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11 pages, 4038 KB  
Article
Effect of Laser Energy Density During LPBF on the Structure and Mechanical Properties of Al–15Sn–5Pb Alloy
by Nikolay M. Rusin, Alexander L. Skorentsev, Kirill O. Akimov, Vadim E. Likharev, Dmitry P. Il’yashchenko and Andrey I. Dmitriev
Materials 2025, 18(23), 5268; https://doi.org/10.3390/ma18235268 - 21 Nov 2025
Abstract
Al–15Sn–5Pb (vol.%) alloy was fabricated by the Laser Powder Bed Fusion (LPBF) method at laser scanning speeds of 0.8, 1.0, and 1.2 m/s and laser powers ranging from 70 to 130 W. The samples were synthesized from a mixture of elemental powders using [...] Read more.
Al–15Sn–5Pb (vol.%) alloy was fabricated by the Laser Powder Bed Fusion (LPBF) method at laser scanning speeds of 0.8, 1.0, and 1.2 m/s and laser powers ranging from 70 to 130 W. The samples were synthesized from a mixture of elemental powders using an ONSINT AM150 3D printer under a flowing argon atmosphere. The structure and mechanical properties under compression tests of the produced material were investigated as a function of the volumetric laser energy density (E) during LPBF. It has been established that low laser energy density during LPBF results in incomplete melting of aluminum particles and a non-uniform distribution of soft inclusions within the material. Increasing the energy density ensures a significantly more uniform distribution of the phases, resulting in the formation of a fine-grained three-phase alloy. It was established that both the ductility and strength of the alloy improve with the increase in E until a critical value is reached. As a result, at E ≥ 48 J·mm−3, the ultimate strength of the alloy reaches 100 ± 5 MPa, and its deformation before fracture is 15 ± 1%. Substituting one quarter of the tin volume with lead results in a significant increase in the ductility of the LPBF-fabricated aluminum alloy. Full article
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17 pages, 3862 KB  
Article
Study of Heat Transfer Characteristics of PCMs Melting Inside Aluminum Foams
by Farjad Shahid Hasan Khan and Andrea Diani
Materials 2025, 18(22), 5130; https://doi.org/10.3390/ma18225130 - 11 Nov 2025
Viewed by 334
Abstract
This study examines the thermal performance of phase change material (PCM)–metal foam composites under base heating, a configuration more relevant to compact thermal energy storage (TES) and electronics-cooling applications, compared to the widely studied side-heated case. Metal foams with pore densities of 10, [...] Read more.
This study examines the thermal performance of phase change material (PCM)–metal foam composites under base heating, a configuration more relevant to compact thermal energy storage (TES) and electronics-cooling applications, compared to the widely studied side-heated case. Metal foams with pore densities of 10, 20, and 40 PPI, but identical porosity (volumetric value), were impregnated with two PCMs (paraffin RT55 and RT64HC) and tested under varying heat fluxes. The thermophysical properties of three PCMs (RT42, RT55, and RT64HC) were first characterized using the T-history method. A control case consisting of pure PCM revealed significant thermal lag between the heater and the PCM, whereas the inclusion of a metal foam improved temperature uniformity and accelerated melting. The results showed that PPI variation had little influence on melting completion time, while PCM type, viz., melting temperature, strongly affected duration. Heat flux was the dominant parameter: higher input power substantially reduced melting times, although diminishing returns were observed at elevated heat fluxes. An empirical correlation from the literature, originally developed for side-heated foams, was applied to the base-heated configuration and reproduced the main melting trends, though it consistently underpredicted completion times at high fluxes. Overall, embedding PCMs in metal foams enhances heat transfer, mitigates localized overheating, and enables more compact and efficient TES systems. Future work should focus on developing correlations for non-adiabatic cases, exploring advanced foam architecture, and scaling the approach for practical energy storage and cooling applications. Full article
(This article belongs to the Special Issue Advances in Porous Lightweight Materials and Lattice Structures)
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24 pages, 15484 KB  
Article
On the Process Optimization, Microstructure Characterization and Mechanical Performance of Ti65 Titanium Alloy Produced by Laser Powder Bed Fusion
by Yuan Meng, Xianglong Wang, Jinjun Wu, Haojie Wang, Ping Gan, Lei Lu, Chengjie Li, Tongling Ma, Jun Niu and Zhigang Zhang
Appl. Sci. 2025, 15(21), 11717; https://doi.org/10.3390/app152111717 - 3 Nov 2025
Viewed by 442
Abstract
Ti65 high-temperature titanium alloy, known for its exceptional high-temperature mechanical properties and oxidation resistance, demonstrates considerable potential for aerospace applications. Nevertheless, conventional manufacturing techniques are often inadequate for achieving high design freedom and fabricating complex geometries. This study presents a systematic investigation into [...] Read more.
Ti65 high-temperature titanium alloy, known for its exceptional high-temperature mechanical properties and oxidation resistance, demonstrates considerable potential for aerospace applications. Nevertheless, conventional manufacturing techniques are often inadequate for achieving high design freedom and fabricating complex geometries. This study presents a systematic investigation into the process optimization, microstructure characterization, and mechanical performance of Ti65 alloy produced by laser powder bed fusion (LPBF). Via meticulously designed single-track, multi-track, and bulk sample experiments, the influences of laser power (P), scanning speed (V), and hatch spacing (h) on molten pool behavior, defect formation, microstructural evolution, and surface roughness were thoroughly examined. The results indicate that under optimized parameters, the specimens attain ultra-high dimensional accuracy, with a near-full density (>99.99%) and reduced surface roughness (Ra = 3.9 ± 1.3 μm). Inadequate energy input (low P or high V) led to lack-of-fusion defects, whereas excessive energy (high P or low V) resulted in keyhole porosity. Microstructural analysis revealed that the rapid solidification inherent to LPBF promotes the formation of fine acicular α′-phase (0.236–0.274 μm), while elevated laser power or reduced scanning speed facilitated the development of coarse lamellar α′-martensite (0.525–0.645 μm). Tensile tests demonstrated that samples produced under the optimized parameters exhibit high ultimate tensile strength (1489 ± 7.5 MPa), yield strength (1278 ± 5.2 MPa), and satisfactory elongation (5.7 ± 0.15%), alongside elevated microhardness (446.7 ± 1.7 HV0.2). The optimized microstructure thereby enables the simultaneous achievement of high density and superior mechanical properties. The fundamental mechanism is attributed to precise control over volumetric energy density, which governs melt pool mode, defect generation, and solidification kinetics, thereby tailoring the resultant microstructure. This study offers valuable insights into defect suppression, microstructure control, and process optimization for LPBF-fabricated Ti65 alloy, facilitating its application in high-temperature structural components. Full article
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27 pages, 6425 KB  
Review
Thermal Insulation and Fireproof Aerogel Composites for Automotive Batteries
by Xianbo Hou, Jia Chen, Xuelei Fang, Rongzhu Xia, Shaowei Zhu, Tao Liu, Keyu Zhu and Liming Chen
Gels 2025, 11(10), 791; https://doi.org/10.3390/gels11100791 - 2 Oct 2025
Viewed by 1598
Abstract
New energy vehicles face a critical challenge in balancing the thermal safety management of high-specific-energy battery systems with the simultaneous improvement of energy density. With the large-scale application of high-energy-density systems such as silicon-based anodes and solid-state batteries, their inherent thermal runaway risks [...] Read more.
New energy vehicles face a critical challenge in balancing the thermal safety management of high-specific-energy battery systems with the simultaneous improvement of energy density. With the large-scale application of high-energy-density systems such as silicon-based anodes and solid-state batteries, their inherent thermal runaway risks pose severe challenges to battery thermal management systems (BTMS). Currently, the thermal insulation performance, temperature resistance, and fire protection capabilities of flame-retardant materials (e.g., foam cotton, fiber felts) used in automotive batteries are inadequate to meet the demands of intense combustion and high temperatures generated during thermal failure in high-energy-density batteries. Against this backdrop, thermal insulation and fireproof aerogel materials are emerging as a revolutionary solution for the next generation of power battery thermal protection systems. Leveraging their nanoporous structure’s exceptional thermal insulation properties (thermal conductivity of 0.013–0.018 W/(m·K) at room temperature) and extreme fire resistance (temperature resistance > 1100 °C/UL94 V-0 flame retardancy), aerogels are gaining prominence. This article provides a systematic review of thermal runaway phenomena in automotive batteries and corresponding protective measures. It highlights recent breakthroughs in the selection of material systems, optimization of preparation processes, and fiber–matrix composite technologies for automotive fireproof aerogel composites. The core engineering values of these materials, such as blocking thermal runaway propagation, reducing system weight, and improving volumetric efficiency, are quantitatively validated. Furthermore, the paper explores future research directions, including the development of low-cost aerogel composites and the design of organic–inorganic hybrid composite structures, aiming to provide a foundation and industrial pathway for the research and development of next-generation high-performance battery thermal management systems. Full article
(This article belongs to the Special Issue Aerogels: Synthesis and Applications)
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33 pages, 7822 KB  
Article
High-Performance Two-Stroke Opposed-Piston Hydrogen Engine: Numerical Study on Injection Strategies, Spark Positioning and Water Injection to Mitigate Pre-Ignition
by Alessandro Marini, Sebastiano Breda, Roberto Tonelli, Michele Di Sacco and Alessandro d’Adamo
Energies 2025, 18(19), 5181; https://doi.org/10.3390/en18195181 - 29 Sep 2025
Viewed by 685
Abstract
In the pursuit of zero-emission mobility, hydrogen represents a promising fuel for internal combustion engines. However, its low volumetric energy density poses challenges, especially for high-performance applications where compactness and lightweight design are crucial. This study investigates the feasibility of an innovative hydrogen-fueled [...] Read more.
In the pursuit of zero-emission mobility, hydrogen represents a promising fuel for internal combustion engines. However, its low volumetric energy density poses challenges, especially for high-performance applications where compactness and lightweight design are crucial. This study investigates the feasibility of an innovative hydrogen-fueled two-stroke opposed-piston (2S-OP) engine, targeting a specific power of 130 kW/L and an indicated thermal efficiency above 40%. A detailed 3D-CFD analysis is conducted to evaluate mixture formation, combustion behavior, abnormal combustion and water injection as a mitigation strategy. Innovative ring-shaped multi-point injection systems with several designs are tested, demonstrating the impact of injector channels’ orientation on the final mixture distribution. The combustion analysis shows that a dual-spark configuration ensures faster combustion compared to a single-spark system, with a 27.5% reduction in 10% to 90% combustion duration. Pre-ignition is identified as the main limiting factor, strongly linked to mixture stratification and high temperatures. To suppress it, water injection is proposed. A 55% evaporation efficiency of the water mass injected lowers the in-cylinder temperature and delays pre-ignition onset. Overall, the study provides key design guidelines for future high-performance hydrogen-fueled 2S-OP engines. Full article
(This article belongs to the Special Issue Internal Combustion Engines: Research and Applications—3rd Edition)
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24 pages, 3089 KB  
Article
Optimal Sizing of a Wind-Powered Green Ammonia Plant for Maritime Fuel Supply—A Case in the Greater Bay Area
by Yimiao Gu and Weihao Lan
Energies 2025, 18(19), 5157; https://doi.org/10.3390/en18195157 - 28 Sep 2025
Viewed by 673
Abstract
Green ammonia has emerged as a promising alternative fuel for maritime decarbonization, owing to its carbon-free combustion, favorable volumetric energy density, and well-established logistics infrastructure compared to other alternatives. However, critical gaps persist in the development of an integrated fuel supply framework, which [...] Read more.
Green ammonia has emerged as a promising alternative fuel for maritime decarbonization, owing to its carbon-free combustion, favorable volumetric energy density, and well-established logistics infrastructure compared to other alternatives. However, critical gaps persist in the development of an integrated fuel supply framework, which hinders the large-scale adoption of ammonia-fueled vessels. Therefore, this paper proposes an onshore wind-powered green ammonia plant located along the Gaolan–Yangpu feeder route. The plant comprises PEM electrolysis, nitrogen separation, Haber–Bosch synthesis, and storage facilities. An optimal plant configuration is subsequently derived through hourly simulations based on wind power generation and a priority-based capacity expansion algorithm. Key findings indicate that a stable ammonia supply—synchronized with monsoon wind patterns and capable of fueling vessels with 10 MW propulsion systems consuming around 680 tons per fortnight—requires a 72 MW onshore wind farm, a 63 MW PEM electrolyzer, 3.6 MW of synthesis facility, and 3205 tons of storage. This configuration yields a levelized cost of ammonia (LCOA) of approximately USD 700/ton, with wind turbines and electrolyzers (including replacement costs) accounting for over 70% of the total cost. Sensitivity analysis further shows that wind turbine and electrolyzer prices are the primary factors affecting ammonia costs. Although variations in operational parameters may significantly alter final configuration, they cause only minor (±1%) fluctuations in the levelized cost without significantly altering its overall trend. Full article
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15 pages, 3903 KB  
Article
Stabilization of Ultrafine Iron Tailings with Acrylic–Styrene Copolymer for Sustainable Geotechnical Applications
by Matheus Machado Lopes, José Wilson dos Santos Ferreira and Michéle Dal Toé Casagrande
Polymers 2025, 17(19), 2624; https://doi.org/10.3390/polym17192624 - 28 Sep 2025
Viewed by 348
Abstract
Considerable research in recent years has examined the reuse of tailings; however, the lack of particle cohesion limits their application as construction materials. Therefore, this study assessed the stabilization of ultrafine iron ore tailings using an acrylic–styrene copolymer. Geotechnical characterization and polymer dosage, [...] Read more.
Considerable research in recent years has examined the reuse of tailings; however, the lack of particle cohesion limits their application as construction materials. Therefore, this study assessed the stabilization of ultrafine iron ore tailings using an acrylic–styrene copolymer. Geotechnical characterization and polymer dosage, hydromechanical and microstructural tests were carried out, including unconfined compressive strength (UCS), permeability, scanning electron microscopy (SEM) and microtomography (μCT). The polymer effectively enhanced the mechanical behavior of the tailings, increasing the UCS from 49 kPa for untreated material to 2114 kPa and 3324 kPa for 30% and 40% polymer content, respectively. A robust power-law model (R2 ≥ 0.90), based on the porosity/volumetric polymer index (η/Pᵢᵥ), was developed to predict strength, showing that mechanical gains can be achieved by increasing either polymer content or dry density, as supported by statistical analyses. Permeability remained on the order of 10−6 cm/s regardless of polymer addition, indicating that the polymer does not fill voids but instead acts as a binding agent, as confirmed by SEM and μCT analyses. Overall, this study establishes a technically feasible and sustainable approach for tailings management, highlighting the potential of polymer stabilization to turn environmentally challenging tailings into functional geotechnical materials. Full article
(This article belongs to the Section Polymer Composites and Nanocomposites)
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26 pages, 3363 KB  
Article
Energy-Efficient Coaxial Electrocoagulation for Integrated Treatment of Urban Wastewater and Acid Mine Drainage: A Response-Surface Approach
by Katherin Quispe-Ramos, Edilberto Melgar-Izaguirre, José Rivera-Rodríguez, César Gutiérrez-Cuba, Luis Carrasco-Venegas, Cesar Rodriguez-Aburto, Yone Ramos-Balcázar and Alex Pilco-Nuñez
Appl. Sci. 2025, 15(19), 10452; https://doi.org/10.3390/app151910452 - 26 Sep 2025
Cited by 1 | Viewed by 742
Abstract
This study determined the influence of experimental factors such as current density, surface-to-volume ratio (S/V), and contact time on the removal of Chemical Oxygen Demand (COD) and energy consumption during electrocoagulation, aiming to optimize the efficiency of a coaxial electrocoagulator for the co-treatment [...] Read more.
This study determined the influence of experimental factors such as current density, surface-to-volume ratio (S/V), and contact time on the removal of Chemical Oxygen Demand (COD) and energy consumption during electrocoagulation, aiming to optimize the efficiency of a coaxial electrocoagulator for the co-treatment of municipal wastewater and acid mine drainage. After identifying the optimal volumetric ratio between both types of effluents, a Box–Behnken design and response-surface methodology were employed to identify the conditions that maximize COD removal while minimizing energy consumption. Under optimal conditions (current density of 2.42 A·m−2, S/V = 300 m2·m−3, 60 min), a COD removal of 91.13% was achieved with a specific energy of =2.59 kWh·kgCOD−1. The statistical model for COD removal demonstrated a good fit (R2 = 0.87), though its predictive power was limited (predicted R2 = 0.53). In contrast, the model for energy consumption exhibited an outstanding fit (R2 = 0.99) and high predictive consistency (predicted R2 = 0.98), confirming the decisive influence of current density on energy demand. Additionally, the S/V ratio emerged as the most impactful factor in COD removal variability. Overall, the findings highlight the importance of balancing removal efficiency with the economic feasibility of the process, contributing to the design of more sustainable and effective strategies for integrated wastewater treatment. Full article
(This article belongs to the Special Issue Environmental Pollution and Wastewater Treatment Strategies)
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20 pages, 5197 KB  
Article
Study on SLM Forming Parameters of Al2O3/CoCr Metal Matrix Composites
by Qin Hong, Peikang Bai, Jianhong Wang and Wei Liu
Coatings 2025, 15(9), 1015; https://doi.org/10.3390/coatings15091015 - 1 Sep 2025
Viewed by 534
Abstract
In the present study, a finite element-based numerical simulation approach was employed to investigate the temperature field distribution and variations in molten pool dimensions during the selective laser melting (SLM) forming process of Al2O3/CoCr metal matrix composites. Building [...] Read more.
In the present study, a finite element-based numerical simulation approach was employed to investigate the temperature field distribution and variations in molten pool dimensions during the selective laser melting (SLM) forming process of Al2O3/CoCr metal matrix composites. Building on this foundation, the present work explored the regulatory effects of volumetric energy density (VED) on the performance of SLM-fabricated components. Ultimately, the optimal process parameters for the selective laser melting of Al2O3/CoCr metal matrix composites were identified and established. The results show that when the laser power is in the range of 150–250 W and the scanning speed is 700–1100 mm/s, it is beneficial to the SLM forming of Al2O3/CoCr metal matrix composites. When the VED is between 133.3 J/mm3 and 171.4 J/mm3, the microstructural defects of the composite are the least. The optimal SLM process parameters are finally determined as follows: laser power 200 W, scanning speed 700 mm/s, scanning line spacing 0.06 mm, and hatch spacing 0.03 mm. Full article
(This article belongs to the Special Issue Trends in Coatings and Surface Technology, 3rd Edition)
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41 pages, 6887 KB  
Review
Charging the Future with Pioneering MXenes: Scalable 2D Materials for Next-Generation Batteries
by William Coley, Amir-Ali Akhavi, Pedro Pena, Ruoxu Shang, Yi Ma, Kevin Moseni, Mihrimah Ozkan and Cengiz S. Ozkan
Nanomaterials 2025, 15(14), 1089; https://doi.org/10.3390/nano15141089 - 14 Jul 2025
Cited by 3 | Viewed by 1071
Abstract
MXenes, a family of two-dimensional carbide and nitride nanomaterials, have demonstrated significant promise across various technological domains, particularly in energy storage applications. This review critically examines scalable synthesis techniques for MXenes and their potential integration into next-generation rechargeable battery systems. We highlight both [...] Read more.
MXenes, a family of two-dimensional carbide and nitride nanomaterials, have demonstrated significant promise across various technological domains, particularly in energy storage applications. This review critically examines scalable synthesis techniques for MXenes and their potential integration into next-generation rechargeable battery systems. We highlight both top-down and emerging bottom-up approaches, exploring their respective efficiencies, environmental impacts, and industrial feasibility. The paper further discusses the electrochemical behavior of MXenes in lithium-ion, sodium-ion, and aluminum-ion batteries, as well as their multifunctional roles in solid-state batteries—including as electrodes, additives, and solid electrolytes. Special emphasis is placed on surface functionalization, interlayer engineering, and ion transport properties. We also compare MXenes with conventional graphite anodes, analyzing their gravimetric and volumetric performance potential. Finally, challenges such as diffusion kinetics, power density limitations, and scalability are addressed, providing a comprehensive outlook on the future of MXenes in sustainable energy storage technologies. Full article
(This article belongs to the Special Issue Pioneering Nanomaterials: Revolutionizing Energy and Catalysis)
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17 pages, 5457 KB  
Article
Multiphysics Modeling of Heat Transfer and Melt Pool Thermo-Fluid Dynamics in Laser-Based Powder Bed Fusion of Metals
by Tingzhong Zhang, Xijian Lin, Yanwen Qin, Dehua Zhu, Jing Wang, Chengguang Zhang and Yuchao Bai
Materials 2025, 18(13), 3183; https://doi.org/10.3390/ma18133183 - 5 Jul 2025
Viewed by 967
Abstract
Laser-based powder bed fusion of metals (PBF-LB/M) is one of the most promising additive manufacturing technologies to fabricate complex-structured metal parts. However, its corresponding applications have been limited by technical bottlenecks and increasingly strict industrial requirements. Process optimization, a scientific issue, urgently needs [...] Read more.
Laser-based powder bed fusion of metals (PBF-LB/M) is one of the most promising additive manufacturing technologies to fabricate complex-structured metal parts. However, its corresponding applications have been limited by technical bottlenecks and increasingly strict industrial requirements. Process optimization, a scientific issue, urgently needs to be solved. In this paper, a three-phase transient model based on the level-set method is established to examine the heat transfer and melt pool behavior in PBF-LB/M. Surface tension, the Marangoni effect, and recoil pressure are implemented in the model, and evaporation-induced mass and thermal loss are fully considered in the computing element. The results show that the surface roughness and density of metal parts induced by heat transfer and melt pool behavior are closely related to process parameters such as laser power, layer thickness, scanning speed, etc. When the volumetric energy density is low, the insufficient fusion of metal particles leads to pore defects. When the line energy density is high, the melt track is smooth with low porosity, resulting in the high density of the products. Additionally, the partial melting of powder particles at the beginning and end of the melting track usually contributes to pore formation. These findings provide valuable insights for improving the quality and reliability of metal additive manufacturing. Full article
(This article belongs to the Special Issue Latest Developments in Advanced Machining Technologies for Materials)
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18 pages, 2905 KB  
Article
Size Reduction in Micro Gas Turbines Using Silicon Carbide
by Ahmad Abuhaiba
Gases 2025, 5(3), 14; https://doi.org/10.3390/gases5030014 - 2 Jul 2025
Viewed by 1876
Abstract
Micro gas turbines serve small-scale generation where swift response and low emissions are highly valued, and they are commonly fuelled by natural gas. True to their ‘micro’ designation, their size is indeed compact; however, a noteworthy portion of the enclosure is devoted to [...] Read more.
Micro gas turbines serve small-scale generation where swift response and low emissions are highly valued, and they are commonly fuelled by natural gas. True to their ‘micro’ designation, their size is indeed compact; however, a noteworthy portion of the enclosure is devoted to power electronics components. This article considers whether these components can be made even smaller by substituting their conventional silicon switches with switches fashioned from silicon carbide. The wider bandgap of silicon carbide permits stronger electric fields and reliable operation at higher temperatures, which together promise lower switching losses, less heat, and simpler cooling arrangements. This study rests on a simple volumetric model. Two data sets feed the model. First come the manufacturer specifications for a pair of converter modules (one silicon, the other silicon carbide) with identical operation ratings. Second are the operating data and dimensions of a commercial 100 kW micro gas turbine. The model splits the converter into two parts: the semiconductor package and its cooling hardware. It then applies scaling factors that capture the higher density of silicon carbide and its lower switching losses. Lower switching losses reduce generated heat, so heatsinks, fans, or coolant channels can be slimmer. Together these effects shrink the cooling section and, therefore, the entire converter. The findings show that a micro gas turbine inverter built with silicon carbide occupies about one fifth less space and delivers more than a quarter higher power density than its silicon counterpart. Full article
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18 pages, 4806 KB  
Article
Laser Powder Bed Fusion Additive Manufacturing of a CoCrFeNiCu High-Entropy Alloy: Processability, Microstructural Insights, and (In Situ) Mechanical Behavior
by Vito Burgio and Ghazal Moeini
Materials 2025, 18(13), 3071; https://doi.org/10.3390/ma18133071 - 27 Jun 2025
Viewed by 1025
Abstract
High-entropy alloys are known for their promising mechanical properties, wear and corrosion resistance, which are maintained across a wide range of temperatures. In this study, a CoCrFeNiCu-based high-entropy alloy, distinguished from conventional CoCrFeNi systems by the addition of Cu, which is known to [...] Read more.
High-entropy alloys are known for their promising mechanical properties, wear and corrosion resistance, which are maintained across a wide range of temperatures. In this study, a CoCrFeNiCu-based high-entropy alloy, distinguished from conventional CoCrFeNi systems by the addition of Cu, which is known to enhance toughness and wear resistance, was investigated to better understand the effects of compositional modification on processability and performance. The influence of key process parameters, specifically laser power and scan speed, on the processability of CoCrFeNiCu-based high-entropy alloys produced by laser powder bed fusion additive manufacturing was investigated, with a focus of low laser power, which is critical for minimizing defects and improving the resulting microstructure and mechanical performance. The printed sample density gradually increases with higher volumetric energy density, achieving densities exceeding 99.0%. However, at higher energy densities, the samples exhibit susceptibility to hot cracking, an issue that cannot be mitigated by adjusting the process parameters. Mechanical properties under optimized parameters were further evaluated using Charpy impact and (in situ) tensile tests. These evaluations were supplemented by in situ tensile experiments conducted within a scanning electron microscope to gain insights into the behavior of defects, such as hot cracks, during tensile testing. Despite the sensitivity to hot cracking, the samples exhibited a respectable ultimate tensile strength of 662 MPa, comparable to fine-grained steels like S500MC (070XLK). These findings underscore the potential of CoCrFeNiCu-based high-entropy alloys for advanced applications. However, they also highlight the necessity for developing strategies to ensure stable and reliable processing methods that can mitigate the susceptibility to hot cracking. Full article
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18 pages, 1379 KB  
Article
The Evaluation and Development of a Prediction Artificial Neural Network Model for Specific Volumetric Fuel Efficiency (SVFE) of a Tractor–Chisel Plow System Based on Field Operation
by Saleh M. Al-Sager, Saad S. Almady, Waleed A. Almasoud, Abdulrahman A. Al-Janobi, Samy A. Marey, Saad A. Al-Hamed and Abdulwahed M. Aboukarima
Processes 2025, 13(6), 1811; https://doi.org/10.3390/pr13061811 - 7 Jun 2025
Viewed by 802
Abstract
For every tractor test carried out on a concrete road under defined conditions, the Nebraska Tractor Test Laboratory (NTTL) provides values of the specific volumetric fuel efficiency (SVFE) in unit of kWh/L). Because soil tillage is a highly energy-intensive process and the energy [...] Read more.
For every tractor test carried out on a concrete road under defined conditions, the Nebraska Tractor Test Laboratory (NTTL) provides values of the specific volumetric fuel efficiency (SVFE) in unit of kWh/L). Because soil tillage is a highly energy-intensive process and the energy consumption of tillage operations is a significant component of a farm budget, there is a growing amount of attention being given to the examination of the SVFE for tillage operations. Nonetheless, the study of the tillage process and a scientific approach to the tillage process are becoming more and more dependent on scientific modeling. Therefore, in this study based on real-tillage field operation, an artificial neural network (ANN) model was built to predict SVFE. This study aimed to confirm that the ANN model could incorporate 10 inputs for prediction: initial soil moisture content, draft force, initial soil bulk density, sand, silt, and clay proportions in the soil tractor power, plow width, tillage depth, and tillage speed. The Qnet v2000, as an ANN simulation software, was employed for the simulation of the SVFE. In this regard, 20,000 runs of Qnet v2000 were completed for the training and testing stages. The anticipated results displayed that the determination coefficient (R2) was larger than 0.96; using the training dataset, R2 was 0.982 and using the testing dataset, R2 was 0.9741, indicating that the recognition of a full ANN model makes it likely to reply to essential enquiries that were previously unanswerable regarding the impact of working and soil conditions on the SVFE of a tractor–tillage implement system. Additionally, sensitivity analyses were completed to specify which modeled parameters were more sensitive to the factors using the obtained ANN model. According to the sensitivity analysis, SVFE was more affected by changes in the tillage speed (21.07%), silt content in the soil (15.56%), draft force (11.01%), and clay content in the soil (10.86%). Predicting SVFE can lead to more appropriate decisions on tractor–chisel plow combination management. Therefore, it is highly advisable to use the newly created ANN model to appropriately manage SVFE to reduce tractor–tillage implement energy dissipation. Additionally, suitable management of some variables, for example, tillage depth, tillage speed, and soil moisture content, can help enhance fuel consumption in the tractor–tillage implementation system. Full article
(This article belongs to the Section Sustainable Processes)
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10 pages, 9064 KB  
Communication
Effects of Process Parameters on Forming Quality and Microstructure of FeCrAl-ODS Alloy Fabricated by Selective Laser Melting
by Shenghua Zhang, Fudong Li, Yu Wang, Hongwen Su and Jun Li
Materials 2025, 18(11), 2462; https://doi.org/10.3390/ma18112462 - 24 May 2025
Viewed by 683
Abstract
This study systematically investigated the effects of selective laser melting (SLM) process parameters on the forming quality and microstructure of FeCrAl oxide dispersion-strengthened (ODS) alloy. Through orthogonal experimental design, the influences of laser power (300–320 W), scanning speed (650–850 mm/s), and hatch spacing [...] Read more.
This study systematically investigated the effects of selective laser melting (SLM) process parameters on the forming quality and microstructure of FeCrAl oxide dispersion-strengthened (ODS) alloy. Through orthogonal experimental design, the influences of laser power (300–320 W), scanning speed (650–850 mm/s), and hatch spacing (0.05–0.07 mm) on the surface morphology and internal defects of as-built samples were analyzed. The microstructural evolution under different volumetric energy densities (VED) was also analyzed. The results indicate that hatch spacing significantly affected crack and pore formation, with minimal defects observed at 0.06 mm. Excessive laser power (320 W) or VED (318.0 J/mm3) led to elevated melt pool temperatures, causing element evaporation, grain coarsening, and <100> preferential oriented texture, thereby reducing hardness to 234 HV. The optimal parameters—laser power of 310 W, scanning speed of 650 mm/s, and hatch spacing of 0.06 mm (VED 265.0 J/mm3)—yielded the highest hardness (293 HV), fine-grained structures, and a high proportion of low-angle grain boundaries (LAGBs) with significant residual stress. This research provides a theoretical foundation for optimizing SLM processes for FeCrAl-ODS alloys. Full article
(This article belongs to the Special Issue Laser Technology for Materials Processing)
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