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Keywords = cruciform sample

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17 pages, 1001 KB  
Article
Reducing Mesh Dependency in Dataset Generation for Machine Learning Prediction of Constitutive Parameters in Sheet Metal Forming
by Dário Mitreiro, Pedro A. Prates and António Andrade-Campos
Metals 2025, 15(5), 534; https://doi.org/10.3390/met15050534 - 10 May 2025
Viewed by 731
Abstract
Given the extensive use of sheet metal-forming processes in the industry and the constant emergence of new materials, the accurate prediction of material constitutive models and their parameters is extremely important to enhance and optimise these processes. Machine learning techniques have proven to [...] Read more.
Given the extensive use of sheet metal-forming processes in the industry and the constant emergence of new materials, the accurate prediction of material constitutive models and their parameters is extremely important to enhance and optimise these processes. Machine learning techniques have proven to be highly promising for predicting these parameters using data obtained either experimentally or through numerical simulations. However, ML models are often constrained by the limited dataset coverage from numerical simulations, which restricts their predictive capability to specific finite element meshes, leading to potential dependency on the discretisation scheme. To address this challenge, a new approach is proposed that integrates ML with inter-extrapolation of strain data to a grid of points within the specimen domain, expanding the dataset coverage and reducing dependency on discrete mesh points. The current work explores this approach by interpolating and extrapolating manipulated data obtained from a Finite Element Analysis, considering a biaxial tensile test on a cruciform-shaped sample. Models are trained and evaluated for performance and robustness. The results show the high accuracy of the interpolated data, along with the excellent performance metrics and robustness of the trained models, ensuring the successful implementation of this approach. Full article
(This article belongs to the Special Issue Advances in Metal Forming and Plasticity)
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10 pages, 3880 KB  
Article
Through the Forming Process of Femtosecond-Laser Nanotextured Sheets for Production of Complex 3D Parts
by Girolamo Mincuzzi, Alexandra Bourtereau, Laura Gemini, Sergi Parareda, Sylwia Rzepa, Martina Koukolíková, Pavel Konopík and Rainer Kling
Appl. Sci. 2023, 13(22), 12500; https://doi.org/10.3390/app132212500 - 20 Nov 2023
Cited by 4 | Viewed by 1488
Abstract
The use of ultra-short pulse lasers in the kW range, combined with an appropriate beam engineering approach, enables the achievement of high-throughput production of laser-functionalised surfaces. However, the manufacturing of complex parts still faces various challenges, such as difficulties in accessing regions with [...] Read more.
The use of ultra-short pulse lasers in the kW range, combined with an appropriate beam engineering approach, enables the achievement of high-throughput production of laser-functionalised surfaces. However, the manufacturing of complex parts still faces various challenges, such as difficulties in accessing regions with high aspect ratio shapes or intricate profiles, which often leads to the necessity of adapting the laser processing workstation to specific geometries. The forming process is a well-established technique for producing parts of any shape from metallic foils by imposing specific constraints. In this study, we aimed to assess the feasibility of producing laser-functionalised 3D complex products by the forming of laser-treated flat thin metallic sheets. Two-hundred micrometre-thick stainless-steel foils were textured with laser-induced periodic surface structures (LIPSS) through a roll-to-roll pilot line. First, we optimized the morphology of LIPSS. Subsequently, we conducted three types of mechanical tests on both laser-treated and untreated foils: standard tensile tests, fatigue tests, and cruciform specimen tests. We measured and compared parameters such as ultimate tensile strength, breaking strength, maximum elongation, and area reduction between specimens with and without LIPSS, all obtained from the same foil. Additionally, we utilized scanning electron microscopy (SEM) to compare the LIPSS morphology of laser-treated samples before and after mechanical tests. Full article
(This article belongs to the Special Issue Current Technologies in Laser Fabrication)
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14 pages, 6327 KB  
Article
Sensitivity Enhancement and Probiotic Detection of Microfluidic Chips Based on Terahertz Radiation Combined with Metamaterial Technology
by Yen-Shuo Lin, Shih-Ting Huang, Shen-Fu Steve Hsu, Kai-Yuan Tang, Ta-Jen Yen and Da-Jeng Yao
Micromachines 2022, 13(6), 904; https://doi.org/10.3390/mi13060904 - 7 Jun 2022
Cited by 7 | Viewed by 2437
Abstract
Terahertz (THz) radiation has attracted wide attention in recent years due to its non-destructive properties and ability to sense molecular structures. In applications combining terahertz radiation with metamaterial technology, the interaction between the terahertz radiation and the metamaterials causes resonance reactions; different analytes [...] Read more.
Terahertz (THz) radiation has attracted wide attention in recent years due to its non-destructive properties and ability to sense molecular structures. In applications combining terahertz radiation with metamaterial technology, the interaction between the terahertz radiation and the metamaterials causes resonance reactions; different analytes have different resonance performances in the frequency domain. In addition, a microfluidic system is able to provide low volume reagents for detection, reduce noise from the environment, and concentrate the sample on the detection area. Through simulation, a cruciform metamaterial pattern was designed; the proportion, periodicity, and width of the metamaterial were adjusted to improve the sensing capability of the chip. In the experiments, the sensing capabilities of Type A, B, and C chips were compared. The Type C chip had the most significant resonant effect; its maximum shift could be increased to 89 GHz. In the probiotic experiment, the cruciform chip could have a 0.72 GHz shift at a concentration of 0.025 mg/50 μL, confirming that terahertz radiation combined with a metamaterial microfluidic chip can perform low-concentration detection. Full article
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16 pages, 8150 KB  
Article
Steel Cruciform Sample with Nitrided Arms Achieves Higher Plastic Strain in the Gauge Region
by Grzegorz Mitukiewicz
Appl. Sci. 2022, 12(6), 3124; https://doi.org/10.3390/app12063124 - 18 Mar 2022
Cited by 1 | Viewed by 1903
Abstract
This paper describes a novel solution to increase plastic strain in the gauge region of a cruciform sample during a forming limit test. A nitriding procedure was used to increase the strength of the arms of the specimen and at the same time [...] Read more.
This paper describes a novel solution to increase plastic strain in the gauge region of a cruciform sample during a forming limit test. A nitriding procedure was used to increase the strength of the arms of the specimen and at the same time enabled higher plastic deformation in the centre of the sample. DC 5 steel sheets were cut in bone-shape samples and subjected to the nitriding procedure. Uniaxial tensile tests were done to obtain the properties of both the raw and thermo-chemically treated material. Two shapes of the gauge region, partially protected against diffusion of nitrogen, were modelled with the use of Abaqus software and a numerical analysis of biaxial tensile tests were conducted. Based on the obtained numerical analysis results DC 5 steel cruciform samples were nitrided while keeping the same gauge region geometries and subsequently subjected to a biaxial tensile test. The obtained results prove the positive influence of the nitriding procedure on increasing the strength of the cruciform sample arms and at the same time the plastic strain in the centre of the sample. The test bench analysis showed almost six times higher plastic deformation, as compared to the raw specimen, however special attention should be paid to the nitriding process parameters and the shape of the protected gauge region. Full article
(This article belongs to the Special Issue Advances in Plastic Deformation Analysis and Process Design)
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11 pages, 9356 KB  
Article
Variation of Surface Nanostructures on (100) PbS Single Crystals during Argon Plasma Treatment
by Sergey P. Zimin, Nikolai N. Kolesnikov, Ildar I. Amirov, Viktor V. Naumov, Egor S. Gorlachev, Sara Kim and Nam-Hoon Kim
Crystals 2022, 12(1), 111; https://doi.org/10.3390/cryst12010111 - 15 Jan 2022
Cited by 3 | Viewed by 2728
Abstract
The nanostructuring of the (100) PbS single crystal surface was studied under varying argon plasma treatment conditions. The initial PbS single crystals were grown by high-pressure vertical zone melting, cut into wafer samples, and polished. Subsequently, the PbS single crystals were treated with [...] Read more.
The nanostructuring of the (100) PbS single crystal surface was studied under varying argon plasma treatment conditions. The initial PbS single crystals were grown by high-pressure vertical zone melting, cut into wafer samples, and polished. Subsequently, the PbS single crystals were treated with inductively coupled argon plasma under varying treatment parameters such as ion energy and sputtering time. Plasma treatment with ions at a minimum energy of 25 eV resulted in the formation of nanotips with heights of 30–50 nm. When the ion energy was increased to 75–200 eV, two types of structures formed on the surface: high submicron cones and arrays of nanostructures with various shapes. In particular, the 120 s plasma treatment formed specific cruciform nanostructures with lateral orthogonal elements oriented in four <100> directions. In contrast, plasma treatment with an ion energy of 75 eV for 180 s led to the formation of submicron quasi-spherical lead structures with diameters of 250–600 nm. The nanostructuring mechanisms included a surface micromasking mechanism with lead formation and the vapor–liquid–solid mechanism, with liquid lead droplets acting as self-forming micromasks and growth catalysts depending on the plasma treatment conditions (sputtering time and rate). Full article
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13 pages, 2482 KB  
Article
Aptamer Embedded Arch-Cruciform DNA Assemblies on 2-D VS2 Scaffolds for Sensitive Detection of Breast Cancer Cells
by Jinfeng Quan, Yihan Wang, Jialei Zhang, Kejing Huang, Xuemei Wang and Hui Jiang
Biosensors 2021, 11(10), 378; https://doi.org/10.3390/bios11100378 - 8 Oct 2021
Cited by 13 | Viewed by 3240
Abstract
Arch-cruciform DNA are self-assembled on AuNPs/VS2 scaffold as a highly sensitive and selective electrochemical biosensor for michigan cancer foundation-7 (MCF-7) breast cancer cells. In the construction, arch DNA is formed using two single-strand DNA sequences embedded with the aptamer for MCF-7 cells. [...] Read more.
Arch-cruciform DNA are self-assembled on AuNPs/VS2 scaffold as a highly sensitive and selective electrochemical biosensor for michigan cancer foundation-7 (MCF-7) breast cancer cells. In the construction, arch DNA is formed using two single-strand DNA sequences embedded with the aptamer for MCF-7 cells. In the absence of MCF-7 cells, a cruciform DNA labeled with three terminal biotin is bound to the top of arch DNA, which further combines with streptavidin-labeled horseradish peroxidase (HRP) to catalyze the hydroquinone-H2O2 reaction on the electrode surface. The presence of MCF-7 cells can release the cruciform DNA and reduce the amount of immobilized HRP, thus effectively inhibiting enzyme-mediated electrocatalysis. The electrochemical response of the sensor is negatively correlated with the concentration of MCF-7 cells, with a linear range of 10~1 × 105 cells/mL, and a limit of detection as low as 5 cells/mL (S/N = 3). Through two-dimensional materials and enzyme-based dual signal amplification, this biosensor may pave new ways for the highly sensitive detection of tumor cells in real samples. Full article
(This article belongs to the Special Issue Biosensing and Bioimaging: Trends and Perspective)
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12 pages, 3731 KB  
Article
Neutron Diffraction and Diffraction Contrast Imaging for Mapping the TRIP Effect under Load Path Change
by Efthymios Polatidis, Manuel Morgano, Florencia Malamud, Michael Bacak, Tobias Panzner, Helena Van Swygenhoven and Markus Strobl
Materials 2020, 13(6), 1450; https://doi.org/10.3390/ma13061450 - 23 Mar 2020
Cited by 21 | Viewed by 3793
Abstract
The transformation induced plasticity (TRIP) effect is investigated during a load path change using a cruciform sample. The transformation properties are followed by in-situ neutron diffraction derived from the central area of the cruciform sample. Additionally, the spatial distribution of the TRIP effect [...] Read more.
The transformation induced plasticity (TRIP) effect is investigated during a load path change using a cruciform sample. The transformation properties are followed by in-situ neutron diffraction derived from the central area of the cruciform sample. Additionally, the spatial distribution of the TRIP effect triggered by stress concentrations is visualized using neutron Bragg edge imaging including, e.g., weak positions of the cruciform geometry. The results demonstrate that neutron diffraction contrast imaging offers the possibility to capture the TRIP effect in objects with complex geometries under complex stress states. Full article
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