Preparation and Characterization of Hydroxyapatite Coating on AZ31 Magnesium Alloy Induced by Carboxymethyl Cellulose-Dopamine
Abstract
:1. Introduction
2. Materials and Methods
2.1. Preparation of AZ31 Samples
2.2. Synthesis of Carboxymethyl Cellulose–Dopamine (CMC-DA) Hydrogels
2.3. Preparation of CMC-DA Films on AZ31 Surfaces
2.4. CMC-DA-Assisted Hydroxyapatite (HA) Formation
2.5. Surface Characterization
2.6. Corrosion Characterization
2.6.1. Electrochemical Test
2.6.2. Hydrogen Evolution Test
2.7. Biocompatibility Evaluation
2.7.1. Materials Preparation
2.7.2. Cell Viability
2.7.3. Live/Dead Assay
3. Results and Discussion
3.1. Analysis of CMC-DA
3.2. Characterization of AZ31, AZ31/CMC-DA, AZ31/HA, and AZ31/CMC-DA/HA Surfaces
3.3. Corrosion Characterization
3.4. Cytocompatibility Tests
4. Conclusions
Author Contributions
Funding
Institutional Review Board Statement
Informed Consent Statement
Data Availability Statement
Acknowledgments
Conflicts of Interest
References
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Samples | Ecorr (V vs. Ag/AgCl) | icorr (A/cm2) |
---|---|---|
AZ31 | −1.53 ± 0.011 | (1.69 ± 0.050) × 10−5 |
AZ31/CMC-DA | −1.51 ± 0.007 | (1.52 ± 0.028) × 10−5 |
AZ31/HA | −1.42 ± 0.003 | (3.54 ± 0.231) × 10−6 |
AZ31/CMC-DA/HA | −1.35 ± 0.012 | (1.25 ± 0.003) × 10−6 |
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Yang, Y.; Wu, Y.; Wei, Y.; Zeng, T.; Cao, B.; Liang, J. Preparation and Characterization of Hydroxyapatite Coating on AZ31 Magnesium Alloy Induced by Carboxymethyl Cellulose-Dopamine. Materials 2021, 14, 1849. https://doi.org/10.3390/ma14081849
Yang Y, Wu Y, Wei Y, Zeng T, Cao B, Liang J. Preparation and Characterization of Hydroxyapatite Coating on AZ31 Magnesium Alloy Induced by Carboxymethyl Cellulose-Dopamine. Materials. 2021; 14(8):1849. https://doi.org/10.3390/ma14081849
Chicago/Turabian StyleYang, Yanxia, Yuanzhi Wu, Yu Wei, Tian Zeng, Baocheng Cao, and Jun Liang. 2021. "Preparation and Characterization of Hydroxyapatite Coating on AZ31 Magnesium Alloy Induced by Carboxymethyl Cellulose-Dopamine" Materials 14, no. 8: 1849. https://doi.org/10.3390/ma14081849