Influence of Non-Thermal Atmospheric Pressure Plasma Treatment on Shear Bond Strength between Y-TZP and Self-Adhesive Resin Cement
Abstract
:1. Introduction
2. Materials and Methods
2.1. Preparation of Y-TZP Specimens
2.2. Non-thermal Atmospheric Pressure Plasma (NTP) Treatment
2.3. Contact Angle Measurement and Surface Energy (SE) Analysis
2.4. Shear Bond Strength (SBS) Test
2.4.1. Fabrication of Y-TZP Specimens Bonded with Self-Adhesive Resin Cement Cylinders
2.4.2. Thermocycling Process and Shear Bond Strength (SBS) Measurement
2.5. Failure Mode Analysis
2.6. Statistical Analysis
3. Results
3.1. Contact Angle Measurement and Surface Energy (SE) Analysis
3.2. Shear Bond Strength (SBS) Test
3.3. Failure Mode Analysis
4. Discussion
5. Conclusions
Author Contributions
Funding
Conflicts of Interest
References
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Groups | Distribution of Y-TZP specimens (n) | ||||
---|---|---|---|---|---|
Surface Energy (SE) analysis | Shear Bond Strength (SBS) test | ||||
G-CEM LinkAce | RelyX U200 | ||||
Non-thermocycling | Thermocycling | Non-thermocycling | Thermocycling | ||
Control | 3 | 10 | 10 | 10 | 10 |
NTP | 3 | 10 | 10 | 10 | 10 |
Sb | 3 | 10 | 10 | 10 | 10 |
Sb + NTP | 3 | 10 | 10 | 10 | 10 |
Material | Manufacture | Type | Composition |
---|---|---|---|
G-CEM LinkAce | GC Corporation, Tokyo, Japan | Self-adhesive Dual-cure Automix | Paste A: Fluoroalumino silicate glass, Urethane dimethacrylate (UDMA), Dimethacrylate, Pigment, Silicon dioxide, Initiator, Inhibitor |
Paste B: Urethane dimethacrylate (UDMA), Dimethacrylate, Phosphoric acid ester monomer, Initiator, stabilizer | |||
RelyX U200 | 3M ESPE, St. Paul, MN, USA | Self-adhesive Dual-cure Automix | Base paste: Methacrylate monomers containing phosphoric acid groups, Methacrylate monomers, Silanated fillers, Initiator components, Stabilizers, Rheological additives |
Catalyst paste: Methacrylate monomers, Alkaline(basic) fillers, Silanated fillers, Initiator components, Stabilizers, Pigments, Rheological additives |
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Kim, D.-S.; Ahn, J.-J.; Bae, E.-B.; Kim, G.-C.; Jeong, C.-M.; Huh, J.-B.; Lee, S.-H. Influence of Non-Thermal Atmospheric Pressure Plasma Treatment on Shear Bond Strength between Y-TZP and Self-Adhesive Resin Cement. Materials 2019, 12, 3321. https://doi.org/10.3390/ma12203321
Kim D-S, Ahn J-J, Bae E-B, Kim G-C, Jeong C-M, Huh J-B, Lee S-H. Influence of Non-Thermal Atmospheric Pressure Plasma Treatment on Shear Bond Strength between Y-TZP and Self-Adhesive Resin Cement. Materials. 2019; 12(20):3321. https://doi.org/10.3390/ma12203321
Chicago/Turabian StyleKim, Dae-Sung, Jong-Ju Ahn, Eun-Bin Bae, Gyoo-Cheon Kim, Chang-Mo Jeong, Jung-Bo Huh, and So-Hyoun Lee. 2019. "Influence of Non-Thermal Atmospheric Pressure Plasma Treatment on Shear Bond Strength between Y-TZP and Self-Adhesive Resin Cement" Materials 12, no. 20: 3321. https://doi.org/10.3390/ma12203321