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Int. J. Mol. Sci., Volume 7, Issue 5 (May-June 2006), Pages 130-185

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Open AccessArticle Reaction of 2,2-Diphenyl-1-picrylhydrazyl with HO•, O2•, HO ,and HOO Radicals and Anions
Int. J. Mol. Sci. 2006, 7(5), 130-143; doi:10.3390/i7050130
Received: 24 March 2006 / Accepted: 15 May 2006 / Published: 15 May 2006
Cited by 13 | PDF Full-text (116 KB) | HTML Full-text | XML Full-text
Abstract
Using electronic absorption spectra and thin layer chromatography, the reactionof 2,2-diphenyl-1-picrylhydrazyl (DPPH) with O2•, HO•, HO, and HOO anions and freeradicals revealed the formation of the para-nitro- and para-hydroxy-derivatives of 2,2-diphenyl-1-picrylhydrazine (DPPH-H) and of DPPH fragmentation products(diphenylamine, [...] Read more.
Using electronic absorption spectra and thin layer chromatography, the reactionof 2,2-diphenyl-1-picrylhydrazyl (DPPH) with O2•, HO•, HO, and HOO anions and freeradicals revealed the formation of the para-nitro- and para-hydroxy-derivatives of 2,2-diphenyl-1-picrylhydrazine (DPPH-H) and of DPPH fragmentation products(diphenylamine, tetraphenylhydrazine). The reaction of DPPH with the O2•anion-radical(from KO2 in benzene solution at room temperature in the presence of 18-crown-6 ether) ispseudo-first-order during the first 25 minutes. Full article
Open AccessArticle Characteristic and Synthetic Approach of Molecularly Imprinted Polymer
Int. J. Mol. Sci. 2006, 7(5), 155-178; doi:10.3390/i7050155
Received: 12 April 2006 / Accepted: 27 June 2006 / Published: 29 June 2006
Cited by 133 | PDF Full-text (174 KB) | HTML Full-text | XML Full-text
Abstract
Molecularly imprinted polymers (MIP) exhibiting high selectivity and affinity tothe predetermined molecule (template) are now seeing a fast growing research. However,optimization of the imprinted products is difficult due to the fact that there are manyvariables to consider, some or all of which [...] Read more.
Molecularly imprinted polymers (MIP) exhibiting high selectivity and affinity tothe predetermined molecule (template) are now seeing a fast growing research. However,optimization of the imprinted products is difficult due to the fact that there are manyvariables to consider, some or all of which can potentially impact upon the chemical,morphological and molecular recognition properties of the imprinted materials. This reviewpresent a summary of the principal synthetic considerations pertaining to good practice in thepolymerization aspects of molecular imprinting, and is primarily aimed at researcher familiarwith molecular imprinting methods but with little or no prior experience in polymersynthesis. The synthesis, characteristic, effect of molecular recognition and differentpreparation methods of MIP in recent few years are discussed in this review, unsolvedproblems and possible developments of MIP were also been briefly discussed. Full article
Open AccessArticle Synthesis and Structure of a Binuclear Cu(II) Complex of 1,3- bis [N,N-bis(2-picolyl)amino]propan-2-ol
Int. J. Mol. Sci. 2006, 7(5), 179-185; doi:10.3390/i7050179
Received: 14 June 2006 / Accepted: 26 June 2006 / Published: 29 June 2006
Cited by 2 | PDF Full-text (162 KB) | HTML Full-text | XML Full-text
Abstract
The synthesis and crystal structure of Cu(II) complex of a binucleating tridentateligand 1,3-bis [N,N-bis(2-picolyl)amino]propan-2-ol (I) is being reported. The two chelatingbispicolylamine arms in I are tethered by a 2-hydroxypropyl group with Cu(II) coordinatingin a slightly distorted square planar geometry to give [Cu [...] Read more.
The synthesis and crystal structure of Cu(II) complex of a binucleating tridentateligand 1,3-bis [N,N-bis(2-picolyl)amino]propan-2-ol (I) is being reported. The two chelatingbispicolylamine arms in I are tethered by a 2-hydroxypropyl group with Cu(II) coordinatingin a slightly distorted square planar geometry to give [Cu2(I)(OH2)(Cl)](ClO4)3·2H2O (II).The crystal data for II: Triclinic, space group Pī with cell dimensions of a = 13.345 (4) å,b = 13.873 (4) å, c = 12.867 (2) å, α = 111.68 (2)°, β = 100.34 (2)°, γ = 65.83 (2)°, V =2018.4 (9) å3, F.W. = 962.46, ρcalc = 1.583 g cm-3 for Z = 2, μ = 13.93 cm-1 Full article

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Open AccessCorrection Publisher's Note - Overlapping Pagination Error
Int. J. Mol. Sci. 2006, 7(5), 144-154; doi:10.3390/i7050144
Published: 3 August 2006
PDF Full-text (104 KB) | HTML Full-text | XML Full-text
Abstract
Publisher's Note added on 3 August 2006: There is an overlapping pagination error. The paper "Int. J. Mol. Sci. 2006, 7, 131-154" is republished as "Int. J. Mol. Sci. 2006, 7, 231-254. Pages 144-154 are thus taken as [...] Read more.
Publisher's Note added on 3 August 2006: There is an overlapping pagination error. The paper "Int. J. Mol. Sci. 2006, 7, 131-154" is republished as "Int. J. Mol. Sci. 2006, 7, 231-254. Pages 144-154 are thus taken as blank pages. We apologize for this error and for any inconvenience. Full article

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