The Impact of Titanium Hydroxyapatite Doping on the Mechanical and Biological Properties of Photocured Resin
Abstract
:1. Introduction
2. Experimental Section
2.1. Ti-HAp Nanopowder Sample Preparation
2.2. Preparation of the Ti-HAp Photocured Composite Resin
2.3. Characterization of Ti-HAp Nanopowders
2.4. Mechanical Capacity of Ti-HAp Photocured Composite Resin
2.5. Biological Properties of Ti-HAp Photocured Composite Resin
2.6. Statistical Analysis
3. Results and Discussion
3.1. Characterization of Ti-HAp Powder
3.2. The Influence of HAp Doping on the Mechanical Characteristics of Resin
3.3. Effects of Ti-HAp Doping Content on Resin Mechanical Characteristics
3.4. The Biological Properties of Ti-HAp Resin
4. Conclusions
Author Contributions
Funding
Data Availability Statement
Acknowledgments
Conflicts of Interest
References
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Ti/Ca Molar Percentage | 1% | 2% | 3% |
---|---|---|---|
hydroxyapatite (HAp) | 5 g | 5 g | 5 g |
titanium dioxide (TiO2) | 1.24 mL | 2.50 mL | 3.78 mL |
deionized water (H2O) | 17.297 mL | 22.5 mL | 18.9 mL |
Pilot Sample | 0wt%HAp | 6wt%HAp | 9wt%HAp | 12wt%HAp |
---|---|---|---|---|
HAp (g) | 0 | 0.6 | 0.9 | 1.2 |
Bis-GMA (g) | 5.88 | 5.52 | 5.34 | 5.16 |
TEGDMA (g) | 3.92 | 3.68 | 3.56 | 3.44 |
Camphorquinone (CQ) (g) | 0.1 | 0.1 | 0.1 | 0.1 |
DMAEMA (g) | 0.1 | 0.1 | 0.1 | 0.1 |
Sample Number | Sampling Quality/g | Constant Volume/mL | Element | Results | ||
---|---|---|---|---|---|---|
Conversion Content | Unit | Mohr’s Percentage | ||||
0.3%Ti-HAp | 0.1025 | 20 | Ca | 375,616.98 (±1842) | mg/kg | 99.7 |
0.56%Ti-HAp | 0.1048 | 20 | Ca | 385,184.16 (±1764) | mg/kg | 99.44 |
1.37%Ti-HAp | 0.1028 | 20 | Ca | 382,608.37 (±1911) | mg/kg | 98.63 |
0.3%Ti-HAp | 0.1025 | 20 | Ti | 1426.15 (±6.2) | mg/kg | 0.30 |
0.56%Ti-HAp | 0.1048 | 20 | Ti | 2597.33 (±10.6) | mg/kg | 0.56 |
1.37%Ti-HAp | 0.1028 | 20 | Ti | 6418.29 (±17.4) | mg/kg | 1.37 |
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Li, X.; Yao, C.; Shen, J.; Zhu, S.; Kong, Y.; Yao, C.; Zhou, Y.; Xia, J. The Impact of Titanium Hydroxyapatite Doping on the Mechanical and Biological Properties of Photocured Resin. Micromachines 2024, 15, 1040. https://doi.org/10.3390/mi15081040
Li X, Yao C, Shen J, Zhu S, Kong Y, Yao C, Zhou Y, Xia J. The Impact of Titanium Hydroxyapatite Doping on the Mechanical and Biological Properties of Photocured Resin. Micromachines. 2024; 15(8):1040. https://doi.org/10.3390/mi15081040
Chicago/Turabian StyleLi, Xiaopan, Chao Yao, Junfu Shen, Siqi Zhu, Yiyun Kong, Chun Yao, Yuankai Zhou, and Jing Xia. 2024. "The Impact of Titanium Hydroxyapatite Doping on the Mechanical and Biological Properties of Photocured Resin" Micromachines 15, no. 8: 1040. https://doi.org/10.3390/mi15081040