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Metal Additive Manufacturing (AM) for the Synthesis of Metastable Materials

A special issue of Materials (ISSN 1996-1944). This special issue belongs to the section "Advanced Materials Characterization".

Deadline for manuscript submissions: closed (20 September 2023) | Viewed by 1827

Special Issue Editor


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Guest Editor
Leibniz-Institut für Festkörper- und Werkstoffforschung Dresden, Dresden, Germany
Interests: metal additive manufacturing; laser powder bed fusion; metastable phase formation; metallic glass

Special Issue Information

Dear Colleagues,

Additive manufacturing (AM) enables the fabrication of complex, near-net shape components with high geometric freedom because of the layer-by-layer build-up. Metal AM technologies have found their way into industry, and are still attracting growing research interest. Key challenges remain with controlling the metal AM processes characterized by extremely high cooling rates (>104 K/s) and directional heat extraction via underlying material which then experiences a repetitive heat treatment. Thus, the evolution of metastable microstructures is kinetically favored. Crystalline phases form during metal AM processing although they are not thermodynamically stable, while the formation of stable crystalline phases can be suppressed. In the most extreme case, the supercooled liquid does not crystallize and instead vitrifies, resulting in the synthesis of metallic glass. Crystal growth is strongly affected by the diverse processing conditions and complex thermal cycles, resulting in peculiar microstructural features and defects that influence the mechanical properties of the resulting component. To be more precise, additively manufactured metals can show elongated grains, cellular solidification structures eventually demarcated by a network with high dislocation density and the segregation of elements. The evolution of anisotropic microstructures can be effectively hindered by the incorporation of high-melting ceramic nucleants, as is done by processing of powder blends with a reinforcing phase.

Although there has been a vast number of studies published in this field, in recent years, new metastable materials fabricated by different metal AM technologies have continued to emerge. Potential topics of the present Special Issue include, but are not limited to, the AM of Al, Co, and Fe-based alloys, high-entropy alloys, as well as bulk metallic glasses and composites fabricated by processing respective powder blends. In addition to the characterization of the metastable microstructure, we seek a deeper understanding of the relationship between processing, microstructure, and properties.

Dr. Konrad Kosiba
Guest Editor

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Keywords

  • additive manufacturing
  • laser powder bed fusion
  • laser metal deposition
  • wire arc additive manufacturing
  • metastable phase formation
  • metal matrix composites
  • bulk metallic glass

Published Papers (1 paper)

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Research

10 pages, 3245 KiB  
Communication
Approach to Estimate the Phase Formation and the Mechanical Properties of Alloys Processed by Laser Powder Bed Fusion via Casting
by Uta Kühn, Jan Sander, Katharina Nicole Gabrysiak, Lars Giebeler, Konrad Kosiba, Stefan Pilz, Kai Neufeld, Anne Veronika Boehm and Julia Kristin Hufenbach
Materials 2022, 15(20), 7266; https://doi.org/10.3390/ma15207266 - 18 Oct 2022
Cited by 2 | Viewed by 1345
Abstract
A high-performance tool steel with the nominal composition Fe85Cr4Mo8V2C1 (wt%) was processed by three different manufacturing techniques with rising cooling rates: conventional gravity casting, centrifugal casting and an additive manufacturing process, using laser powder bed fusion (LPBF). The resulting material of all processing [...] Read more.
A high-performance tool steel with the nominal composition Fe85Cr4Mo8V2C1 (wt%) was processed by three different manufacturing techniques with rising cooling rates: conventional gravity casting, centrifugal casting and an additive manufacturing process, using laser powder bed fusion (LPBF). The resulting material of all processing routes reveals a microstructure, which is composed of martensite, austenite and carbides. However, comparing the size, the morphology and the weight fraction of the present phases, a significant difference of the gravity cast samples is evident, whereas the centrifugal cast material and the LPBF samples show certain commonalities leading finally to similar mechanical properties. This provides the opportunity to roughly estimate the mechanical properties of the material fabricated by LPBF. The major benefit arises from the required small material quantity and the low resources for the preparation of samples by centrifugal casting in comparison to the additive manufacturing process. Concluding, the present findings demonstrate the high attractiveness of centrifugal casting for the effective material screening and hence development of novel alloys adapted to LPBF-processing. Full article
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