Surface Modification of Bacterial Cellulose by Copper and Zinc Oxide Sputter Coating for UV-Resistance/Antistatic/Antibacterial Characteristics
Abstract
:1. Introduction
2. Experimental Methods
2.1. Materials
2.2. Synthesis of Bacterial Cellulose
2.3. Synthesis of Copper and Zinc Oxide Nanocomposite Films
2.4. Characterization
3. Results and Discussion
3.1. XPS Analysis
3.2. EDS Analysis
3.3. XRD Analysis
3.4. Antistatic Analysis
3.5. Ultraviolet Resistance Analysis
3.6. Antibacterial Analysis
4. Conclusions
Author Contributions
Funding
Acknowledgments
Conflicts of Interest
References
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Samples | Atomic Content % of Elements | |||
---|---|---|---|---|
Carbon | Oxygen | Copper | Zinc | |
Bacterial Cellulose/Copper | 17.64 | 14.08 | 68.28 | |
Bacterial Cellulose/Copper/Zinc Oxide | 16.44 | 38.87 | 1.22 | 43.47 |
Nanocomposite Materials | Static Half Period/s | Instantaneous Electrostatic Voltage/V | Reference |
---|---|---|---|
Polyester fabric/Ag | 0.51 ± 0.23 | 188 ± 9.83 | [56] |
Polyester fabric/Ag2O | 4.658 ± 0.39 | 380 ± 8.94 | |
Polyester fabric/Ag/ZnO | 70.34 ± 10.42 | 565 ± 5.48 | |
Polyester fabric/Ag2O/ZnO | 25.83 ± 3.58 | 315 ± 5.48 | |
Bacterial Cellulose/Copper | 3.386 ± 0.56 | 259.66 ± 5.50 | This work |
Bacterial Cellulose/Copper/Zinc Oxide | 51.50 ± 4.10 | 349.3 ± 6.02 |
Nanocomposite Materials | T(UVA)/% | T(UVB)/% | UPF | Reference |
---|---|---|---|---|
Polyester fabric/Ag | 3.52 ± 0.02 | 2.69 ± 0.05 | 35.26 ± 0.61 | [56] |
Polyester fabric/Ag2O | 4.36 ± 0.43 | 3.67 ± 0.18 | 26.70 ± 1.64 | |
Polyester fabric/Ag/ZnO | 3.94 ± 0.07 | 3.55 ± 0.14 | 27.68 ± 1.21 | |
Polyester fabric/Ag2O/ZnO | 3.86 ± 0.24 | 3.21 ± 0.01 | 30.37 ± 0.20 | |
Bacterial Cellulose/Copper | 0.22 ± 0.01 | 0.12 ± 0.02 | 918.27 ± 1.90 | This work |
Bacterial Cellulose/Copper/Zinc Oxide | 0.16 ± 0.02 | 0.07 ± 0.01 | 1850.33 ± 2.12 |
Samples | Bacterial Growth (%) | ||
---|---|---|---|
E. Coli (ATCC 22125) | S. aureus (ATCC 6538) | Reference | |
FPEI-A | 5.99 | 7.89 | [61] |
FPEI-AZ | 5.45 | 6.86 | |
FPEI-AZC | 4.9 | 5.83 | |
PMC-A | 2.49 | 1.85 | |
PMC-AZ | 2.22 | 1.84 | |
PMC-AZC | 1.95 | 1.83 | |
Pure Bacterial Cellulose | 100 | 100 | This work |
Bacterial Cellulose/Copper | 2.63 | 3.15 | |
Bacterial Cellulose/Copper/Zinc Oxide | 1.55 | 1.89 |
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Wasim, M.; Khan, M.R.; Mushtaq, M.; Naeem, A.; Han, M.; Wei, Q. Surface Modification of Bacterial Cellulose by Copper and Zinc Oxide Sputter Coating for UV-Resistance/Antistatic/Antibacterial Characteristics. Coatings 2020, 10, 364. https://doi.org/10.3390/coatings10040364
Wasim M, Khan MR, Mushtaq M, Naeem A, Han M, Wei Q. Surface Modification of Bacterial Cellulose by Copper and Zinc Oxide Sputter Coating for UV-Resistance/Antistatic/Antibacterial Characteristics. Coatings. 2020; 10(4):364. https://doi.org/10.3390/coatings10040364
Chicago/Turabian StyleWasim, Muhammad, Muhammad Rafique Khan, Muhammad Mushtaq, Awais Naeem, Mengchen Han, and Qufu Wei. 2020. "Surface Modification of Bacterial Cellulose by Copper and Zinc Oxide Sputter Coating for UV-Resistance/Antistatic/Antibacterial Characteristics" Coatings 10, no. 4: 364. https://doi.org/10.3390/coatings10040364