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Keywords = pore fluid identification

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15 pages, 5513 KB  
Article
Genesis Mechanism and Logging Evaluation Methods for Low-Resistivity Contrast Gas-Bearing Layers in Shallow Gas Reservoirs
by Ruijie Huang, Liang Xiao, Wei Zhang, Ruize Shi, Xiaopeng Liu and Ning Wu
Processes 2025, 13(9), 2695; https://doi.org/10.3390/pr13092695 - 24 Aug 2025
Viewed by 403
Abstract
Shallow gas reservoirs exhibit low formation pressure and gas injection levels, leading to low-resistivity contrast between gas-bearing reservoirs and fully water-saturated layers. Gas-bearing formation identification and water saturation estimation face great challenges. To improve the accuracy of shallow gas reservoir identification and logging [...] Read more.
Shallow gas reservoirs exhibit low formation pressure and gas injection levels, leading to low-resistivity contrast between gas-bearing reservoirs and fully water-saturated layers. Gas-bearing formation identification and water saturation estimation face great challenges. To improve the accuracy of shallow gas reservoir identification and logging evaluation, it is essential to analyze the genesis mechanisms underlying the low-resistivity contrast. This study used the HJ Formation, a typical shallow gas reservoir located in the BY Sag of the eastern South China Sea Basin as an example. Combining the results of nuclear magnetic resonance (NMR), full rock mineral analysis and X-ray diffraction of clay minerals in the laboratory, it was determined that the genesis mechanism for the low-resistivity contrast in the gas-bearing reservoir was due to the high irreducible water saturation (Swi) and the cation-induced supplementary conductivity. Afterwards, we integrated three methods, density–neutron correlation, calculation of the apparent formation water resistivity, and cross-plots of conventional and gas-logging curves, to identify shallow gas reservoirs. In addition, we also established a Waxman–Smits-based model to estimate water saturation. Compared with the typical Archie’s equation, the predicted water saturation curve using the Waxman–Smits-based model was more reasonable. The established methods and models can be used in target shallow gas reservoir evaluations, and it also has reference value for other types of oilfields with similar physical characteristics. Full article
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24 pages, 11697 KB  
Article
Layered Production Allocation Method for Dual-Gas Co-Production Wells
by Guangai Wu, Zhun Li, Yanfeng Cao, Jifei Yu, Guoqing Han and Zhisheng Xing
Energies 2025, 18(15), 4039; https://doi.org/10.3390/en18154039 - 29 Jul 2025
Viewed by 298
Abstract
The synergistic development of low-permeability reservoirs such as deep coalbed methane (CBM) and tight gas has emerged as a key technology to reduce development costs, enhance single-well productivity, and improve gas recovery. However, due to fundamental differences between coal seams and tight sandstones [...] Read more.
The synergistic development of low-permeability reservoirs such as deep coalbed methane (CBM) and tight gas has emerged as a key technology to reduce development costs, enhance single-well productivity, and improve gas recovery. However, due to fundamental differences between coal seams and tight sandstones in their pore structure, permeability, water saturation, and pressure sensitivity, significant variations exist in their flow capacities and fluid production behaviors. To address the challenges of production allocation and main reservoir identification in the co-development of CBM and tight gas within deep gas-bearing basins, this study employs the transient multiphase flow simulation software OLGA to construct a representative dual-gas co-production well model. The regulatory mechanisms of the gas–liquid distribution, deliquification efficiency, and interlayer interference under two typical vertical stacking relationships—“coal over sand” and “sand over coal”—are systematically analyzed with respect to different tubing setting depths. A high-precision dynamic production allocation method is proposed, which couples the wellbore structure with real-time monitoring parameters. The results demonstrate that positioning the tubing near the bottom of both reservoirs significantly enhances the deliquification efficiency and bottomhole pressure differential, reduces the liquid holdup in the wellbore, and improves the synergistic productivity of the dual-reservoirs, achieving optimal drainage and production performance. Building upon this, a physically constrained model integrating real-time monitoring data—such as the gas and liquid production from tubing and casing, wellhead pressures, and other parameters—is established. Specifically, the model is built upon fundamental physical constraints, including mass conservation and the pressure equilibrium, to logically model the flow paths and phase distribution behaviors of the gas–liquid two-phase flow. This enables the accurate derivation of the respective contributions of each reservoir interval and dynamic production allocation without the need for downhole logging. Validation results show that the proposed method reliably reconstructs reservoir contribution rates under various operational conditions and wellbore configurations. Through a comparison of calculated and simulated results, the maximum relative error occurs during abrupt changes in the production capacity, approximately 6.37%, while for most time periods, the error remains within 1%, with an average error of 0.49% throughout the process. These results substantially improve the timeliness and accuracy of the reservoir identification. This study offers a novel approach for the co-optimization of complex multi-reservoir gas fields, enriching the theoretical framework of dual-gas co-production and providing technically adaptive solutions and engineering guidance for multilayer unconventional gas exploitation. Full article
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22 pages, 5215 KB  
Article
Analysis and Modeling of Elastic and Electrical Response Characteristics of Tight Sandstone in the Kuqa Foreland Basin of the Tarim Basin
by Juanli Cui, Kui Xiang, Xiaolong Tong, Yanling Shi, Zuzhi Hu and Liangjun Yan
Minerals 2025, 15(7), 764; https://doi.org/10.3390/min15070764 - 21 Jul 2025
Viewed by 259
Abstract
This study addresses the limitations of conventional evaluation methods caused by low porosity, strong heterogeneity, and complex pore structures in tight sandstone reservoirs. Through integrated rock physics experiments and multi-physical field modeling, the research systematically investigates the coupled response mechanisms between electrical and [...] Read more.
This study addresses the limitations of conventional evaluation methods caused by low porosity, strong heterogeneity, and complex pore structures in tight sandstone reservoirs. Through integrated rock physics experiments and multi-physical field modeling, the research systematically investigates the coupled response mechanisms between electrical and elastic parameters. The experimental approach includes pore structure characterization, quantitative mineral composition analysis, resistivity and polarizability measurements under various saturation conditions, P- and S-wave velocity testing, and scanning electron microscopy (SEM) imaging. The key findings show that increasing porosity leads to significant reductions in resistivity and elastic wave velocities, while also increasing surface conductivity. Specifically, clay minerals enhance surface conductivity through interfacial polarization effects and decrease rock stiffness, which exacerbates wave velocity attenuation. Furthermore, resistivity exhibits a nonlinear negative correlation with water saturation, with sharp increases at low saturation levels due to the disruption of conductive pathways. By integrating the Modified Generalized Effective Medium Theory of Induced Polarization (MGEMTIP) and Kuster–Toksöz models, this study establishes quantitative relationships between porosity, saturation, and electrical/elastic parameters, and constructs cross-plot templates that correlate elastic wave velocities with resistivity and surface conductivity. These analyses reveal that high-porosity, high-saturation zones are characterized by lower resistivity and wave velocities, coupled with significantly higher surface conductivity. The proposed methodology significantly improves the accuracy of reservoir evaluation and enhances fluid identification capabilities, providing a solid theoretical foundation for the efficient exploration and development of tight sandstone reservoirs. Full article
(This article belongs to the Special Issue Electromagnetic Inversion for Deep Ore Explorations)
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14 pages, 6249 KB  
Article
Application of the NOA-Optimized Random Forest Algorithm to Fluid Identification—Low-Porosity and Low-Permeability Reservoirs
by Qunying Tang, Yangdi Lu, Xiaojing Yang, Yuping Li, Wei Zhang, Qiangqiang Yang, Zhen Tian and Rui Deng
Processes 2025, 13(7), 2132; https://doi.org/10.3390/pr13072132 - 4 Jul 2025
Viewed by 357
Abstract
As an important unconventional oil and gas resource, tight oil exploration and development is of great significance to ensure energy supply under the background of continuous growth of global energy demand. Low-porosity and low-permeability reservoirs are characterized by tight rock properties, poor physical [...] Read more.
As an important unconventional oil and gas resource, tight oil exploration and development is of great significance to ensure energy supply under the background of continuous growth of global energy demand. Low-porosity and low-permeability reservoirs are characterized by tight rock properties, poor physical properties, and complex pore structure, and as a result the fine calculation of logging reservoir parameters faces great challenges. In addition, the crude oil in this area has high viscosity, the formation water salinity is low, and the oil reservoir resistivity shows significant spatial variability in the horizontal direction, which further increases the difficulty of oil and water reservoir identification and affects the accuracy of oil saturation calculation. Targeting the above problems, the Nutcracker Optimization Algorithm (NOA) was used to optimize the hyperparameters of the random forest classification model, and then the optimal hyperparameters were input into the random forest model, and the conventional logging curve and oil test data were combined to identify and classify the reservoir fluids, with the final accuracy reaching 94.92%. Compared with the traditional Hingle map intersection method, the accuracy of this method is improved by 14.92%, which verifies the reliability of the model for fluid identification of low-porosity and low-permeability reservoirs in the research block and provides reference significance for the next oil test and production test layer in this block. Full article
(This article belongs to the Special Issue Oil and Gas Drilling Processes: Control and Optimization, 2nd Edition)
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39 pages, 4219 KB  
Review
Bottom-Simulating Reflectors (BSRs) in Gas Hydrate Systems: A Comprehensive Review
by Shiyuan Shi, Linsen Zhan, Wenjiu Cai, Ran Yang and Hailong Lu
J. Mar. Sci. Eng. 2025, 13(6), 1137; https://doi.org/10.3390/jmse13061137 - 6 Jun 2025
Viewed by 864
Abstract
The bottom-simulating reflector (BSR) serves as an important seismic indicator for identifying gas hydrate-bearing sediments. This review synthesizes global BSR observations and demonstrates that spatial relationships among BSRs, free gas, and gas hydrates frequently deviate from one-to-one correspondence. Moreover, our analysis reveals that [...] Read more.
The bottom-simulating reflector (BSR) serves as an important seismic indicator for identifying gas hydrate-bearing sediments. This review synthesizes global BSR observations and demonstrates that spatial relationships among BSRs, free gas, and gas hydrates frequently deviate from one-to-one correspondence. Moreover, our analysis reveals that more than 35% of global BSRs occur shallower than the bases of gas hydrate stability zones, especially in deepwater regions, suggesting that the BSRs more accurately represent the interface between the gas hydrate occurrence zone and the underlying free gas zone. BSR morphology is influenced by geological settings, sediment properties, and seismic acquisition parameters. We find that ~70–80% of BSRs occur in fine-grained, grain-displacive sediments with hydrate lenses/nodules, while coarse-grained pore-filling sediments host <20%. BSR interpretation remains challenging due to limitations in traditional P-wave seismic profiles and conventional amplitude versus offset (AVO) analysis, which hinder accurate fluid identification. To address these gaps, future research should focus on frequency-dependent AVO inversion based on viscoelastic theory, multicomponent full-waveform inversion, improved anisotropy assessment, and quantitative links between rock microstructure and elastic properties. These innovations will shift BSR research from static feature mapping to dynamic process analysis, enhancing hydrate detection and our understanding of hydrate–environment interactions. Full article
(This article belongs to the Special Issue Advances in Marine Gas Hydrates)
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15 pages, 11766 KB  
Article
Occurrence State and Time-Shift Characteristics of Residual Oil in Low-Permeability Reservoirs After Long-Term Waterflooding in Changqing Oilfield
by Yangnan Shangguan, Boying Li, Chunning Gao, Junhong Jia, Yongqiang Zhang, Jinghua Wang and Tao Xu
Energies 2025, 18(8), 2001; https://doi.org/10.3390/en18082001 - 14 Apr 2025
Viewed by 439
Abstract
This study focuses on a low-permeability sandstone reservoir in the Changqing Oilfield, aiming to elucidate the formation mechanism and occurrence state of residual oil during late-stage waterflooding development, thereby providing theoretical guidance for refined residual oil recovery. By integrating scanning electron microscopy (SEM), [...] Read more.
This study focuses on a low-permeability sandstone reservoir in the Changqing Oilfield, aiming to elucidate the formation mechanism and occurrence state of residual oil during late-stage waterflooding development, thereby providing theoretical guidance for refined residual oil recovery. By integrating scanning electron microscopy (SEM), nuclear magnetic resonance (NMR), and digital core analysis, the oil–water occurrence state and dynamic characteristics during waterflooding were systematically investigated. NMR was employed to determine fluid distribution within core pores, while CT scanning was utilized to construct a 3D digital core model, enabling the identification of microscopic residual oil displacement and occurrence states at different flooding stages. The oil displacement efficiency was further analyzed based on variations in oil–water distribution and occurrence states within the core. The results demonstrate that pore and throat size and connectivity are the primary factors governing reservoir permeability. After high-pore-volume (PV) waterflooding, microscopic residual oil predominantly exists as dispersed droplets, films, and small-scale clusters or columns. Although prolonged high-PV waterflooding effectively expands the sweep volume, localized displacement efficiency declines, and reservoir heterogeneity adversely affects sweep volume maintenance. The post-flooding residual oil characteristics are collectively determined by the core’s local connectivity, wettability, and pore–throat morphology. This research systematically analyzes the occurrence patterns and evolutionary trends of residual oil in low-permeability reservoirs during long-term waterflooding, providing critical theoretical insights and technical support for enhanced oil recovery and residual oil exploitation. Full article
(This article belongs to the Special Issue Digitization and Low Carbon Transformation of Petroleum Engineering)
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18 pages, 3641 KB  
Article
Distribution, Origin, and Impact on Diagenesis of Organic Acids in Representative Continental Shale Oil
by Wenjun Pang, Jing Li, Shixin Zhou, Yaoyu Li, Liangliang Liu, Hao Wang and Gengrong Chen
Processes 2024, 12(10), 2092; https://doi.org/10.3390/pr12102092 - 26 Sep 2024
Cited by 1 | Viewed by 1137
Abstract
This investigation focuses on the prevalent continental oil shale within the Triassic Chang 7, a member of the Yanchang Formation in the Ordos Basin and the Permian Lucaogou Formation in the Junggar Basin of western China, and delves into the impacts of hydrocarbon [...] Read more.
This investigation focuses on the prevalent continental oil shale within the Triassic Chang 7, a member of the Yanchang Formation in the Ordos Basin and the Permian Lucaogou Formation in the Junggar Basin of western China, and delves into the impacts of hydrocarbon generation and the derived organic acids on the physical attributes of oil shale reservoirs. Water-soluble organic acids (WSOAs) were extracted via Soxhlet extraction and analyzed by a 940 ion chromatograph (Metrohm AG), supplemented with core observations, thin-section analyses, pyrolysis, and trace element assays, as well as the qualitative observation of pore structures via FIB-SEM scanning electron microscopy. The study discloses substantial disparities in the types and abundances of organic acids within the oil shale strata of the two regions, with mono-acids being conspicuously more prevalent than dicarboxylic acids. The spatial distribution of organic acids within the oil shale strata in the two regions is non-uniform, and their generation is inextricably correlated with the type of organic matter, thermal maturity, and depth at which they are buried. During diverse stages of diagenesis, the hydrocarbons and organic acids produced from the pyrolysis of organic matter not only exert an impact on the properties of pore fluids but also interact with diagenetic processes such as compaction, dissolution, and metasomatism to enhance the reservoir quality of oil shale. The synergy between chemical interactions and physical alterations collectively governs the migration and distribution patterns of organic acids as well as the characteristics of oil shale reservoirs. Furthermore, the sources of organic acids within the oil shale series in the two regions demonstrate pronounced dissimilarities, which are intimately associated with the peculiarities of their sedimentary milieu. The oil shale of the Yanchang Formation was formed in a warm and humid freshwater lacustrine basin environment, while the oil shale of the Lucaogou Formation was deposited in a brackish to saline lacustrine setting under an arid to semi-arid climatic regime. These variances not only illuminate the intricacy and multiplicity of the sedimentary attributes of oil shale but also accentuate the impact of the sedimentary environment on the genesis and distribution of organic acids, especially the transformation and optimization of reservoir dissolution by organic acids generated during hydrocarbon generation—a factor of paramount significance for the precise identification and effective development of the “sweet spot” area of shale oil. These areas, characterized by an abundance of organic matter, their maturity, and superior reservoir properties, are the foci of the efficient exploration and development of continental shale oil. Full article
(This article belongs to the Section Chemical Processes and Systems)
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19 pages, 3945 KB  
Article
A Novel Finite Element-Based Method for Predicting the Permeability of Heterogeneous and Anisotropic Porous Microstructures
by Paris Mulye, Elena Syerko, Christophe Binetruy and Adrien Leygue
Materials 2024, 17(12), 2873; https://doi.org/10.3390/ma17122873 - 12 Jun 2024
Cited by 3 | Viewed by 1559
Abstract
Permeability is a fundamental property of porous media. It quantifies the ease with which a fluid can flow under the effect of a pressure gradient in a network of connected pores. Porous materials can be natural, such as soil and rocks, or synthetic, [...] Read more.
Permeability is a fundamental property of porous media. It quantifies the ease with which a fluid can flow under the effect of a pressure gradient in a network of connected pores. Porous materials can be natural, such as soil and rocks, or synthetic, such as a densified network of fibres or open-cell foams. The measurement of permeability is difficult and time-consuming in heterogeneous and anisotropic porous media; thus, a numerical approach based on the calculation of the tensor components on a 3D image of the material can be very advantageous. For this type of microstructure, it is important to perform calculations on large samples using boundary conditions that do not suppress the transverse flows that occur when flow is forced out of the principal directions. Since these are not necessarily known in complex media, the permeability determination method must not introduce bias by generating non-physical flows. A new finite element-based method proposed in this study allows us to solve very high-dimensional flow problems while limiting the biases associated with boundary conditions and the small size of the numerical samples addressed. This method includes a new boundary condition, full permeability tensor identification based on the multiscale homogenization approach, and an optimized solver to handle flow problems with a large number of degrees of freedom. The method is first validated against academic test cases and against the results of a recent permeability benchmark exercise. The results underline the suitability of the proposed approach for heterogeneous and anisotropic microstructures. Full article
(This article belongs to the Special Issue Finite Element Modeling of Microstructures in Composite Materials)
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34 pages, 17043 KB  
Review
Microscopic Characterization and Fractal Analysis of Pore Systems for Unconventional Reservoirs
by Wen Guan, Wenjiu Cai, Zhenchao Li and Hailong Lu
J. Mar. Sci. Eng. 2024, 12(6), 908; https://doi.org/10.3390/jmse12060908 - 29 May 2024
Cited by 5 | Viewed by 2055
Abstract
The complex pore structure of unconventional oil and gas reservoirs is one of the reasons for the difficulties in resource evaluation and development. Therefore, it is crucial to comprehensively characterize the pore structure, understand reservoir heterogeneity from multiple perspectives, and gain an in-depth [...] Read more.
The complex pore structure of unconventional oil and gas reservoirs is one of the reasons for the difficulties in resource evaluation and development. Therefore, it is crucial to comprehensively characterize the pore structure, understand reservoir heterogeneity from multiple perspectives, and gain an in-depth understanding of fluid migration and accumulation mechanisms. This review outlines the methods and basic principles for characterizing microporous systems in unconventional reservoirs, summarizes the fractal analysis corresponding to the different methods, sorts out the relationship between the fractals and reservoir macroscopic physical properties (porosity, permeability, etc.) with the reservoir microscopic pore structures (pore structure parameters, pore connectivity, etc.). The research focuses on cutting-edge applications of characterization techniques, such as improved characterization accuracy, calibration of PSD ranges, and identification of different hydrogen compositions in pore systems for dynamic assessment of unconventional reservoirs. Fractal dimension analysis can effectively identify the quality level of the reservoir; complex pore-throat structures reduce permeability and destroy free fluid storage space, and the saturation of removable fluids is negatively correlated with Df. As for the mineral composition, the fractal dimension is positively correlated with quartz, negatively correlated with feldspar, and weakly correlated with clay mineral content. In future qualitative characterization studies, the application and combination of contrast agents, molecular dynamics simulations, artificial intelligence techniques, and 4D imaging techniques can effectively improve the spatial resolution of the images and explore the adsorption/desorption of gases within the pores, and also help to reduce the computational cost of these processes; these could also attempt to link reservoir characterization to research on supercritical carbon dioxide-enhanced integrated shale gas recovery, carbon geological sequestration, and advanced underground hydrogen storage. Full article
(This article belongs to the Section Geological Oceanography)
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18 pages, 5129 KB  
Article
Study on Sensitivity Mechanism of Low-Permeability Sandstone Reservoir in Huilu Area of Pearl River Mouth Basin
by Hongbo Li, Lin Ding, Qibiao Zang, Qiongling Wu, Yongkun Ma, Yuchen Wang, Sandong Zhou, Qiaoyun Cheng, Xin Tian, Jiancheng Niu and Mengdi Sun
J. Mar. Sci. Eng. 2024, 12(6), 888; https://doi.org/10.3390/jmse12060888 - 27 May 2024
Cited by 1 | Viewed by 1193
Abstract
Reservoir sensitivity is a parameter that is used to evaluate the degree of change in reservoir permeability under the influence of external fluids. Accurate evaluation of reservoir sensitivity is conducive to the optimization of fluid parameters during exploration and development. Taking the Wenchang [...] Read more.
Reservoir sensitivity is a parameter that is used to evaluate the degree of change in reservoir permeability under the influence of external fluids. Accurate evaluation of reservoir sensitivity is conducive to the optimization of fluid parameters during exploration and development. Taking the Wenchang Formation and Enping Formation of the Paleogene in the Huilu area of the Pearl River Mouth Basin as the research object, reservoir sensitivity experiments were carried out. Combined with the corresponding experimental results obtained using methods such as thin section identification, scanning electron microscopy (SEM), X-ray diffraction (XRD), mercury intrusion porosimetry (MIP), and screening analysis, based on mineral sensitization and pore structure sensitization, qualitative and quantitative evaluations of reservoir sensitivity were carried out, and factors affecting sensitivity and sensitization mechanisms were analyzed. This work shows the following: (1) The sandstone reservoirs in the two areas have the same clay type, but the total clay content of the Wenchang Formation is greater than that of the Enping Formation. The porosity of the Wenchang Formation is less developed than the Enping Formation. (2) The Wenchang Formation has weak or moderately weak water sensitivity and moderately weak or moderately strong flow velocity sensitivity. The water sensitivity of the Enping Group samples is moderately weak or moderately strong, the flow rate sensitivity is moderately weak, the alkali sensitivity is weak, the acid sensitivity is moderately weak, and the salinity sensitivity is moderately weak or moderately strong. (3) The sensitivity of the Wenchang Formation is mainly affected by the content of clay minerals. The sensitivity of the Enping Formation is also affected by the clay content and type. Although the clay content is not high, the permeability is more susceptible to sensitivity due to the pore structure and debris particle distribution characteristics. These conclusions are beneficial for the selection of fluid parameters and efficient reservoir development. Full article
(This article belongs to the Special Issue Exploration and Development of Marine Energy)
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16 pages, 14962 KB  
Article
Genesis and Related Reservoir Development Model of Ordovician Dolomite in Shuntogol Area, Tarim Basin
by Liangxuanzi Zhong, Leli Cheng, Heng Fu, Shaoze Zhao, Xiaobin Ye, Yidong Ding and Yin Senlin
Minerals 2024, 14(6), 545; https://doi.org/10.3390/min14060545 - 25 May 2024
Viewed by 1487
Abstract
The Ordovician thick dolostone in Shuntogol area of the Tarim Basin has the potential to form a large-scale reservoir, but its genesis and reservoir development model are still unclear. Starting from a sedimentary sequence, this study takes a batch of dolostone samples obtained [...] Read more.
The Ordovician thick dolostone in Shuntogol area of the Tarim Basin has the potential to form a large-scale reservoir, but its genesis and reservoir development model are still unclear. Starting from a sedimentary sequence, this study takes a batch of dolostone samples obtained from new drilling cores in recent years as the research object. On the basis of core observation and thin section identification, trace elements, cathodoluminescence, carbon and oxygen isotopes, rare earth elements, and X-ray diffraction order degree tests were carried out to discuss the origin of the dolomite and summarize the development model of the dolostone reservoir. The analysis results show that the Ordovician dolomite in the study area had a good crystalline shape, large thickness, high Fe and Mn values, and mostly showed bright red light or bright orange–red light under cathode rays. The ratio of δ18O values to seawater values at the same time showed a negative bias; the δCe values were negative anomalies, the δEu values were positive anomalies, and the order degree was high. This indicates that the dolomitization process occurred in a relatively closed diagenetic environment. The Ordovician carbonate rocks in the study area were low-lying during the sedimentary period, and with the rise of sea level, the open platform facies continued to develop. When the Middle and Lower Ordovician series entered the burial stage, the main hydrocarbon source rocks of the lower Cambrian Series entered the oil generation peak, and the resulting formation overpressure provided the dynamic source for the upward migration of the lower magnesium-rich fluid, and the dolomitization fluid entered the karst pore system in the target layer to produce all the dolomitization. This set of dolostone reservoirs is large in scale and can be used as a favorable substitute area for deep carbonate exploration for continuous study. Full article
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17 pages, 7199 KB  
Article
Design, Characterization, and Incorporation of the Alkaline Aluminosilicate Binder in Temperature-Insulating Composites
by Pavlo Kryvenko, Igor Rudenko, Oleksandr Konstantynovskyi and Oleksandr Gelevera
Materials 2024, 17(3), 664; https://doi.org/10.3390/ma17030664 - 29 Jan 2024
Cited by 2 | Viewed by 1208
Abstract
This paper covers the design of binder formulations and technology for low-energy building materials based on alkaline aluminosilicate binders developed for special uses. The microstructure of the binders was investigated using scanning electron and atomic force microscopy examination techniques. The identification of phase [...] Read more.
This paper covers the design of binder formulations and technology for low-energy building materials based on alkaline aluminosilicate binders developed for special uses. The microstructure of the binders was investigated using scanning electron and atomic force microscopy examination techniques. The identification of phase compositions was performed by means of X-ray diffraction. The degree of binding of the alkali metal ions within the binder was determined with the help of chemical analysis of the pore fluid. Structure formation depending upon binder mix design and curing conditions was also studied. Some examples of the manufacture and application of binder-based glues and adhesives, including those developed for heat insulation and fire prevention, are discussed. The advantages of binder-based temperature-insulating composite materials compared with traditionally used materials are highlighted. Full article
(This article belongs to the Special Issue Advances in Rock and Mineral Materials)
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13 pages, 3449 KB  
Article
Diagnostics of Secondary Fracture Properties Using Pressure Decline Data during the Post-Fracturing Soaking Process for Shale Gas Wells
by Jianfa Wu, Liming Ren, Cheng Chang, Shuyao Sheng, Jian Zhu, Sha Liu, Weiyang Xie and Fei Wang
Processes 2024, 12(2), 239; https://doi.org/10.3390/pr12020239 - 23 Jan 2024
Viewed by 8789
Abstract
In addition to main fractures, a large number of secondary fractures are formed after the volumetric fracturing of shale gas wells. The secondary fracture properties are so complex, that it is difficult to identify and diagnose by direct monitoring methods. In this study, [...] Read more.
In addition to main fractures, a large number of secondary fractures are formed after the volumetric fracturing of shale gas wells. The secondary fracture properties are so complex, that it is difficult to identify and diagnose by direct monitoring methods. In this study, a new approach to model and diagnose secondary fracture properties is presented. First, a new pressure decline model, which is composed of four interconnected domains, i.e., wellbore, main fractures, secondary fractures, and reservoir matrix pores, is built. Then, the fracturing fluid pumping and post-fracturing soaking processes are simulated. The simulated pressure derivatives reflect five fracture-dominated flow regimes, which correspond to multiple alternating positive and negative slopes of the pressure decline derivative. The results of sensitivity simulation show that the density, permeability, and width of secondary fractures are the main controlling factors affecting the size ratio. Finally, based on the simulated pressure decline characteristics, a diagnostic method for the identification and analysis of secondary fracture properties is formed. This method is then applied to three platform wells in the Changning shale gas field in China. This study builds the correlation between the secondary fracture properties and the shut-in pressure decline characteristics, and also provides a theoretical method for comprehensive post-fracturing evaluation of shale gas horizontal wells. Full article
(This article belongs to the Special Issue Oil and Gas Drilling Rock Mechanics and Engineering)
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15 pages, 7038 KB  
Article
Fluid Identification Method of Nuclear Magnetic Resonance and Array Acoustic Logging for Complex Oil and Water Layers in Tight Sandstone Reservoir
by Ze Bai, Maojin Tan, Bo Li, Yujiang Shi, Haitao Zhang and Gaoren Li
Processes 2023, 11(11), 3051; https://doi.org/10.3390/pr11113051 - 24 Oct 2023
Cited by 5 | Viewed by 1850
Abstract
In order to improve the logging interpretation accuracy for complex oil and water layers developed in tight sandstone reservoirs, this study takes the Chang 8 member of the Yanchang Formation in the Huanxian area as the research object, and two new fluid identification [...] Read more.
In order to improve the logging interpretation accuracy for complex oil and water layers developed in tight sandstone reservoirs, this study takes the Chang 8 member of the Yanchang Formation in the Huanxian area as the research object, and two new fluid identification methods were constructed based on nuclear magnetic resonance (NMR) logging and array acoustic logging. Firstly, the reservoir characteristics of physical properties and conductivity were studied in the research area, and the limitations of conventional logging methods in identifying complex oil and water layers were clarified. Then, the sensitive parameters for identifying different pore fluids were established by analyzing the relationship between NMR logging and array acoustic logging with different pore fluids. On this basis, the fluid identification plate, composed of movable fluid apparent diffusion coefficient and effective porosity difference (Daφe) by NMR logging data of D9TWE3 observation mode, and the other fluid identification plate, composed of apparent bulk modulus of pore fluid and elastic parameter sensitive factor (Kf-Fac), were constructed, respectively. Finally, these two fluid identification methods were used for reservoir interpretation of actual logging data. This study shows that the two new fluid identification methods constructed by NMR logging and array acoustic logging can effectively eliminate the interference of rock skeleton on logging interpretation, which make them more effective in identifying complex oil and water layers than the conventional logging method. Additionally, the two methods have their own advantages and disadvantages when used separately for interpreting complex oil and water layers, and the comprehensive interpretation of the two methods provides a technical development direction for further improving the accuracy of logging the interpretation of complex oil and water layers. Full article
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19 pages, 8824 KB  
Article
Quantitative Characterization of Shale Pores and Microfractures Based on NMR T2 Analysis: A Case Study of the Lower Silurian Longmaxi Formation in Southeast Sichuan Basin, China
by Chuxiong Li, Baojian Shen, Longfei Lu, Anyang Pan, Zhiming Li, Qingmin Zhu and Zhongliang Sun
Processes 2023, 11(10), 2823; https://doi.org/10.3390/pr11102823 - 25 Sep 2023
Cited by 5 | Viewed by 1661
Abstract
In order to quantitatively characterize shale pores and microfractures, twelve marine shale samples from the Longmaxi Formation in the southeastern Sichuan Basin were selected and their NMR T2 spectra were analyzed under the conditions of full brine saturation, cyclic centrifugal treatment and [...] Read more.
In order to quantitatively characterize shale pores and microfractures, twelve marine shale samples from the Longmaxi Formation in the southeastern Sichuan Basin were selected and their NMR T2 spectra were analyzed under the conditions of full brine saturation, cyclic centrifugal treatment and cyclic heat treatment. Then, movable, capillary bound and unrecoverable fluid of shale samples were distinguished and the NMR porosity and full-scale PSD were calculated. Based on NMR spectral peak identification, the relative content of pores and microfractures was determined and their influence factors were analyzed. The results show that the PSD of shale samples is bimodal, with pores distributed in the range of 1 nm to 200 nm and microfractures distributed in the range of 200 nm to 5000 nm, with relative contents in the ranges of 3.44–6.79% and 0.22–1.43%, respectively. Nanoscale organic pores are the dominant type of pores, while inorganic pores and microfractures contribute much less to the shale reservoir space than organic pores. The T2 cutoff values range from 0.55 ms to 6.73 ms, and the surface relaxivities range from 0.0032 µm/ms to 0.0391 µm/ms. Their strong correlation with TOC suggests that organic matter is the main factor controlling the pore type and structure. In addition, the main difference between NMR porosity and He porosity is that gas logging porosity is used to detect connected pores, while NMR porosity also includes closed pores and microfractures. Combined with NMR and high-temperature pressure displacement experimental facilities, this will be a further step towards studying the pore structure of shale under simulated formation conditions. Full article
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