Synergistic Reinforcement with SEBS-g-MAH for Enhanced Thermal Stability and Processability in GO/rGO-Filled PC/ABS Composites
Abstract
:1. Introduction
2. Materials and Methods
2.1. Materials
2.2. Methods
2.2.1. Fabrication of Samples
2.2.2. Mechanical Properties Analysis
Tensile Testing
Flexural Testing
Impact Testing
2.2.3. Thermal Properties Analysis
2.2.4. FTIR Analysis
2.2.5. Rheological Properties Analysis
3. Results and Discussion
3.1. FTIR
3.2. Rheological Analysis
3.3. Mechanical Analysis
3.4. Thermal Analysis
4. Conclusions
Author Contributions
Funding
Institutional Review Board Statement
Data Availability Statement
Conflicts of Interest
References
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No. | Sample | PC/ABS (phr) | GO (phr) | rGO (phr) | SEBS-g-MAH (phr) |
---|---|---|---|---|---|
1 | PC/ABS | 100.0 | - | - | - |
2 | PAS1 | - | - | 1 | |
3 | PAS5 | - | - | 5 | |
4 | PAGO4.0 | 100.0 | 4.0 | - | - |
5 | PArGO4.0 | 100.0 | - | 4.0 | - |
6 | PAGO4.0-S1 | 100.0 | 4.0 | - | 1 |
7 | PAGO4.0-S5 | 100.0 | 4.0 | - | 5 |
8 | PArGO4.0-S1 | 100.0 | - | 4.0 | 1 |
9 | PArGO4.0-S5 | 100.0 | - | 4.0 | 5 |
Samples | PC/ABS | PAS-1 | PAS-5 | PAGO4.0 | PAGO4.0-S1 | PAGO4.0-S5 | PArGO4.0 | PArGO4.0-S1 | PArGO4.0-S5 |
---|---|---|---|---|---|---|---|---|---|
MFI (g/10 min) 260 °C, 3.8 kg | 13.27 | 17.79 | 17.07 | 12.68 | 19.29 | 19.31 | 11.14 | 16.63 | 17.98 |
Sample | TS (MPa) | YM (MPa) | EB (%) | FS (MPa) | FM (MPa) | ISN (kJ/m2) | ISUN (kJ/m2) |
---|---|---|---|---|---|---|---|
PC/ABS | 38.84 ± 1.2 c,d,e | 1041.60 ± 27.4 c,d | 29.09 ± 10.8 b | 29.55 ± 0.9 f | 421.52 ± 17.3 e | 38.68 ± 0.4 a | 54.11 ± 8.6 d,e |
PAS-1 | 39.38 ± 0.4 b,c,d | 1049.40 ± 20.9 b,c,d | 51.33 ± 9.0 a | 29.77 ± 0.1 e,f | 433.94 ± 10.0 d,e | 37.32 ± 0.3 a | 75.14 ± 4.6 b,c |
PAS-5 | 37.80 ± 1.3 d,e | 1062.40 ± 33.0 a,b,c,d | 45.83 ± 3.4 a | 30.44 ± 0.2 d,e | 423.74 ± 4.3 e | 36.91 ± 3.0 a | 86.69 ± 13.8 b |
PAGO-4.0 | 40.17 ± 1.1 a,b,c | 1092.40 ± 31.7 a,b | 13.14 ± 1.3 d | 31.57 ± 0.2 b,c | 456.24 ± 2.2 b,c | 9.70 ± 0.2 d | 48.75 ± 5.4 e |
PArGO-4.0 | 42.35 ± 1.1 a | 1095.00 ± 13.4 a | 9.97 ± 1.4 d | 32.39 ± 0.2 a | 485.28 ± 3.6 a | 5.47 ± 0.2 e | 52.54 ± 1.8 e |
PAGO4.0-S1 | 39.82 ± 0.5 b,c,d | 1067.60 ± 18.7 a,b,c,d | 15.40 ± 2.1 c,d | 31.97 ± 0.2 a,b | 460.11 ± 4.0 b | 10.50 ± 0.2 d | 79.97 ± 3.9 b,c |
PAGO4.0-S5 | 36.60 ± 0.5 e | 1028.20 ± 12.5 d | 17.51 ± 1.4 b,c,d | 30.82 ± 0.7 c,d | 440.71 ± 4.8 c,d | 11.47 ± 0.2 d | 85.28 ± 12.3 b,c |
PArGO4.0-S1 | 41.36 ± 0.7 a,b | 1074.80 ± 15.5 a,b,c | 10.84 ± 1.6 d | 32.04 ± 0.2 a,b | 464.16 ± 7.3 b | 4.66 ± 0.2 e | 51.18 ± 2.7 e |
PArGO4.0-S5 | 37.93 ± 2.1 c,d,e | 1068.80 ± 11.3 a,b,c,d | 17.28 ± 1.1 b,c,d | 31.48 ± 0.1 b,c | 455.36 ± 7.1 b,c | 4.61 ± 0.3 e | 69.57 ± 4.6 c,d |
Sample | Degradation Temperature | Inflection Point (°C) | Char Residue at 800 °C (%) | |||
---|---|---|---|---|---|---|
T5% | T10% | T50% | T80% | |||
PC/ABS | 410 | 423 | 457 | 488 | 462 | 6.24 |
PAS1 | 400 | 415 | 466 | 497 | 478 | 11.93 |
PAS5 | 408 | 420 | 451 | 481 | 445 | 9.82 |
PAGO04.0 | 357 | 402 | 438 | 461 | 438 | 4.80 |
PAGO4.0-S1 | 403 | 420 | 497 | 538 | 502 | 14.66 |
PAGO4.0-S5 | 404 | 419 | 486 | 521 | 497 | 13.63 |
PArGO4.0 | 397 | 415 | 449 | 512 | 449 | 14.40 |
PArGO4.0-S1 | 400 | 415 | 461 | 502 | 458 | 14.17 |
PArGO4.0-S5 | 402 | 417 | 469 | 510 | 464 | 13.69 |
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Joynal Abedin, F.N.; Fizal, A.N.S.; Alkarkhi, A.F.M.; Khalil, N.A.; Ahmad Yahaya, A.N.; Hossain, M.S.; Safie, S.I.; Ismail, N.A.; Zulkifli, M. Synergistic Reinforcement with SEBS-g-MAH for Enhanced Thermal Stability and Processability in GO/rGO-Filled PC/ABS Composites. Polymers 2024, 16, 2554. https://doi.org/10.3390/polym16182554
Joynal Abedin FN, Fizal ANS, Alkarkhi AFM, Khalil NA, Ahmad Yahaya AN, Hossain MS, Safie SI, Ismail NA, Zulkifli M. Synergistic Reinforcement with SEBS-g-MAH for Enhanced Thermal Stability and Processability in GO/rGO-Filled PC/ABS Composites. Polymers. 2024; 16(18):2554. https://doi.org/10.3390/polym16182554
Chicago/Turabian StyleJoynal Abedin, Fatin Najwa, Ahmad Noor Syimir Fizal, Abbas F. M. Alkarkhi, Nor Afifah Khalil, Ahmad Naim Ahmad Yahaya, Md. Sohrab Hossain, Sairul Izwan Safie, Nurul Ain Ismail, and Muzafar Zulkifli. 2024. "Synergistic Reinforcement with SEBS-g-MAH for Enhanced Thermal Stability and Processability in GO/rGO-Filled PC/ABS Composites" Polymers 16, no. 18: 2554. https://doi.org/10.3390/polym16182554