Table of Contents
Batteries, Volume 3, Issue 3 (September 2017)
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Cover Story (view full-size image) We have investigated a chloride-free, sol-gel synthesis of antimony products for use in Na-ion [...] Read more. We have investigated a chloride-free, sol-gel synthesis of antimony products for use in Na-ion batteries. Over a dozen compositions were prepared from citric acid and antimony acetate or oxide, leading to differing ratios of crystalline Sb, amorphous carbon, and traces of Sb2O3. We have identified several key synthetic parameters in the search for a facile, one-pot route. The influence of reaction conditions on particle size, morphology, and electrochemistry is discussed in detail. View this paper