Transformation of Glass Fiber Waste into Mesoporous Zeolite-Like Nanomaterials with Efficient Adsorption of Methylene Blue
Abstract
:1. Introduction
2. Materials and Methods
2.1. Reagents
2.2. Fabrication of MZN by Taguchi Experimental Design
2.3. Characterization
2.4. Adsorption of MB onto Mesoporous Zeolite-Like Nanomaterials
2.5. Thermal Reusability Study
3. Result and Discussion
3.1. Optimization Using Taguchi Approach
3.2. Surface Characterization of Mesoporous Zeolite-Like Nanomaterial
3.3. The Pore Texture of Mesoporous Zeolite-Like Nanomaterials
3.4. Adsorption of Methylene Blue by MZN
3.4.1. Effect of pH
3.4.2. Adsorption Isotherm of MB by MZN
3.4.3. Adsorption Kinetics
3.4.4. Adsorption Thermodynamics
3.5. Reusability Evaluation of MZN
4. Conclusions
Supplementary Materials
Author Contributions
Funding
Institutional Review Board Statement
Informed Consent Statement
Data Availability Statement
Acknowledgments
Conflicts of Interest
References
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Factors | qe (mg g−1) | S/N Ratio | |||
---|---|---|---|---|---|
Agent Ratio (w/w) | Agent Conc. (M) | Temp. (K) | Time (HR) | ||
1:2.5 | 1 | 393 | 8 | 36.6 | 31.28 |
1:2.5 | 2.5 | 423 | 16 | 114 | 41.18 |
1:2.5 | 5 | 453 | 24 | 88.1 | 38.90 |
1:5 | 1 | 423 | 24 | 107 | 40.58 |
1:5 | 2.5 | 453 | 8 | 84.6 | 38.54 |
1:5 | 5 | 393 | 16 | 114 | 41.15 |
1:10 | 1 | 453 | 16 | 106 | 40.53 |
1:10 | 2.5 | 393 | 24 | 111 | 40.93 |
1:10 | 5 | 423 | 8 | 103 | 40.27 |
Level | Agent Ratio (w/w) | Agent Conc. (M) | Temp. (K) | Time (HR) |
---|---|---|---|---|
L1 | 37.12 | 37.46 | 37.79 | 36.7 |
L2 | 40.09 | 40.22 | 40.68 | 40.95 |
L3 | 40.58 | 40.11 | 39.32 | 40.14 |
Delta | 3.46 | 2.75 | 2.89 | 4.25 |
Rank | 2 | 4 | 3 | 1 |
Adsorbent | pH | Surface Area (m2 g−1) | Temp. (K) | Adsorption Capacity (mg g−1) | Ref. |
---|---|---|---|---|---|
PVDF/glass as-prepared membrane | 7 | 278 | 298 | 44.4 | [Zhang et al., 2019] |
Silica xerogel | 5 | 195 | 313 | 51.9 | [Guzel Kaya et al., 2019] |
Pure silica | 6.5 | 421 | - | 102 | [Alizadeh Arasi, et al., 2020] |
Hollow silica | 7 | 67.0 | 298 | 64.0 | [Verma, et al., 2020] |
Ag/SiO2 | 7 | 208 | - | 55.0 | [Hu, et al., 2019] |
Hydroxyl group silica aerogel | 7 | 628 | - | 47.2 | [Han, et al., 2016] |
Montomorillonite/graphene oxide | 7 | 74.6 | 303 | 471 | [Yang et al., 2019] |
Mesoporous zeolite (ZSM-5) | 7 | 164 | 298 | 115 | [Brião, et al., 2018] |
Zeolite/chitosan composite | - | 83.0 | 303 | 152 | [Khanday, et al., 2017] |
Mesoporous zeolite-like material | 6 | 166 | 298 | 132 | This study |
Kinetic Model | Equation a | Parameters | MB |
---|---|---|---|
Adsorbed amount | - | qe, exp (mg g−1) | 111.0 |
Pseudo-first order | qe, cal (mg g−1) | 23.8 | |
k1 (min−1) | 0.0046 | ||
R2 | 0.858 | ||
Pseudo-second order | qe, cal (mg g−1) | 113.0 | |
k2 (g mg−1 min−1) | 0.0023 | ||
R2 | 0.998 | ||
Intra-particle diffusion | kid (mg g−1 min0.5) | 5.12 | |
C | 64.6 | ||
R2 | 0.921 |
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Tsai, C.-K.; Horng, J.-J. Transformation of Glass Fiber Waste into Mesoporous Zeolite-Like Nanomaterials with Efficient Adsorption of Methylene Blue. Sustainability 2021, 13, 6207. https://doi.org/10.3390/su13116207
Tsai C-K, Horng J-J. Transformation of Glass Fiber Waste into Mesoporous Zeolite-Like Nanomaterials with Efficient Adsorption of Methylene Blue. Sustainability. 2021; 13(11):6207. https://doi.org/10.3390/su13116207
Chicago/Turabian StyleTsai, Cheng-Kuo, and Jao-Jia Horng. 2021. "Transformation of Glass Fiber Waste into Mesoporous Zeolite-Like Nanomaterials with Efficient Adsorption of Methylene Blue" Sustainability 13, no. 11: 6207. https://doi.org/10.3390/su13116207