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Keywords = three-point bending fatigue test

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17 pages, 4189 KB  
Article
Effect of Fiber Characteristics on Cracking Resistance Properties of Stone Mastic Asphalt (SMA) Mixture
by Kai Yang, Wenyuan Huang, Mutian Sun, Zhixian Zheng and Hongwei Lin
Polymers 2025, 17(19), 2623; https://doi.org/10.3390/polym17192623 - 28 Sep 2025
Viewed by 256
Abstract
Cracking is a critical distress that reduces an asphalt pavement’s service life, and fiber reinforcement is an effective strategy to enhance anti-cracking capacity. However, the effects of fiber type, morphology, and length on key cracking modes remain insufficiently understood, limiting rational fiber selection [...] Read more.
Cracking is a critical distress that reduces an asphalt pavement’s service life, and fiber reinforcement is an effective strategy to enhance anti-cracking capacity. However, the effects of fiber type, morphology, and length on key cracking modes remain insufficiently understood, limiting rational fiber selection in practice. This study systematically evaluated the influence of four representative fiber types on the anti-cracking performance of Stone Mastic Asphalt (SMA) mixture, combining mechanical testing and microstructural analysis. The fibers included lignin fiber (LF); polyester fiber (PF); chopped basalt fiber (CBF) with lengths of 3 mm, 6 mm, 9 mm; and flocculent basalt fiber (FBF). Key mechanical tests assessed specific cracking behaviors: three-point bending (low-temperature cracking), indirect tensile (tensile cracking), pre-cracked semi-circular bending (crack propagation), overlay (reflective cracking), and four-point bending (fatigue resistance) tests. A scanning electron microscopy (SEM) test characterized fiber morphology and fiber–asphalt interface interactions, revealing microstructural mechanisms underlying performance improvements. The results showed that all fibers improved anti-cracking performance, but their efficacy varied with fiber type, appearance, and length. PF exhibited the best low-temperature cracking resistance, with a 26.8% increase in bending strength and a 16.6% increase in maximum bending strain. For tensile and crack propagation resistance, 6 mm CBF and FBF outperformed the other fibers, with fracture energy increases of up to 53.2% (6 mm CBF) and CTindex improvements of 72.8% (FBF). FBF optimized reflective cracking resistance, increasing the loading cycles by 48.0%, while 6 mm CBF achieved the most significant fatigue life improvement (36.9%) by balancing rigidity and deformation. Additionally, SEM analysis confirmed that effective fiber dispersion and strong fiber–asphalt bonding were critical for enhancing stress transfer and inhibiting crack initiation/propagation. These findings provide quantitative insights into the relationship between fiber characteristics (type, morphology, length) and anti-cracking performance, offering practical guidance for rational fiber selection to improve pavement durability. Full article
(This article belongs to the Special Issue Polymer Materials for Pavement Applications)
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16 pages, 7726 KB  
Article
Digital Shearography for NDE of Crack Classification in Composite Materials
by Zhongfang Gao, Siyuan Fang, Riad Dandan and Lianxiang Yang
Appl. Sci. 2025, 15(19), 10317; https://doi.org/10.3390/app151910317 - 23 Sep 2025
Viewed by 278
Abstract
This paper presents a relevant and timely study on the application of thermal loaded digital shearography for crack classification in glass fiber reinforced plastic (GFRP) structures, particularly air-cooled condenser (ACC) fan blades. A thermal loaded digital shearography system was applied to measure strain [...] Read more.
This paper presents a relevant and timely study on the application of thermal loaded digital shearography for crack classification in glass fiber reinforced plastic (GFRP) structures, particularly air-cooled condenser (ACC) fan blades. A thermal loaded digital shearography system was applied to measure strain concentration caused by the cracks at different fatigue cycles. A thermomechanical model was introduced to estimate the heating temperature and the time to ensure heat can reach to the desired depth and that both shallow and deep cracks can be detected. In order to correlate the information of strain concentration in the shearograms to the different stages of cracks, fatigue testing with dynamic three-point bending was conducted. The fatigue tests demonstrated how the strain concentration evolved in the shearograms, while the crack developed from the early (no noticeable strain concentration), to the middle (strain concentration is forming), to the late stage (significant strain concentration is found). The relationships between the degrees of strain concentration in the shearograms and the different stages of cracks can be obtained from testing of the artificial cracks. Using the rules and experimental results obtained from artificial samples, digital shearography was applied to classify the crack stages in parts of ACC fan blades from industry. The combination of artificial crack testing, fatigue loading experiments, and validation with CT scans demonstrates a comprehensive approach and provides potential guidance for industry to determine criticality and maintenance criteria. Full article
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11 pages, 2881 KB  
Article
Experimental Investigation of Very High Cycle Fatigue and Fatigue Crack Growth Behaviors of X17CrNi15-2 Stainless Steel
by Ran Li, Fengcai Liu, Mengyu Wu, Wenshu Wei, Yuehua Lai, Hao Liu, Jian Ye, Tianze Cao, Jianfeng Li and Wenbo Li
Processes 2025, 13(9), 3004; https://doi.org/10.3390/pr13093004 - 20 Sep 2025
Viewed by 309
Abstract
Understanding the fatigue behavior of materials is essential for designing components capable of enduring prolonged use under varying stress conditions. This study investigates the high-cycle fatigue and fatigue crack growth characteristics of X17CrNi15-2 stainless steel. Very high-cycle fatigue (VHCF) and fatigue crack growth [...] Read more.
Understanding the fatigue behavior of materials is essential for designing components capable of enduring prolonged use under varying stress conditions. This study investigates the high-cycle fatigue and fatigue crack growth characteristics of X17CrNi15-2 stainless steel. Very high-cycle fatigue (VHCF) and fatigue crack growth tests were conducted on conventional fatigue and compact tension (CT) specimens fabricated from X17CrNi15-2 stainless steel. The fatigue crack growth behavior of the CT specimens was analyzed using Paris’ law. A revised version of Paris’ law was suggested based on the fatigue crack growth rate plotted against the stress intensity factor range, expanding on prior research utilizing three-point single-edge notch bend specimens. Scanning electron microscopy (SEM) was employed to examine the fracture mechanisms of both fatigue specimen types. The results indicated that the fatigue specimens failed in the VHCF regime under stress amplitudes ranging from 100 to 450 MPa. A power law correlation between stress amplitude and fatigue life was established, with material constants of 7670.3954 and −0.1663. These findings offer valuable insights into the material’s performance and are crucial for enhancing its suitability in engineering applications where high-cycle fatigue is a critical factor. Full article
(This article belongs to the Section Manufacturing Processes and Systems)
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17 pages, 4181 KB  
Article
Fatigue Life Assessment of Railway Rails with Lubrication Holes: Experimental Validation and Finite Element Modelling
by Jose Sainz-Aja, Pablo San Roman, Jose A. Casado, Isidro Carrascal, Borja Arroyo, Diego Ferreño, Raul Moreno, David Peribañez, Hugo Vegas and Soraya Diego
Metals 2025, 15(9), 992; https://doi.org/10.3390/met15090992 - 8 Sep 2025
Viewed by 388
Abstract
This study investigates the fatigue behavior of railway rails with lubrication holes through a finite element modeling approach validated against full-scale laboratory tests. Fatigue tests were conducted on rail coupons subjected to three-point bending with the rail positioned upside-down, replicating the most critical [...] Read more.
This study investigates the fatigue behavior of railway rails with lubrication holes through a finite element modeling approach validated against full-scale laboratory tests. Fatigue tests were conducted on rail coupons subjected to three-point bending with the rail positioned upside-down, replicating the most critical loading configuration. Two finite element models were developed using ANSYS 2024 R2: a reduced model reproducing the laboratory setup, and a more comprehensive model representing a real rail track segment with multiple spans. The first model was calibrated against experimental S–N curve data to ensure consistency with the mechanical behavior observed in tests. The second model was used to evaluate the effect of wheel position, hole diameter, and hole location on the fatigue life of the rail. Simulation results highlight the influence of geometric and load parameters on crack initiation near the hole, providing valuable insights for optimizing hole design and placement in operational conditions. Full article
(This article belongs to the Special Issue Recent Insights into Mechanical Properties of Metallic Alloys)
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17 pages, 5651 KB  
Article
Experimental Investigation on Fatigue Crack Propagation in Surface-Hardened Layer of High-Speed Train Axles
by Chun Gao, Zhengwei Yu, Yuanyuan Zhang, Tao Fan, Bo Zhang, Huajian Song and Hang Su
Crystals 2025, 15(7), 638; https://doi.org/10.3390/cryst15070638 - 11 Jul 2025
Viewed by 588
Abstract
This study examines fatigue crack growth behavior in induction-hardened S38C axle steel with a gradient microstructure. High-frequency three-point bending fatigue tests were conducted to evaluate crack growth rates (da/dN) across three depth-defined regions: a hardened layer, a heterogeneous transition [...] Read more.
This study examines fatigue crack growth behavior in induction-hardened S38C axle steel with a gradient microstructure. High-frequency three-point bending fatigue tests were conducted to evaluate crack growth rates (da/dN) across three depth-defined regions: a hardened layer, a heterogeneous transition zone, and a normalized core. Depth-resolved da/dN–ΔK relationships were established, and Paris Law parameters were extracted. The surface-hardened layer exhibited the lowest crack growth rates and flattest Paris slope, while the transition zone showed notable scatter due to microstructural heterogeneity and residual stress effects. These findings provide experimental insight into the fatigue performance of gradient-structured axle steels and offer guidance for fatigue life prediction and inspection planning. Full article
(This article belongs to the Special Issue Fatigue and Fracture of Crystalline Metal Structures)
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24 pages, 7600 KB  
Article
Microstructure, Porosity, and Bending Fatigue Behaviour of PBF-LB/M SS316L for Biomedical Applications
by Conall Kirk, Weijie Xie, Shubhangi Das, Ben Ferguson, Chenliang Wu, Hau-Chung Man and Chi-Wai Chan
Metals 2025, 15(6), 650; https://doi.org/10.3390/met15060650 - 11 Jun 2025
Viewed by 1302
Abstract
Bending fatigue significantly affects the mechanical stability and lifespan of biomedical implants, such as bone plates and orthopaedic fixation devices, which undergo cyclic loading in the human body. This study examines the microstructure, porosity, and bending fatigue properties of PBF-LB/M SS316L. Samples were [...] Read more.
Bending fatigue significantly affects the mechanical stability and lifespan of biomedical implants, such as bone plates and orthopaedic fixation devices, which undergo cyclic loading in the human body. This study examines the microstructure, porosity, and bending fatigue properties of PBF-LB/M SS316L. Samples were analysed across three faces (top, front, and side) using optical microscopy (OM) and scanning electron microscopy (SEM) to observe microstructural features and porosity. Elemental composition was measured by energy-dispersive X-ray spectroscopy (EDX). Phase structures and grain orientations were characterised via X-ray diffraction (XRD) and electron backscatter diffraction (EBSD). Four-point bending fatigue tests, conducted under two loading conditions, below and slightly above the yield point, demonstrated that defects inherent to the PBF-LB/M process, particularly micropores and unmelted powder particles, strongly influence fatigue crack initiation. Real-time monitoring of crack initiation and propagation on the external sample surface was performed using a high-speed digital microscope. These findings indicate the influence of microstructural defects on fatigue performance in PBF-LB/M SS316L, supporting the design and development of more reliable patient-specific biomedical implants. Full article
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14 pages, 1907 KB  
Article
Performance Evaluation of Stone Mastic Asphalt Involving Coarse Steel Slag and Fine RAP
by Yan Wu, Weidong Cao, Chao Xu, Fanshuo Meng, Guangyong Wang and Shutang Liu
Materials 2025, 18(11), 2598; https://doi.org/10.3390/ma18112598 - 2 Jun 2025
Viewed by 736
Abstract
Stone mastic asphalt (SMA) is the most widely adopted asphalt mixture on highway pavement in China. However, the cost of SMA is rising continually due to the increasing shortage of high-quality basalt aggregate. On the other hand, China’s steel slag and reclaimed asphalt [...] Read more.
Stone mastic asphalt (SMA) is the most widely adopted asphalt mixture on highway pavement in China. However, the cost of SMA is rising continually due to the increasing shortage of high-quality basalt aggregate. On the other hand, China’s steel slag and reclaimed asphalt pavement (RAP) stock is abundant, and steel slag has excellent strength and wear-resistant performance, which can fully or partially replace part of the basalt aggregate. The content of asphalt may be increased due to the porosity of the steel slag. If fine RAP rich in asphalt is also used for SMA, it can partially fill the voids of steel slag and reduce the amount of new asphalt and fine aggregate. For this objective, SMA 13 was designed with two particle sizes of coarse steel slag aggregate (5–10 mm, 10–15 mm) and one fine RAP (0–5 mm), named SR-SMA. The fundamental pavement performance of SR-SMA was evaluated through a wheel-tracking test, low-temperature beam bending test, freeze–thaw indirect tensile test, and four-point bending fatigue test. For comparison, the mix design and performance tests of two SMAs involving coarse steel slag and fine basalt aggregate (named SB-SMA), and coarse and fine basalt aggregates (named B-SMA), respectively, were conducted. The results indicated that SR-SMA (dynamic stability of 4865 passes/mm) shows the best rutting resistance, followed by SB-SMA (dynamic stability of 4312 passes/mm), and B-SMA (dynamic stability of 4135 passes/mm) comes in last. Additionally, the dynamic stability values of three SMAs have significant differences. SR-SMA has better low-temperature cracking resistance with a failure strain of 3150 με, between SB-SMA and B-SMA (failure strain values are 4436, 2608 με). Compared to B-SMA and SB-SMA, the moisture stability of SR-SMA is relatively poor but meets Chinese specification. While the fatigue resistance of SR-SMA is the worst among three SMAs, their differences are insignificant. Furthermore, SR-SMA reduces material cost by approximately 35% per ton compared to conventional B-SMA. Overall, SR-SMA is cost-effective and can be used as an alternative material to traditional B-SMA. Full article
(This article belongs to the Section Construction and Building Materials)
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25 pages, 7210 KB  
Article
Determination of Interface Fracture Parameters in Thermoplastic Fiber Metal Laminates Under Mixed-Mode I+II
by Michał Smolnicki and Szymon Duda
Polymers 2025, 17(11), 1462; https://doi.org/10.3390/polym17111462 - 24 May 2025
Cited by 1 | Viewed by 806
Abstract
Thermoplastic fiber metal laminates (FMLs) are hybrid material systems that consist of a thin aluminum alloy sheet bonded to plies of fiber-reinforced adhesive. They provide excellent properties like fatigue strength, damage-tolerant properties, and inherent resistance to corrosion. However, they are still challenging materials [...] Read more.
Thermoplastic fiber metal laminates (FMLs) are hybrid material systems that consist of a thin aluminum alloy sheet bonded to plies of fiber-reinforced adhesive. They provide excellent properties like fatigue strength, damage-tolerant properties, and inherent resistance to corrosion. However, they are still challenging materials in terms of the metal–composite interface, which is the weakest link in this material system. In this paper, an experimental–numerical method for the determination of the fracture stress and energy for metal–composite interlayer is presented and verified. The proposed method utilizes four different experimental tests: DCB test (interface opening—mode I), ENF test (interface shearing—mode II), MMB test (mixed-mode I+II—opening with the shearing of the interface) and three-point bending test (3PB). For each test, digital twin in the form of a numerical model is prepared. The established numerical models for DCB and ENF allowed us to determine fracture stress and energy for mode I and mode II, respectively. On the basis of the numerical and experimental (from the MMB test) data, the B-K exponent is determined. Finally, the developed material model is verified in a three-point bending test, which results in mixed-mode conditions. The research is conducted on the thermoplastic FML made of aluminum alloy sheet and glass fiber reinforced polyamide 6. The research presented is complemented by fundamental mechanical tests, image processing and Scanning Electron Microscopy (SEM) analysis. As an effect, for the tested material, fracture parameters are determined using the described method. Full article
(This article belongs to the Special Issue Advances in Fatigue and Fracture of Fiber-Reinforced Polymers)
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26 pages, 3160 KB  
Article
Research on Pavement Performance of Steel Slag Asphalt Mastic and Mixtures
by Jianmin Guo, Jincheng Wei, Feiping Xu, Qinsheng Xu, Liang Kang, Wenjuan Wu, Wencheng Shi and Xiangpeng Yan
Coatings 2025, 15(5), 525; https://doi.org/10.3390/coatings15050525 - 28 Apr 2025
Cited by 1 | Viewed by 859
Abstract
In order to explore the influence of steel slag on the road performance of asphalt mastic and its mixtures, steel slag powder (SSP) and steel slag aggregate (SSA) were used to replace limestone mineral powder filler (MF) and natural limestone aggregate (LA) respectively [...] Read more.
In order to explore the influence of steel slag on the road performance of asphalt mastic and its mixtures, steel slag powder (SSP) and steel slag aggregate (SSA) were used to replace limestone mineral powder filler (MF) and natural limestone aggregate (LA) respectively to prepare asphalt mastic and mixture. A series of standardized tests including penetration, softening point, ductility, viscosity, pull-off strength, dynamic shear rheometer (DSR), and bending beam rheometer (BBR) were carried out to evaluate the performance of asphalt mastics with SSP. Meanwhile, high- and low-temperature performance, moisture stability, volumetric stability, and fatigue resistance were evaluated by wheel tracking, uniaxial penetration strength, Hamburg, three-point bending, freeze–thaw splitting, immersed Marshall stability, water immersion expansion, and two-point bending trapezoidal beam fatigue tests. The results show that compared to the asphalt mastic with MF, enhanced high-temperature deformation resistance and reduced low-temperature cracking resistance of asphalt mastic with SSP were observed, as well as superior aging resistance. The improvements in high-temperature stability, moisture resistance, and fatigue performance were confirmed for asphalt mixtures with SSP/SSA. Additionally, compromised volumetric stability and low-temperature crack resistance were found when SSP/SSA was used in mixtures. Although asphalt mixtures with SSA exhibited 257.79%–424.60% higher expansion rate after 21-day immersion than those with LA, the 3-day immersion expansion rates complied with specification limits (<1.5% per JTG F40-2004). Critical volume expansion control measures should be adopted for full-component applications of steel slag powder/aggregates due to the hydration potential of free lime (f-CaO) and magnesium oxide (MgO) in steel slag under moisture exposure. Full article
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18 pages, 3439 KB  
Article
Assessment of Fatigue Life in Grouted Polyurethane Composites for Pavement Maintenance
by Fang Wang, Shiyi Zhang, Muyang Huang, Kai Liu and Chaoliang Fu
Materials 2025, 18(8), 1806; https://doi.org/10.3390/ma18081806 - 15 Apr 2025
Viewed by 568
Abstract
Polyurethane grouting technology is widely employed to maintain critical transportation infrastructure, including pavements, airports, and railways. After injection, foamed polyurethane bonds with surrounding aggregates to form a polyurethane–aggregate composite material (PACM). The gradation of aggregates in PACM, stress levels, and loading frequencies significantly [...] Read more.
Polyurethane grouting technology is widely employed to maintain critical transportation infrastructure, including pavements, airports, and railways. After injection, foamed polyurethane bonds with surrounding aggregates to form a polyurethane–aggregate composite material (PACM). The gradation of aggregates in PACM, stress levels, and loading frequencies significantly influence fatigue performance under cyclic traffic loading. This study investigates the fatigue behavior of three distinct PACM gradation types through three-point bending fatigue tests under varying stress levels and loading frequencies. Results reveal that the finer gradations of PACM tend to exhibit higher flexural stiffness and longer fatigue life but also greater sensitivity to stress levels. Conversely, coarser gradations show lower stiffness but improved energy dissipation characteristics. Additionally, the flexural stiffness modulus, fatigue life, and cumulative dissipated energy decrease with increasing stress levels, while they grow with higher loading frequencies. In contrast, the dissipated angle follows an opposite trend. Additionally, mathematical models were developed to describe the evolution of dissipated energy, uncovering a three-stage pattern dominated by a prolonged plateau phase accounting for over 80% of the fatigue process. Based on this characteristic plateau, fatigue life prediction models were established for each gradation type, achieving high prediction accuracy with relative errors below 10%. These findings not only highlight the significant impact of aggregate gradation on PACM fatigue performance but also provide practical tools for optimizing material design in pavement maintenance. Full article
(This article belongs to the Special Issue Asphalt Mixtures and Pavements Design (2nd Edition))
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21 pages, 16071 KB  
Article
Chemical Mechanisms of Cement Stabilization and Durability Enhancement in High-Content Modified Phosphogypsum
by Bin Xu, Yingxin Zhou, Zijing Wu, Kaiji Lu, Hongbing Wang and Aodong Gao
Buildings 2025, 15(5), 723; https://doi.org/10.3390/buildings15050723 - 24 Feb 2025
Cited by 2 | Viewed by 932
Abstract
Phosphogypsum, a byproduct of phosphate fertilizer production, accumulates in large quantities annually, posing significant environmental challenges due to harmful components such as fluorine, heavy metals, and acidic salts. To mitigate these issues, phosphogypsum is often combined with cement and single modifiers such as [...] Read more.
Phosphogypsum, a byproduct of phosphate fertilizer production, accumulates in large quantities annually, posing significant environmental challenges due to harmful components such as fluorine, heavy metals, and acidic salts. To mitigate these issues, phosphogypsum is often combined with cement and single modifiers such as sodium silicate, hydrated lime, and defluorinating agents for use in pavement applications. However, concerns about the durability of unmodified or singly modified high-content phosphogypsum have hindered its widespread adoption. To address this issue, this study explored the use of sodium silicate, hydrated lime, and defluorinating agents as composite modifiers to enhance the durability of cement-stabilized phosphogypsum. The mechanisms of modification by individual and composite additives were investigated using X-ray diffraction (XRD) and scanning electron microscopy (SEM). Durability was evaluated through three-point bending fatigue, freeze–thaw, and drying shrinkage tests on both unmodified and modified cement-stabilized phosphogypsum. The results demonstrated that the composite modification of sodium silicate, hydrated lime, and defluorinating agents significantly improved the material’s density, strength, and stability by enhancing hydration products and stabilizing fluoride ions. The modified material exhibited superior fatigue and freeze–thaw resistance, with reduced mass loss and slower strength decline compared to unmodified phosphogypsum. Additionally, the modified material showed improved drying shrinkage performance due to enhanced hydration. However, caution is recommended when using these materials in regions with high moisture content and significant temperature fluctuations. Full article
(This article belongs to the Section Building Materials, and Repair & Renovation)
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24 pages, 13851 KB  
Article
Analysis of the Influence of Manufacturing Technology on Selected Static, Fatigue and Morphological Properties of CFRP Composites
by Andrzej Kubit, Kishore Debnath, Ján Slota, Filip Dominik, Ankit Dhar Dubey, Gorrepotu Surya Rao and Krzysztof Żaba
Materials 2025, 18(1), 102; https://doi.org/10.3390/ma18010102 - 30 Dec 2024
Viewed by 1345
Abstract
The aim of this study was to compare the mechanical properties of carbon-fiber-reinforced polymer (CFRP) composites produced using three popular technologies. The tests were performed on composites produced from prepregs in an autoclave, the next variant is composites produced using the infusion method, [...] Read more.
The aim of this study was to compare the mechanical properties of carbon-fiber-reinforced polymer (CFRP) composites produced using three popular technologies. The tests were performed on composites produced from prepregs in an autoclave, the next variant is composites produced using the infusion method, and the third variant concerns composites produced using the vacuum-assisted hand lay-up method. For each variant, flat plates with dimensions of 1000 mm × 1000 mm were produced while maintaining similar material properties and fabric arrangement configuration. Samples for testing were cut using a plotter in the 0° and 45° directions. Non-destructive tests (NDTs) were carried out using the active thermography method, demonstrating the correctness of the composites, i.e., the absence of structural defects for all variants. Static peel strength tests were carried out for samples with different directional orientations. The tests were carried out at temperatures of +25 °C and +80 °C. At room temperature, similar strengths were demonstrated, which for the 0° orientation were 619 MPa, 599 MPa and 536 MPa for the autoclave, vacuum and infusion variants, respectively. However, at a temperature of +80 °C, only the composite produced in the autoclave maintained the stability of its properties, showing a strength of 668 MPa. Meanwhile, in the case of the composite produced by the infusion method, a decrease in strength at an elevated temperature of 46.5% was demonstrated, while for the composite produced by the hand lay-up method, there was a decrease of 46.2%. For the last two variants, differential scanning calorimetry (DSC) analysis of epoxy resins constituting the composite matrices was carried out, showing a glass transition temperature value of 49.91 °C for the infusion variant and 56.07 °C for the vacuum variant. In the three-point static bending test, the highest strength was also demonstrated for the 0ᵒ orientation, and the bending strength was 1088 MPa for the autoclave variant, 634 MPa for the infusion variant and 547 MPa for the vacuum variant. The fatigue strength tests in tension at 80% of the static strength for the infusion variant showed an average fatigue life of 678.788 × 103 cycles for the autoclave variant, 176.620 × 103 cycles for the vacuum variant and 159.539 × 103 cycles for the infusion variant. Full article
(This article belongs to the Special Issue Advances in Carbon Fiber/Resin Matrix Polymer Composites)
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16 pages, 3551 KB  
Article
Modifying Bitumen with Recycled PET Plastics to Enhance Its Water Resistance and Strength Characteristics
by Assel Jexembayeva, Marat Konkanov, Lyazat Aruova, Akpan Kirgizbayev and Lailya Zhaksylykova
Polymers 2024, 16(23), 3300; https://doi.org/10.3390/polym16233300 - 26 Nov 2024
Cited by 3 | Viewed by 1920
Abstract
This study investigates the modification of bituminous mixtures by varying percentages of PET particles (1%, 3%, 5%, 8%, 10%, and 12% PET). The following methods were employed to analyze the samples: the ring-and-ball softening point determination method (ASTM D36/D36M-14), the Fraass breaking point [...] Read more.
This study investigates the modification of bituminous mixtures by varying percentages of PET particles (1%, 3%, 5%, 8%, 10%, and 12% PET). The following methods were employed to analyze the samples: the ring-and-ball softening point determination method (ASTM D36/D36M-14), the Fraass breaking point determination method (EN 12593: 2015), the elongation determination method (EN 13589: 2014), and the needle penetration depth determination method (EN 1426: 2015). Optimal bitumen/PET ratios were identified to obtain modified bituminous mixtures (MBMs) with enhanced operational characteristics (5% and 8% PET). The physical and mechanical properties of the investigated bitumen samples and PET were determined. A comparative analysis of the modified bituminous mixture samples based on their physical and mechanical properties was conducted. Microstructures of the surface of modified bituminous mixture samples with varying modifier contents were obtained. An X-ray structural analysis was performed on the samples of modified bituminous mixtures with varying PET contents. The dependencies of the moisture absorption rate on time were determined for the samples of modified bituminous mixtures with different modifier contents. The values of the stress intensity factor were determined based on the number of loading cycles in fatigue tests using three-point bending for the samples of modified bituminous mixtures with varying modifier contents. Full article
(This article belongs to the Section Circular and Green Sustainable Polymer Science)
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17 pages, 4406 KB  
Article
Enhanced Experimental Setup and Methodology for the Investigation of Corrosion Fatigue in Metallic Biodegradable Implant Materials
by Lukas Schumacher, Ikra-Nur Cetin, Sira Bielefeldt, Frank Rupp and Ariadne Roehler
Materials 2024, 17(21), 5146; https://doi.org/10.3390/ma17215146 - 22 Oct 2024
Viewed by 985
Abstract
Biodegradable implants as bone fixations may present a safe alternative to traditional permanent implants, reducing the risk of infections, promoting bone healing, and eliminating the need for removal surgeries. Structural integrity is an important consideration when choosing an implant material. As a biodegradable [...] Read more.
Biodegradable implants as bone fixations may present a safe alternative to traditional permanent implants, reducing the risk of infections, promoting bone healing, and eliminating the need for removal surgeries. Structural integrity is an important consideration when choosing an implant material. As a biodegradable implant is being resorbed, until the natural bone has regrown, the implant material needs to provide mechanical stability. However, the corrosive environment of the human body may affect the fatigue life of the material. Conversely, mechanical stress can have an effect on electrochemical corrosion processes. This is known as corrosion fatigue. In the presented work, an experimental setup and methodology was established to analyze the corrosion fatigue of experimental bioresorbable materials while simultaneously monitoring the electrochemical processes. A double-walled measurement cell was constructed for a three-point bending test in Dulbecco‘s Phosphate-Buffered Saline (DPBS− −), which was used as simulated body fluid (SBF), at 37 ± 1 °C. The setup was combined with a three-electrode setup for corrosion measurements. Rod-shaped zinc samples were used to validate the setup’s functionality. Preliminary static and dynamic bending tests were carried out as per the outlined methodology to determine the test parameters. Open-circuit as well as potentiostatic polarization measurements were performed with and without mechanical loading. For the control, fatigue tests were performed in an air environment. The tested zinc samples were inspected via scanning electron microscopy (SEM). Based on the measured mechanical and electrochemical values as well as the SEM images, the effects of the different environments were investigated, and the setup’s functionality was verified. An analysis of the data showed that a comprehensive investigation of corrosion fatigue characteristics is feasible with the outlined approach. Therefore, this novel methodology shows great potential for furthering our understanding of the effects of corrosion on the fatigue of biodegradable implant materials. Full article
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19 pages, 8451 KB  
Article
Flammability and Mechanical Testing of Sandwich Composite for Rolling Stock Structural Applications
by Marcin Kalinowski, Mirosław Szczepanik and Małgorzata Szymiczek
Materials 2024, 17(20), 5125; https://doi.org/10.3390/ma17205125 - 21 Oct 2024
Cited by 2 | Viewed by 1163
Abstract
Components made of composite materials are being increasingly used in the construction of rolling stock. Currently, the use of components made of composite materials as train structural elements is increasingly being considered. Non-structural components made of composites are most often found inside rail [...] Read more.
Components made of composite materials are being increasingly used in the construction of rolling stock. Currently, the use of components made of composite materials as train structural elements is increasingly being considered. Non-structural components made of composites are most often found inside rail vehicles (e.g., the interior lining), while structural components made of sandwich composite materials can be used for the roof, sidewalls, and underframe constructions. This article provides a description of an innovative sandwich composite developed for a metro’s underframe, as well as the production process and preparation of the composite specimens. The main parts of the work are flammability and mechanical (static and fatigue) tests of the innovative sandwich composite. The scope of the flammability tests included the testing of the fire properties using the radial plate method, the optical density of smoke, and the content of toxic gases. The mechanical strength of the sandwich composite was examined during a flexural (three-point bending) test and a fatigue strength under a given dynamic load. The results presented in the article are very significant, both in terms of flammability and the mechanical strength tests. In order to produce large-size train components, appropriately large patches of component layers of the composite are required; this may pose production problems. Full article
(This article belongs to the Special Issue Mechanical Behavior and Numerical Simulation of Sandwich Composites)
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