Calcium Phosphate Coatings Deposited on 3D-Printed Ti–6Al–4V Alloy by Plasma Electrolytic Oxidation
Abstract
:1. Introduction
2. Materials and Methods
3. Results and Discussion
3.1. SEM–EDS Analysis of the Coatings
3.2. The X-ray Diffraction and FTIR Analysis of the Coatings
3.3. The Tribological and Mechanical Properties of the Coatings
4. Conclusions
Author Contributions
Funding
Institutional Review Board Statement
Informed Consent Statement
Data Availability Statement
Conflicts of Interest
References
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Pulse Voltage | Current Density | Duty Cycle | Pulse Frequency | Processing Time |
---|---|---|---|---|
200 V | 0.057 A/cm2 | 10% | 50 Hz | 5 min |
250 V | 0.11 A/cm2 | 10% | 50 Hz | 5 min |
300 V | 0.2 A/cm2 | 10% | 50 Hz | 5 min |
Element (wt.%) | 200 V | 250 V | 300 V |
---|---|---|---|
O | 44.15 ± 3.31 | 41.88 ± 5.72 | 39.63 ± 9.15 |
P | 1.81 ± 0.19 | 2.15 ± 0.27 | 20.03 ± 2.00 |
Ca | 4.06 ± 0.69 | 6.44 ± 0.92 | 39.34 ± 7.30 |
Ti | 45.24 ± 3.16 | 45.36 ± 5.22 | 1.01 ± 0.13 |
Al | 2.75 ± 0.11 | 2.24 ± 0.18 | - |
V | 1.99 ± 0.24 | 1.93 ± 0.33 | - |
Ca/P | 2.24 | 2.99 | 1.96 |
Sample | Coefficient of Friction | Wear Rate (mm³/N/m) |
---|---|---|
Control sample (Ti–6Al–4V) | 0.396 | 3.087 × 10−4 |
200 V | 0.540 | 3.447 × 10−4 |
250 V | 0.546 | 2.765 × 10−4 |
300 V | 0.600 | 3.270 × 10−4 |
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Sagidugumar, A.; Dogadkin, D.; Turlybekuly, A.; Kaliyev, D. Calcium Phosphate Coatings Deposited on 3D-Printed Ti–6Al–4V Alloy by Plasma Electrolytic Oxidation. Coatings 2024, 14, 696. https://doi.org/10.3390/coatings14060696
Sagidugumar A, Dogadkin D, Turlybekuly A, Kaliyev D. Calcium Phosphate Coatings Deposited on 3D-Printed Ti–6Al–4V Alloy by Plasma Electrolytic Oxidation. Coatings. 2024; 14(6):696. https://doi.org/10.3390/coatings14060696
Chicago/Turabian StyleSagidugumar, Amangeldi, Dmitriy Dogadkin, Amanzhol Turlybekuly, and Daniyar Kaliyev. 2024. "Calcium Phosphate Coatings Deposited on 3D-Printed Ti–6Al–4V Alloy by Plasma Electrolytic Oxidation" Coatings 14, no. 6: 696. https://doi.org/10.3390/coatings14060696