.9. Digital Optical Microscope
3. Results
3.1. The High-Temperature Annealing of CL20ES, ZnFe2O4 Powders, and Their Mixture
3.2. ZnFe2O4 Layers on CL2OES 3D-Printed Parts
4. Conclusions
Supplementary Materials
Author Contributions
Funding
Institutional Review Board Statement
Informed Consent Statement
Data Availability Statement
Acknowledgments
Conflicts of Interest
References
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Element | Cr | Ni | Mo | Mn | Si | P | C, S |
---|---|---|---|---|---|---|---|
Min | |||||||
Max |
Sample | FWHM | RA | Component | ||
---|---|---|---|---|---|
±0.02 | ±0.02 | ±0.02 | ±3 | ||
(mm s−1) | (mm s−1) | (mm s−1) | (%) | ||
Zn-CL20-RT | 0.34 | 0.82 | 0.45 | 100 | Fe3+ |
Zn-CL20-300 | 0.34 * | 0.71 | 0.44 | 29 | Fe3+ |
−0.10 | — | 0.44 | 71 | γ-Fe | |
Zn-CL20-400 | 0.34 * | 0.61 | 0.33 | 26 | Fe3+ |
−0.11 | — | 0.41 | 74 | γ-Fe | |
Zn-CL20-500 | 0.34 * | 0.50 | 0.34 | 34 | Fe3+ |
−0.10 | — | 0.39 | 66 | γ-Fe | |
Zn-CL20-600 | 0.34 * | 0.48 | 0.35 | 41 | Fe3+ |
−0.11 | — | 0.41 | 59 | γ-Fe | |
Zn-CL20-800 | 0.34 * | 0.41 | 0.27 | 24 | Fe3+ |
−0.10 | — | 0.40 | 76 | γ-Fe | |
Zn-CL20-900 | 0.34 * | 0.39 | 0.24 | 22 | Fe3+ |
−0.09 | — | 0.40 | 78 | γ-Fe |
Sample | FWHM | RA | Component | ||
---|---|---|---|---|---|
(mm s−1) | (mm s−1) | (mm s−1) | (%) | ||
CL20ES | −0.10 | 0.15 | 0.29 | 100 | γ-Fe |
Zn-CL20-A-RT | 0.34 | 0.97 | 0.53 | 100 | Fe3+ |
Zn-CL20-A-350 | −0.10 | 0.09 | 0.30 | 18 | γ-Fe |
0.18 | 0.93 | 0.49 | 82 | Fe3+ | |
Zn-CL20-A-500 | 0.24 | 0.50 | 0.41 | 100 | Fe3+ |
Sample | Hardness | Improvement |
---|---|---|
(HRC) | (%) | |
CL20ES | 42 | — |
Zn-CL20-A-350 | 47 | 12 |
Zn-CL20-A-500 | 52 | 24 |
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Ochmann, M.; Machala, L.; Mašláň, M.; Heger, V.; Krátký, T. Zinc Ferrite Nanoparticle Coatings on Austenitic Alloy Steel. Materials 2024, 17, 857. https://doi.org/10.3390/ma17040857
Ochmann M, Machala L, Mašláň M, Heger V, Krátký T. Zinc Ferrite Nanoparticle Coatings on Austenitic Alloy Steel. Materials. 2024; 17(4):857. https://doi.org/10.3390/ma17040857
Chicago/Turabian StyleOchmann, Martin, Libor Machala, Miroslav Mašláň, Vítězslav Heger, and Tomáš Krátký. 2024. "Zinc Ferrite Nanoparticle Coatings on Austenitic Alloy Steel" Materials 17, no. 4: 857. https://doi.org/10.3390/ma17040857