Journal Description
Processes
Processes
is an international, peer-reviewed, open access journal on processes/systems in chemistry, biology, material, energy, environment, food, pharmaceutical, manufacturing, automation control, catalysis, separation, particle and allied engineering fields published monthly online by MDPI. The Systems and Control Division of the Canadian Society for Chemical Engineering (CSChE S&C Division) and the Brazilian Association of Chemical Engineering (ABEQ) are affiliated with Processes and their members receive discounts on the article processing charges. Please visit Society Collaborations for more details.
- Open Access— free for readers, with article processing charges (APC) paid by authors or their institutions.
- High Visibility: indexed within Scopus, SCIE (Web of Science), Ei Compendex, Inspec, AGRIS, and other databases.
- Journal Rank: JCR - Q2 (Engineering, Chemical) / CiteScore - Q2 (Chemical Engineering (miscellaneous))
- Rapid Publication: manuscripts are peer-reviewed and a first decision is provided to authors approximately 13.7 days after submission; acceptance to publication is undertaken in 2.8 days (median values for papers published in this journal in the second half of 2023).
- Recognition of Reviewers: reviewers who provide timely, thorough peer-review reports receive vouchers entitling them to a discount on the APC of their next publication in any MDPI journal, in appreciation of the work done.
Impact Factor:
3.5 (2022);
5-Year Impact Factor:
3.4 (2022)
Latest Articles
Confluence Effect of Debris-Filled Damage and Temperature Variations on Guided-Wave Ultrasonic Testing (GWUT)
Processes 2024, 12(5), 957; https://doi.org/10.3390/pr12050957 - 8 May 2024
Abstract
Continuous monitoring of structural health is essential for the timely detection of damage and avoidance of structural failure. Guided-wave ultrasonic testing (GWUT) assesses structural damages by correlating its sensitive features with the damage parameter of interest. However, few or no studies have been
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Continuous monitoring of structural health is essential for the timely detection of damage and avoidance of structural failure. Guided-wave ultrasonic testing (GWUT) assesses structural damages by correlating its sensitive features with the damage parameter of interest. However, few or no studies have been performed on the detection and influence of debris-filled damage on GWUT under environmental conditions. This paper used the pitch–catch technique of GWUT, signal cross-correlation, statistical root mean square (RMS) and root mean square deviation (RMSD) to study the combined influence of varying debris-filled damage percentages and temperatures on damage detection. Through experimental result analysis, a predictive model with an R2 of about 78% and RMSE values of about was established. When validated, the model proved effective, with a comparable relative error of less than 10%.
Full article
(This article belongs to the Special Issue Industrial Process Operation State Sensing and Performance Optimization)
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Open AccessFeature PaperArticle
Hydrothermal Hydrolysis of Cocoa Bean Shell to Obtain Bioactive Compounds
by
Marta Sánchez, Tamara Bernal, Amanda Laca, Adriana Laca and Mario Díaz
Processes 2024, 12(5), 956; https://doi.org/10.3390/pr12050956 - 8 May 2024
Abstract
Cocoa bean shell (CBS), a by-product from the chocolate industry, is an interesting source of bioactive compounds. In this work, the effects of time and pH on the hydrothermal hydrolysis of CBS were evaluated with the aim of maximizing the extraction of antioxidant
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Cocoa bean shell (CBS), a by-product from the chocolate industry, is an interesting source of bioactive compounds. In this work, the effects of time and pH on the hydrothermal hydrolysis of CBS were evaluated with the aim of maximizing the extraction of antioxidant and functional compounds from this biomass. In general, all treatments tested led to improvements in the extraction of bioactive compounds compared to untreated samples. The maximum values for antioxidant activity (187 µmol TE/g CBS dw) and phenolic compounds (14.5 mg GAE/g CBS dw) were obtained when CBS was treated at pH 4 for 10 min. In addition, maximum amounts of flavonoids (10.1 mg CE/g CBS dw), tannins (6.5 mg CE/g CBS dw) and methylxanthines (9 mg/g CBS dw) were obtained under mild pH conditions (4–5). It is noteworthy that these values are higher than those reported in the literature for other vegetable substrates, highlighting the potential of CBS to be valorized as a source of different value-adding products.
Full article
(This article belongs to the Special Issue Technologies for Production, Processing, and Extractions of Nature Product Compounds, 2nd Volume)
Open AccessReview
Mass Transport and Energy Conversion of Magnetic Nanofluids from Nanoparticles’ Movement and Liquid Manipulation
by
Fei Xu, Yaowen Cao, Hanwen Gong, Juan Li, Ying Xu and Lei Shi
Processes 2024, 12(5), 955; https://doi.org/10.3390/pr12050955 - 8 May 2024
Abstract
Magnetic nanofluids, also referred to as ferromagnetic particle levitation systems, are materials with highly responsive magnetic properties. Due to their magnetic responsiveness, excellent controllability, favorable thermal characteristics, and versatility, magnetic nanofluids have sparked considerable interest in both industrial manufacturing and scientific research. Magnetic
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Magnetic nanofluids, also referred to as ferromagnetic particle levitation systems, are materials with highly responsive magnetic properties. Due to their magnetic responsiveness, excellent controllability, favorable thermal characteristics, and versatility, magnetic nanofluids have sparked considerable interest in both industrial manufacturing and scientific research. Magnetic nanofluids have been used and developed in diverse areas such as materials science, physics, chemistry and engineering due to their remarkable characteristics such as rapid magnetic reaction, elastic flow capacities, and tunable thermal and optical properties. This paper provides a full and in-depth introduction to the diverse uses of ferrofluids including material fabrication, fluid droplet manipulation, and biomedicine for the power and machinery sectors. As a result, magnetic nanofluids have shown promising applications and have provided innovative ideas for multidisciplinary research in biology, chemistry, physics and materials science. This paper also presents an overview of the device construction and the latest developments in magnetic-nanofluid-related equipment, as well as possible challenging issues and promising future scenarios.
Full article
(This article belongs to the Special Issue Magnetic Nanoparticles in Green Manufacturing for Sustainability)
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Open AccessArticle
Wind Shear Model Considering Atmospheric Stability to Improve Accuracy of Wind Resource Assessment
by
Hongpeng Liu, Guanjin Chen, Zejia Hua, Jingang Zhang and Qing Wang
Processes 2024, 12(5), 954; https://doi.org/10.3390/pr12050954 - 8 May 2024
Abstract
An accurate wind shear model is an important prerequisite in extrapolating the wind resource from lower heights to the increasing hub height of wind turbines. Based on the 1-year dataset (collected in 2014) consisting of 15-minute intervals collected at heights of 2, 10,
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An accurate wind shear model is an important prerequisite in extrapolating the wind resource from lower heights to the increasing hub height of wind turbines. Based on the 1-year dataset (collected in 2014) consisting of 15-minute intervals collected at heights of 2, 10, 50, 100, and 150 m on an anemometer tower in northern China, the present study focuses on the time-varying relationship between the wind shear coefficient (WSC) and atmospheric stability and proposes a wind shear model considering atmospheric stability. Through the relationship between Monin–Obukhov (M-O) length and gradient Richardson number, the M-O length is directly calculated by wind data, and the WSC is calculated by combining the Panofsky and Dutton (PD) models, which enhances the engineering practicability of the model. Then, the performance of the model is quantified and compared with two alternative methods: the use of annual average WSC and the use of stability change WSC extrapolation. The analysis demonstrates that the proposed model outperforms the other approaches in terms of normal root mean square error (NRMSE) and normal bias (NB). More specifically, this method reduces the NRMSE and NB by 24–29% and 76–95%, respectively. Meanwhile, it reaches the highest extrapolation accuracy under unstable and stable atmospheric conditions. The results are verified using the Weibull distribution.
Full article
(This article belongs to the Special Issue Wind Energy Assessment Based on CFD Simulations and Analytical Techniques)
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Open AccessEditorial
Progress of Optimization in Manufacturing Industries and Energy System
by
Dapeng Zhang, Qiangda Yang and Yuwen You
Processes 2024, 12(5), 953; https://doi.org/10.3390/pr12050953 - 8 May 2024
Abstract
The manufacturing and energy industry are typical complex large systems which cover a long cycle such as design [...]
Full article
(This article belongs to the Special Issue Design, Modeling, Optimization and Control in Manufacturing Industries and Energy System)
Open AccessArticle
Study and Application of Rock Drilling Resistance Characteristics in the Jiyang Depression Formation
by
Xiaoyong Ma, Wei Cheng and Liang Zhu
Processes 2024, 12(5), 952; https://doi.org/10.3390/pr12050952 - 8 May 2024
Abstract
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In response to the unclear drilling resistance characteristics of rocks in the Ji’yang Depression, low drilling efficiency of PDC drill bits, and difficulties in drill bit selection, this study selected rock samples from different depths in the area for indoor drilling resistance analysis
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In response to the unclear drilling resistance characteristics of rocks in the Ji’yang Depression, low drilling efficiency of PDC drill bits, and difficulties in drill bit selection, this study selected rock samples from different depths in the area for indoor drilling resistance analysis testing. Based on logging data, a prediction model was established for drilling resistance characteristics parameters of the strata in the area, and a graph of drilling resistance characteristic parameters of the rocks in the area was drawn. The study showed that the uniaxial compressive strength of the strata rocks was 50–110 MPa, with a hardness of 500–1300 MPa, a plasticity coefficient ranging from 1 to 2, a rock drillability grade of 8–20, and an abrasiveness index of 5–20. Combining the analysis of on-site drilling bit failures, PDC drill bits adapted to the strata in the area were selected, and the mechanical drilling speed of the selected bits reached 12.58 m/h, successfully drilling through the target layer. The above research results are of guiding significance for understanding the reasons for the difficulty of drilling into the Jiyang Depression strata and for improving mechanical drilling speed and drill bit selection in this area.
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Open AccessFeature PaperArticle
Ultrasonically Assisted Electrocoagulation Combined with Zeolite in Compost Wastewater Treatment
by
Sandra Svilović, Nediljka Vukojević Medvidović, Ladislav Vrsalović, Senka Gudić and Ana-Marija Mikulandra
Processes 2024, 12(5), 951; https://doi.org/10.3390/pr12050951 - 8 May 2024
Abstract
In this paper, the possibility of combining electrocoagulation (EC), ultrasound, and the addition of zeolite for wastewater treatment was investigated for the first time. The following combinations of hybrid processes were tested: electrocoagulation with zeolite (ECZ), simultaneous electrocoagulation with zeolite and ultrasound (ECZ+US),
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In this paper, the possibility of combining electrocoagulation (EC), ultrasound, and the addition of zeolite for wastewater treatment was investigated for the first time. The following combinations of hybrid processes were tested: electrocoagulation with zeolite (ECZ), simultaneous electrocoagulation with zeolite and ultrasound (ECZ+US), and two-stage electrocoagulation with zeolite and ultrasound (US+Z - EC), carried out with three different electrode materials. The results show that the simultaneous assistance of ultrasound in the ECZ leads to a lower increase in pH, while the temperature increase is higher. Regarding the COD, the assistance of ultrasound is only useful for Zn electrodes in the two-stage US+Z - EC, while the reduction in voltage consumption occurs for Fe and Al electrodes. Ultrasonic assistance caused more damage to the anodes, but anode consumption was reduced for Al and Zn electrodes. The total amount of zeolite that can be recovered is between 55–97%, and recovery is higher in systems with higher turbidity reduction. Good settling ability is only achieved with Al and Fe electrodes in simultaneous performance. Taguchi’s orthogonal L9 array design was applied to analyze the effects of electrode material, process type, mixing speed, and time duration on COD decrease, settling velocity, electrode, and voltage consumption. The results show that the use of ultrasound does not contribute to the desired result and generally only has a favorable effect on voltage and electrode consumption, while it has no positive effect on settling ability or COD decrease. Furthermore, although longer times and higher mixing speeds negatively impact cost due to voltage and electrode consumption, it is advisable not to choose the shortest duration and lowest speed to obtain adequate wastewater treatment quality.
Full article
(This article belongs to the Special Issue Treatment and Remediation of Organic and Inorganic Pollutants)
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Open AccessArticle
Research on Multi-Objective Process Parameter Optimization Method in Hard Turning Based on an Improved NSGA-II Algorithm
by
Zhengrui Zhang, Fei Wu and Aonan Wu
Processes 2024, 12(5), 950; https://doi.org/10.3390/pr12050950 - 7 May 2024
Abstract
To address the issue of local optima encountered during the multi-objective optimization process with the Non-dominated Sorting Genetic Algorithm II (NSGA-II) algorithm, this paper introduces an enhanced version of the NSGA-II. This improved NSGA-II incorporates polynomial and simulated binary crossover operators into the
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To address the issue of local optima encountered during the multi-objective optimization process with the Non-dominated Sorting Genetic Algorithm II (NSGA-II) algorithm, this paper introduces an enhanced version of the NSGA-II. This improved NSGA-II incorporates polynomial and simulated binary crossover operators into the genetic algorithm’s crossover phase to refine its performance. For evaluation purposes, the classic ZDT benchmark functions are employed. The findings reveal that the enhanced NSGA-II algorithm achieves higher convergence accuracy and surpasses the performance of the original NSGA-II algorithm. When applied to the machining of the high-hardness material 20MnCrTi, four algorithms were utilized: the improved NSGA-II, the conventional NSGA-II, NSGA-III, and MOEA/D. The experimental outcomes show that the improved NSGA-II algorithm delivers a more optimal combination of process parameters, effectively enhancing the workpiece’s surface roughness and material removal rate. This leads to a significant improvement in the machining quality of the workpiece surface, demonstrating the superiority of the improved algorithm in optimizing machining processes.
Full article
(This article belongs to the Section Manufacturing Processes and Systems)
Open AccessArticle
Catalytic Conversion of Oil Shale over Fe or Ni Catalysts under Sub-Critical Water
by
Chang Che, Junwen Wu, Zhibing Shen, Haolong Ning, Ruiyuan Tang, Shengrong Liang, Juntao Zhang, Haiyan Jiang and Shibao Yuan
Processes 2024, 12(5), 949; https://doi.org/10.3390/pr12050949 - 7 May 2024
Abstract
Sub-critical water is an environment-friendly solvent. It is widely used for the extraction of various organic compounds. It can be used to dissolve and transport organic matter in oil shale. In this study, the conversion of oil shale was synergistically catalyzed by the
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Sub-critical water is an environment-friendly solvent. It is widely used for the extraction of various organic compounds. It can be used to dissolve and transport organic matter in oil shale. In this study, the conversion of oil shale was synergistically catalyzed by the addition of Fe or Ni to the Fe inherent in samples under sub-critical water conditions. Oil shale can be converted to gas, oil and residues of oil. Thermogravimetric (TG) analysis results presented that the weight loss of raw oil shale was up to 15.85%. After sub-critical water extraction, the weight loss rate of the residues was reduced to 8.41%. With the application of a metal catalyst, Fe or Ni, the weight loss of residues was further reduced to 7.43% and 6.57%, respectively. According to DTG curves, it was found that there were two weight-loss rate peaks. The decomposition process of kerogen in oil shale could be divided into two cracking processes. One is decomposed at a high velocity at around 420 °C, and another is decomposed at a low velocity at around 515 °C. Gas chromatography (GC) results of gas products indicated that Fe or Ni could contribute to producing normal alkanes, such as methane, ethane, propane, etc., which are produced by the hydrogenation of alkenes via hydrogen transfer during the conversion process of kerogen. Gas chromatography-mass spectrometry (GC–MS) was conducted to analyze the components of the liquid products. The results showed that n-alkanes, iso-alkane, oxygenated hydrocarbons and aromatic compounds were the major components of the kerogen cracking products. When Ni was introduced as a catalyst, the contents of aromatic compounds and oxygenated hydrocarbons in the liquid products were increased from 19.55% and 6.87% to 22.38% and 13.77%, respectively. This is due to the synergistic effect of the addition of Ni with the inherent Fe in oil shale under sub-critical water which ensures kerogen is more easily cracked to produce aromatic compounds and oxygenated hydrocarbons.
Full article
(This article belongs to the Special Issue Process Technologies for Heavy Oils and Residua Upgradings)
Open AccessArticle
Texture and Twinning Evolution of Cold-Rolled Industrial Pure Zirconium
by
Yuan Liu, Yiming Li, Weimin Mao, Huiyi Bai, Qi Fang, Yunping Ji and Huiping Ren
Processes 2024, 12(5), 948; https://doi.org/10.3390/pr12050948 - 7 May 2024
Abstract
Industrial pure zirconium plays an essential role as a structural material in the nuclear energy sector. Understanding the deformation mechanisms is crucial for effectively managing the plasticity and texture evolution of industrial pure zirconium. In the present study, the texture and microstructure evolution
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Industrial pure zirconium plays an essential role as a structural material in the nuclear energy sector. Understanding the deformation mechanisms is crucial for effectively managing the plasticity and texture evolution of industrial pure zirconium. In the present study, the texture and microstructure evolution of industrial pure zirconium during the cold-rolling process have been characterized by XRD, EBSD, and TEM. The influences of various twins on texture evolution have also been simulated by the reaction stress model. The effects of slip and twinning on the deformation behavior and texture evolution have been discussed based on crystallographic and experimental considerations. Cold rolling yields a typical bimodal texture, resulting in the preferential <2110>//RD orientation. The activation of the deformation mechanisms during cold rolling follows the sequential trend of slip, twinning, local slip. Experimental characterization and reaction stress simulation illustrate that T1 twins dominate in the early stage, whereas C2 twins develop at the later stage of the cold-rolling process. Twinning, especially the T1 twin, contributes to the formation of the {0001}<1010> orientation.
Full article
(This article belongs to the Special Issue Digital Research and Development of Materials and Processes)
Open AccessFeature PaperArticle
Novel Ferrocene-Containing Triacyl Derivative of Resveratrol Protects Ovarian Cells from Toxicity Caused by Ortho-Substituted Polychlorinated Biphenyls
by
Ivana Kmetič, Teuta Murati, Veronika Kovač, Lidija Barišić, Nina Bilandžić, Branimir Šimić and Marina Miletić
Processes 2024, 12(5), 947; https://doi.org/10.3390/pr12050947 - 7 May 2024
Abstract
Polychlorinated biphenyls (PCBs) can induce neurotoxicity, immunotoxicity, reproductive toxicity, genotoxicity, and carcinogenicity (IARC group 1 Carcinogens). Scientific data suggest that resveratrol possesses the ability to attenuate ortho-PCB-induced toxicity. Recently, a novel ferrocene-containing triacyl derivative of resveratrol (RF) was synthesized and in this
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Polychlorinated biphenyls (PCBs) can induce neurotoxicity, immunotoxicity, reproductive toxicity, genotoxicity, and carcinogenicity (IARC group 1 Carcinogens). Scientific data suggest that resveratrol possesses the ability to attenuate ortho-PCB-induced toxicity. Recently, a novel ferrocene-containing triacyl derivative of resveratrol (RF) was synthesized and in this study, its potential to protect CHO-K1 cells from selected PCB congeners (75 µM) was evaluated. Cell viability/proliferation was observed by Trypan Blue (TB), Neutral Red (NR), Kenacid Blue (KB), and MTT bioassays, ROS formation by fluorescent probes, and the extent of apoptosis by flow cytometry. All applied bioassays confirmed that RF (2.5–100 μM) remarkably improves viability in PCB 153-treated cells with an increase in cell survival almost up to control levels. This effect was not determined after PCB 77 exposure, although ROS formation was decreased at RF ≥ 50 µM. Apoptosis was significant (p < 0.05) for both congeners. In PCB 77-treated cells, RF did not suppress the induction of cell death. The intended protective effect of RF was evident when cells were treated with PCB 153, and this correlates with results obtained for cell viability. Compared to resveratrol, the novel RF showed promising results in terms of improved biological activity and cell protection against PCB 153 toxicity at all concentrations tested.
Full article
(This article belongs to the Special Issue Valorization of Medicinal and Aromatic Plants in Biotechnological Applications)
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Open AccessArticle
Investment Strategy and Benefit Analysis of Power and Heat Hybrid Energy Storage in Industrial Parks Based on Energy Performance Contracting
by
Feng Xiao and Yali Wang
Processes 2024, 12(5), 946; https://doi.org/10.3390/pr12050946 - 7 May 2024
Abstract
To solve the problems of a single mode of energy supply and high energy cost in the park, the investment strategy of power and heat hybrid energy storage in the park based on contract energy management is proposed. Firstly, the concept of energy
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To solve the problems of a single mode of energy supply and high energy cost in the park, the investment strategy of power and heat hybrid energy storage in the park based on contract energy management is proposed. Firstly, the concept of energy performance contracting (EPC) and the advantages and disadvantages of its main modes are analyzed, and the basic scheme of EPC for parks is proposed combined with the actual demand. Furthermore, the multiple energy storage model for power and heat storage in parks is established, which includes lithium batteries and heat storage tanks. Based on this, minimizing the annual operation cost of parks is taken as the optimization goal, and the capacity optimization model for power and heat storage is constructed, which considers the investment costs, operation and maintenance costs, purchased energy costs, peak-shaving subsidy, and environmental subsidy. Finally, an industrial park is selected as an example of EPC to verify the effectiveness of our proposed investment strategy. The results show that compared with the situation before the energy-saving renovation, the park can save 35.14 ten thousand CNY in annual cost expenses. When the unit power price of the lithium battery exceeds 3900 CNY/kW, the unit capacity price exceeds 5460 CNY/kWh, the unit power price of the heat storage tank (HST) exceeds 6000 CNY/kW, and the unit capacity price exceeds 1000 CNY/kWh, the configuration of the lithium battery and HST in the park is no longer the optimal choice to perform the energy-saving renovation.
Full article
(This article belongs to the Section Energy Systems)
Open AccessArticle
Preparation and Application of CO2-Resistant Latex in Shale Reservoir Cementing
by
Chunyuan Jiang, Xuecheng Zheng, Yuanqiang Zhu, Lei Tang, Yuhao Liu, Zhijun Zhao and Hongyu Zhang
Processes 2024, 12(5), 945; https://doi.org/10.3390/pr12050945 - 7 May 2024
Abstract
With the application of CO2 fracturing, CO2 huff and puff, CO2 flooding, and other stimulation technologies in shale reservoirs, a large amount of CO2 remained in the formation, which also lead to the serious corrosion problem of CO2
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With the application of CO2 fracturing, CO2 huff and puff, CO2 flooding, and other stimulation technologies in shale reservoirs, a large amount of CO2 remained in the formation, which also lead to the serious corrosion problem of CO2 in shale reservoirs. In order to solve the harm caused by CO2 corrosion, it is necessary to curb CO2 corrosion from the cementing cement ring to ensure the long-term stable exploitation of shale oil. Therefore, a new latex was created using liquid polybutadiene, styrene, 2-acrylamide-2-methylpropanesulfonic acid, and maleic anhydride to increase the cement ring’s resistance to CO2 corrosion. The latex’s structure and characteristics were then confirmed using infrared, particle size analyzer, thermogravimetric analysis, and transmission electron microscopy. The major size distribution of latex is between 160 and 220 nm, with a solid content of 32.2% and an apparent viscosity of 36.8 mPa·s. And it had good physical properties and stability. Latex can effectively improve the properties of cement slurry and cement composite. When the amount of latex was 8%, the fluidity index of cement slurry was 0.76, the consistency index was 0.5363, the free liquid content was only 0.1%, and the water loss was reduced to 108 mL. At the same time, latex has a certain retarding ability. With 8% latex, the cement slurry has a specific retarding ability, is 0.76 and 0.5363, has a free liquid content of just 0.1%, and reduces water loss to 108 mL. Moreover, latex had certain retarding properties. The compressive strength and flexural strength of the latex cement composite were increased by 13.47% and 33.64% compared with the blank cement composite. A long-term CO2 corrosion experiment also showed that latex significantly increased the cement composite’s resilience to corrosion, lowering the blank cement composite’s growth rate of permeability from 46.88% to 19.41% and its compressive strength drop rate from 27.39% to 11.74%. Through the use of XRD and SEM, the latex’s anti-corrosion mechanism, hydration products, and microstructure were examined. In addition to forming a continuous network structure with the hydrated calcium silicate and other gels, the latex can form a latex film to attach and fill the hydration products. This slows down the rate of CO2 corrosion of the hydration products, enhancing the cement composite’s resistance to corrosion. CO2-resistant toughened latex can effectively solve the CO2 corrosion problem of the cementing cement ring in shale reservoirs.
Full article
(This article belongs to the Special Issue Advances in Technology for Enhancing Oil and Gas Recovery in Shale Reservoirs)
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Open AccessArticle
Biomimetic Approach for Enhanced Mechanical Properties and Stability of Self-Mineralized Calcium Phosphate Dibasic–Sodium Alginate–Gelatine Hydrogel as Bone Replacement and Structural Building Material
by
Alberto T. Estevez and Yomna K. Abdallah
Processes 2024, 12(5), 944; https://doi.org/10.3390/pr12050944 - 7 May 2024
Abstract
Mineralized materials are gaining increased interest recently in a number of fields, especially in bone tissue engineering as bone replacement materials as well as in the architecture-built environment as structural building materials. Until the moment, there has not been a unified sustainable approach
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Mineralized materials are gaining increased interest recently in a number of fields, especially in bone tissue engineering as bone replacement materials as well as in the architecture-built environment as structural building materials. Until the moment, there has not been a unified sustainable approach that addresses this multi-scale application objective by developing a self-mineralized material with minimum consumption of materials and processes. Thus, in the current study, a hydrogel developed from sodium alginate, gelatine, and calcium phosphate dibasic (CPDB) was optimized in terms of rheological properties and mineralization capacity through the formation of hydroxyapatite crystals. The hydrogel composition process adopted a three-stage, thermally induced chemical cross-linking to achieve a stable and enhanced hydrogel. The 6% CPDB-modified SA–gelatine hydrogel achieved the best rheological properties in terms of elasticity and hardness. Different concentrations of epigallocatechin gallate were tested as well as a rheological enhancer to optimize the hydrogel and to boost its anti-microbial properties. However, the results from the addition of EPGCG were not considered significant; thus, the 6% CPDB-modified SA–gelatine hydrogel was further tested for mineralization by incubation in various media, without and with cells, for 7 and 14 days, respectively, using scanning electron microscopy. The results revealed significantly enhanced mineralization of the hydrogel by forming hydroxyapatite platelets of the air-incubated hydrogel (without cells) in non-sterile conditions, exhibiting antimicrobial properties as well. Similarly, the air-incubated bioink with osteosarcoma SaOs-2 cells exhibited dense mineralized topology with hydroxyapatite crystals in the form of faceted spheres. Finally, the FBS-incubated hydrogel and FBS-incubated bioink, incubated for 7 and 14 days, respectively, exhibited less densely mineralized topology and less distribution of the hydroxyapatite crystals. The degradation rate of the hydrogel and bioink incubated in FBS after 14 days was determined by the increase in dimensions of the 3D-printed samples, which was between 5 to 20%, with increase in the bioink samples dimensions in comparison to their dimensions post cross-linking. Meanwhile, after 14 days, the hydrogel and bioink samples incubated in air exhibited shrinkage: a 2% decrease in the dimensions of the 3D-printed samples in comparison to their dimensions post cross-linking. The results prove the capacity of the developed hydrogel in achieving mineralized material with anti-microbial properties and a slow-to-moderate degradation rate for application in bone tissue engineering as well as in the built environment as a structural material using a sustainable approach.
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(This article belongs to the Special Issue Innovations in Manufacturing Processes and Systems for Sustainable Practices)
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Open AccessArticle
Study on the Effect of Thermal Assisted Combined Plant-Based Biomass Conditioning on Dehydrated Sludge Bio-Drying
by
He Li, Yujie Luo, Chang Jiang, Yizhuo Wang and Lu Xiang
Processes 2024, 12(5), 943; https://doi.org/10.3390/pr12050943 - 7 May 2024
Abstract
In recent years, the production of municipal sludge has gradually increased, and finding suitable sludge treatment and disposal technologies is an urgent problem that needs to be solved. Bio-drying of sludge is a relatively efficient and convenient drying method, but currently, there are
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In recent years, the production of municipal sludge has gradually increased, and finding suitable sludge treatment and disposal technologies is an urgent problem that needs to be solved. Bio-drying of sludge is a relatively efficient and convenient drying method, but currently, there are still problems with unstable drying effects and high moisture content of dried products, which limits the subsequent utilization of bio-drying products. This article uses a thermal assisted bio-drying device that simulates carbonization waste heat reflux, and uses corncob, straw, sawdust, and rice husk as conditioners to carry out bio-drying of dehydrated sludge. The influence of the types and ratios of conditioner under thermal assistance on the bio-drying of dehydrated sludge is explored. The results showed that the moisture removal efficiency of the corncob and straw groups was better, and their material moisture content could be reduced to below 10% within 24 h. The lower calorific value of straw-sludge drying products was the highest, at 11,608.8 kJ/kg. The best conditioner under the conditions of this experiment was straw, and the drying effect was best when the mass ratio of dehydrated sludge to straw was 4:1. The research results contribute to promoting the development of sludge bio-drying technology.
Full article
(This article belongs to the Special Issue Agricultural and Industrial Waste Recovery Technology and Process Optimization)
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Open AccessReview
Recent Advances in Drying Processing Technologies for Aquatic Products
by
Weibin Wu, Haoxin Li, Yingmei Chen, Yuanqiang Luo, Jinbin Zeng, Jingkai Huang and Ting Gao
Processes 2024, 12(5), 942; https://doi.org/10.3390/pr12050942 - 6 May 2024
Abstract
Fresh aquatic products, due to their high water activity, are susceptible to microbial contamination and spoilage, resulting in a short shelf life. Drying is a commonly used method to extend the shelf life of these products by reducing the moisture content, inhibiting microbial
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Fresh aquatic products, due to their high water activity, are susceptible to microbial contamination and spoilage, resulting in a short shelf life. Drying is a commonly used method to extend the shelf life of these products by reducing the moisture content, inhibiting microbial growth, and slowing down enzymatic and chemical reactions. However, the drying process of aquatic products involves chemical reactions such as oxidation and hydrolysis, which pose challenges in obtaining high-quality dried products. This paper provides a comprehensive review of drying processing techniques for aquatic products, including drying preprocessing, drying technologies, and non-destructive monitoring techniques, and discusses their advantages and challenges. Furthermore, the impact of the drying process on the quality attributes of dried products, including sensory quality, nutritional components, and microbial aspects, is analyzed. Finally, the challenges faced by drying processing techniques for aquatic products are identified, and future research prospects are outlined, aiming to further advance research and innovation in this field.
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(This article belongs to the Special Issue Advanced Drying Technologies in Food Processing)
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Open AccessArticle
Characteristics of Deformation and Stability of Ultra-Deep Pit in Plateau Alluvial–Lacustrine Gravel Strata
by
Yanhui Guo and Shaoqian Liu
Processes 2024, 12(5), 941; https://doi.org/10.3390/pr12050941 - 6 May 2024
Abstract
Deformation of ultra-deep pit walls and surrounding geotechnical bodies due to engineering disturbances typically shows intricate spatiotemporal patterns. In this study, deformations at critical steps of the construction process were first numerically simulated by Midas GTS NX, and this was followed by lab-scale
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Deformation of ultra-deep pit walls and surrounding geotechnical bodies due to engineering disturbances typically shows intricate spatiotemporal patterns. In this study, deformations at critical steps of the construction process were first numerically simulated by Midas GTS NX, and this was followed by lab-scale geophysical model tests of the entire process of the pit construction. Data on deformation obtained from numerical simulations and lab-scale geophysical model tests were compared with those obtained from a dynamic monitoring scheme in the field to analyze the characteristics of the deformation and evolution of the pit wall. This was used to derive a generally applicable theoretical expression to predict variations in the horizontal displacements.
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(This article belongs to the Special Issue Intelligent Computational Modeling and Processes Optimization Techniques in Geo-Engineering)
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The Recovery of Sulfuric Acid in the Presence of Zr(IV) and Hf(IV) by Solvent Extraction with TEHA and Its Mixtures
by
Xiaoxi Ding, Jiaxin Jiang, Yafang Zhao, Zaichao Dong, Lingyun Wang and Yang Liu
Processes 2024, 12(5), 940; https://doi.org/10.3390/pr12050940 - 6 May 2024
Abstract
The recovery of sulfuric acid in the presence of Zr(IV) and Hf(IV) was studied via solvent extraction using TEHA (tri-2-ethylhexyl amine) and its mixtures. A solidification phenomenon occurred in the loaded organic phase when a single TEHA was employed in the extraction of
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The recovery of sulfuric acid in the presence of Zr(IV) and Hf(IV) was studied via solvent extraction using TEHA (tri-2-ethylhexyl amine) and its mixtures. A solidification phenomenon occurred in the loaded organic phase when a single TEHA was employed in the extraction of 1 to 5 M H2SO4. Octanol, decanol and TBP (tri butyl phosphate) were mixed with TEHA, separately, to prevent the solidification of sulfuric-acid-loaded organic. Due to the relatively high aqueous solubility of octanol and decanol, the mixture of TEHA + TBP was selected as the optimal system for the extraction of H2SO4. Simulated counter-current extraction and stripping experiments were performed on the basis of the McCabe–Thiele diagrams, indicating that sulfuric acid could be reduced by TEHA + TBP from 4.2 to around 0.5 M without Zr(IV) and Hf(IV) extraction and recovered by its complete stripping with water. The proposed sulfuric acid recovery step would contribute to the completion of the closed-circuit of the Zr(IV) and Hf(IV) separation process in our previous work and help to re-separate the remaining Zr(IV) and Hf(IV) in the sulfuric acid stripping solution.
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(This article belongs to the Special Issue Recent Advances in Processing Technologies for Substance Extraction, Separation, and Enrichment)
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A Study of the Feasibility of Pinus patula Biochar: The Regeneration of the Indigo Carmine-Loaded Biochar and Its Efficiency for Real Textile Wastewater Treatment
by
Carolina Gallego-Ramírez, Edwin Chica and Ainhoa Rubio-Clemente
Processes 2024, 12(5), 939; https://doi.org/10.3390/pr12050939 - 5 May 2024
Abstract
The feasibility of an adsorbent material like biochar (BC) depends on its regeneration capacity and its ability to achieve high removal efficiencies on real wastewater (WW) effluents. In this study, the regeneration capacity of the Pinus patula BC previously used in the removal
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The feasibility of an adsorbent material like biochar (BC) depends on its regeneration capacity and its ability to achieve high removal efficiencies on real wastewater (WW) effluents. In this study, the regeneration capacity of the Pinus patula BC previously used in the removal of Indigo Carmine from water was evaluated. The regeneration technique that resulted in the highest desorption efficiency was a thermo-chemical method that consisted of heating the spent BC in a stove at 160 °C for 45 min followed by regeneration with ethanol (C2H6O) at a concentration of 75% for 6 h. Through this regeneration method, it was found that Pinus patula BC could be used in seven consecutive adsorption–desorption cycles. The feasibility of this BC was also assessed by evaluating the adsorbent’s efficiency in real textile WW. Under optimal operational conditions (solution pH = 3, BC dose = 13.5 g/L, and BC particle size = 300–450 µm), the highest removal efficiencies in terms of colour and dissolved organic carbon (DOC) were 81.3 and 76.8%, respectively, for 120 min of treatment. The results obtained in the regeneration studies and the treatment of real textile WW suggested that the use of Pinus patula BC could be suitable to be scaled to an industrial level, contributing to sustainable development and the circular bioeconomy by using a waste to solve the dye pollution problem of another waste.
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(This article belongs to the Special Issue A Themed Issue in Honor of Professor Vicente Gómez Serrano: Innovation in Production, Characterization and Applications of Activated Carbon, Biochar and Other Carbon-Based Materials)
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Effects of the Nozzle Configuration with and without an Internal Guide Vane on the Efficiency in Cross-Flow Small Hydro Turbines
by
Fredys Romero-Menco, Juan Pineda-Aguirre, Laura Velásquez, Ainhoa Rubio-Clemente and Edwin Chica
Processes 2024, 12(5), 938; https://doi.org/10.3390/pr12050938 - 5 May 2024
Abstract
In this work, an experimental analysis of the performance of a cross-flow turbine, commonly referred to as a Michell–Banki turbine (MBT), is carried out for small-scale hydropower production in rural areas located in developing countries to support their social and economic development activities.
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In this work, an experimental analysis of the performance of a cross-flow turbine, commonly referred to as a Michell–Banki turbine (MBT), is carried out for small-scale hydropower production in rural areas located in developing countries to support their social and economic development activities. The study investigates how the efficiency of the MBT is influenced by the presence or absence of a nozzle, along with variations in the internal guide vane (GV) and its angle. The runner had 26 blades that were arranged symmetrically in the periphery between two circular plates. The designed MBT had the ability to generate a maximum of 100 W of power at a water flow rate and a head of 0.009 m3/s and 0.6311 m, respectively. The experimental tests were carried out using a hydraulic bench. The turbine efficiency without the inner GV was found to be higher than that of the turbine with the inner GV; i.e., it was found that the utilization of the GV did not enhance the efficiency of the MBT due to the occurrence of a choking effect. A maximum hydraulic efficiency of 85% was achieved in the turbine without an inner GV in comparison with the efficiency achieved (77%) with this device and an optimum opening angle of the GV of 24° (75% of opening). In this regard, the GV design should be carefully carried out to improve the MBT efficiency. Additionally, the effect of the GV shape on the MBT performance should be experimentally investigated to obtain a more general judgment regarding the role of this device.
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(This article belongs to the Special Issue Process and Modelling of Renewable and Sustainable Energy Sources)
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