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Molbank, Volume 2010, Issue 2 (June 2010)

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Open AccessShort Note 7-(3-Chlorophenylamino)-1-cyclopropyl-6-fluoro-8-nitro-4-oxo-1,4-dihydroquinoline-3-carboxylic Acid
Molbank 2010, 2010(2), M669; doi:10.3390/M669
Received: 8 March 2010 / Accepted: 22 March 2010 / Published: 24 March 2010
PDF Full-text (117 KB) | Supplementary Files
Abstract 7-(3-Chlorophenylamino)-1-cyclopropyl-6-fluoro-8-nitro-4-oxo-1,4-dihydro-quinoline-3-carboxylic acid (2) was prepared and fully characterized by NMR, IR, and MS. Compound 2 exhibited good antibacterial activity against gram-positive standard and resistant strains. Full article
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Open AccessShort Note 2-Methyl-7-(phenylsulfanylmethyl)naphthalene
Molbank 2010, 2010(2), M670; doi:10.3390/M670
Received: 16 March 2010 / Accepted: 24 March 2010 / Published: 30 March 2010
PDF Full-text (89 KB) | Supplementary Files
Abstract A new sulfide, 2-methyl-7-(phenylsulfanylmethyl)naphthalene was synthesized and its MS, IR, 1H NMR, 13C NMR and DEPT-135 data are reported. Full article
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Open AccessShort Note 6,7,8,10-Tetra-O-benzyl-1,2,3,4-tetradeoxy-α-D-gluco-dec-5-ulopyranosyl 2,3,4,6-Tetra-O-benzyl-α-D-glucopyranoside
Molbank 2010, 2010(2), M671; doi:10.3390/M671
Received: 17 March 2010 / Accepted: 1 April 2010 / Published: 7 April 2010
PDF Full-text (206 KB) | Supplementary Files
Abstract The title compound 1 was synthesized by the coupling reaction of 6,7,8,10-tetra-O-benzyl-1,2,3,4-tetradeoxy-α-D-gluco-dec-5-ulopyranose (2) with 2,3,4,6-tetra-O-benzyl-D-glucopyranose (3) in the presence of 5 mol% bismuth(III) triflate in dichloromethane at 0 °C. Full article
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Open AccessShort Note Ethyl 3,5-Dimethyl-4-[(4-phenyl-1,3-thiazol-2-yl)carbamoyl]-1H-pyrrole-2-carboxylate
Molbank 2010, 2010(2), M672; doi:10.3390/M672
Received: 19 March 2010 / Accepted: 31 March 2010 / Published: 7 April 2010
PDF Full-text (192 KB) | Supplementary Files
Abstract A new compound, ethyl 3,5-dimethyl-4-[(4-phenyl-1,3-thiazol-2-yl)carbamoyl]-1H-pyrrole-2-carboxylate (3) was synthesized by the amination method. The synthesized compound (3) was characterized by IR, 1H-NMR, 13C-NMR, mass spectral data and elemental analysis. Full article
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Open AccessShort Note 3-Hydroxy-4-{[(4-fluorophenyl)imino]methyl}phenyl Octadecanoate
Molbank 2010, 2010(2), M673; doi:10.3390/M673
Received: 25 March 2010 / Accepted: 8 April 2010 / Published: 9 April 2010
PDF Full-text (243 KB) | Supplementary Files
Abstract A new Schiff base ester, 3-hydroxy-4-{[(4-fluorophenyl)imino]methyl}phenyl octadecanoate, was synthesized and its IR, 1H NMR, 13C NMR and MS spectroscopic data are presented. Full article
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Open AccessShort Note 3-Hydroxy-4-{[(4-chlorophenyl)imino]methyl}phenyl Octadecanoate
Molbank 2010, 2010(2), M674; doi:10.3390/M674
Received: 25 March 2010 / Accepted: 8 April 2010 / Published: 9 April 2010
PDF Full-text (319 KB) | Supplementary Files
Abstract A new Schiff base ester, 3-hydroxy-4-{[(4-chlorophenyl)imino]methyl}phenyl octadecanoate, was synthesized and its IR, 1H NMR, 13C NMR and MS spectroscopic data are presented. Full article
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Open AccessShort Note 3-Hydroxy-4-{[(4-bromophenyl)imino]methyl}phenyl Octadecanoate
Molbank 2010, 2010(2), M675; doi:10.3390/M675
Received: 25 March 2010 / Accepted: 8 April 2010 / Published: 9 April 2010
PDF Full-text (290 KB) | Supplementary Files
Abstract A new Schiff base ester, 3-hydroxy-4-{[(4-bromophenyl)imino]methyl}phenyl octadecanoate, was synthesized and its IR, 1H NMR, 13C NMR and MS spectroscopic data are presented. Full article
Open AccessShort Note (E)-2-((4R,5R)-5-((Benzyloxy)methyl)-2,2-dimethyl-1,3-dioxolan-4-yl)but-2-ene-1,4-diol
Molbank 2010, 2010(2), M676; doi:10.3390/M676
Received: 11 March 2010 / Accepted: 14 April 2010 / Published: 19 April 2010
PDF Full-text (373 KB) | Supplementary Files
Abstract The synthesis of (E)-2-((4R,5R)-5-((benzyloxy)methyl)-2,2-dimethyl-1,3-dioxolan-4-yl)but-2-ene-1,4-diol by a one-step reduction of the appropriate 2-substituted butenolide is reported. Product characterization was carried out by IR, 1H NMR, 13C NMR, MS, elemental analysis and optical rotation. Full article
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Open AccessShort Note Tris{4-[(1,3-diphenyl-1H-pyrazol-4-yl)methylene]-41-aminobiphenyl}amine
Molbank 2010, 2010(2), M677; doi:10.3390/M677
Received: 25 February 2010 / Accepted: 31 March 2010 / Published: 20 April 2010
PDF Full-text (136 KB) | Supplementary Files
Abstract Tris{4-[(1,3-diphenyl-1H-pyrazol-4-yl)methylene]-41-aminobiphenyl}amine was synthesized from N-(4-bromophenyl)-N-[(1,3-diphenyl-1H-pyrazol-4-yl)methylene]amine and tris(4-bromophenyl)amine based on Ullmann coupling reaction. The synthesized compound was characterized by NMR, IR, MS and elemental analysis. Full article
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Open AccessShort Note 1-Phenylpyrazolo[4',3':5,6]pyrano[3,2-c]pyridine-4(1H)-thione
Molbank 2010, 2010(2), M678; doi:10.3390/M678
Received: 29 March 2010 / Accepted: 23 April 2010 / Published: 26 April 2010
PDF Full-text (328 KB) | Supplementary Files
Abstract The title compound is prepared by treatment of 1-phenylpyrazolo[4',3':5,6]pyrano[3,2-c]pyridin-4(1H)-one with Lawesson’s reagent in refluxing toluene. Detailed spectroscopic data (1H NMR, 13C NMR, 15N NMR, MS) are presented. Full article
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Open AccessShort Note (2E)-3-(3,5-Dimethyl-1-phenyl-1H-pyrazol-4-yl)-1-(2,5-dimethyl-3-thienyl)prop-2-en-1-one
Molbank 2010, 2010(2), M679; doi:10.3390/M679
Received: 30 March 2010 / Accepted: 22 April 2010 / Published: 27 April 2010
PDF Full-text (90 KB) | Supplementary Files
Abstract The title compound, (2E)-3-(3,5-dimethyl-1-phenyl-1H-pyrazol-4-yl)-1-(2,5-dimethyl-3-thienyl)prop-2-en-1-one (3) was synthesized in high yield by aldol condensation of 3-acetyl-2,5-dimethylthiophene and 3,5-dimethyl-1-phenylpyrazole-4-carboxaldehyde in ethanolic NaOH at room temperature. Its structure was fully characterized by elemental analysis, IR, 1H NMR, 13C NMR and EI-MS spectral analysis. Full article
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Open AccessShort Note (–)-5-[(4R,5R)-5-(Benzyloxymethyl)-2,2-dimethyl-1,3-dioxolan-4-yl]-2,2-dimethyl-4,7-dihydro-1,3-dioxepine
Molbank 2010, 2010(2), M680; doi:10.3390/M680
Received: 11 March 2010 / Accepted: 30 April 2010 / Published: 30 April 2010
PDF Full-text (170 KB) | Supplementary Files
Abstract The synthesis of(–)-5-[(4R,5R)-5-(benzyloxymethyl)-2,2-dimethyl-1,3-dioxolan-4-yl]-2,2-dimethyl-4,7-dihydro-1,3-dioxepine is reported. Product characterization was carried out by IR, 1H NMR, 13C NMR, MS, elemental analysis and optical rotation. Full article
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Open AccessShort Note 3-Hydroxy-4-{[(4-ethylphenyl)imino]methyl}phenyl Octadecanoate
Molbank 2010, 2010(2), M681; doi:10.3390/M681
Received: 29 March 2010 / Accepted: 30 April 2010 / Published: 30 April 2010
PDF Full-text (98 KB) | Supplementary Files
Abstract A new Schiff base ester, 3-hydroxy-4-{[(4-ethylphenyl)imino]methyl}phenyl octadecanoate, was synthesized and its IR, 1H NMR, 13C NMR and MS spectroscopic data are presented. Full article
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Open AccessShort Note N-[(2,5-Dimethyl-3-oxo-1-phenyl-2,3-dihydro-1H-pyrazol-4-yl)carbamothioyl]isonicotinamide
Molbank 2010, 2010(2), M682; doi:10.3390/M682
Received: 8 February 2010 / Accepted: 8 April 2010 / Published: 11 May 2010
PDF Full-text (161 KB) | Supplementary Files
Abstract A new heterocyclic compound, N-[(2,5-dimethyl-3-oxo-1-phenyl-2,3-dihydro-1H-pyrazol-4-yl)carbamothioyl]isonicotinamide, was synthesized from isonicotinoyl isothiocyanate and 4-aminoantipyrine in acetonitrile solution. The title compound was characterized by FT-IR, 1H NMR, 13C NMR and MS spectroscopic methods. Physical parameters of the compound were examinated. Full article
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Open AccessShort Note 2,2'-(2,2'-Oxybis(ethane-2,1-diyl)bis(oxy))bis(N-(2,2'-bithiophen-5-ylmethylene)aniline)
Molbank 2010, 2010(2), M683; doi:10.3390/M683
Received: 8 April 2010 / Accepted: 10 May 2010 / Published: 11 May 2010
Cited by 1 | PDF Full-text (183 KB) | Supplementary Files
Abstract
A new flexible fluorescent compound L derived from 1,5-bis(2-aminophenoxy)-3-oxapentane (A) has been synthesized by classical Schiff-base reaction between (A) and 2,2´-bithiophene carbaldehyde (B). The same synthesis was reproduced by a green methodology using an ultrasonication reaction in
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A new flexible fluorescent compound L derived from 1,5-bis(2-aminophenoxy)-3-oxapentane (A) has been synthesized by classical Schiff-base reaction between (A) and 2,2´-bithiophene carbaldehyde (B). The same synthesis was reproduced by a green methodology using an ultrasonication reaction in a classical sonication bath. The structure of the new compound was confirmed by elemental analysis, IR, 1H-NMR, MALDI-TOF-MS and EI-MS-spectra, UV-vis and fluorescence emission spectroscopy. Full article
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Open AccessShort Note N-[(9-Ethyl-9H-carbazol-3-yl)methylene]-3,4-dimethylisoxazol-5-amine
Molbank 2010, 2010(2), M684; doi:10.3390/M684
Received: 14 April 2010 / Accepted: 20 May 2010 / Published: 25 May 2010
PDF Full-text (86 KB) | Supplementary Files
Abstract The title compound, N-[(9-ethyl-9H-carbazol-3-yl)methylene]-3,4-dimethylisoxazol-5-amine has been synthesized by reaction of 9-ethyl-9H-carbazole-3-carbaldehyde with 5-amino-3,4-dimethylisoxazole in the presence of acetic acid in ethanol. The structure of this new compound was confirmed by elemental analysis, IR, 1H-NMR, 13C-NMR and EI-MS spectral analysis. Full article
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Open AccessShort Note 9-Methyl-3,5-dioxo-4-azatricyclo[5.2.2.02,6]undec-8-ene-1,8-diyl Diacetate
Molbank 2010, 2010(2), M685; doi:10.3390/M685
Received: 5 May 2010 / Accepted: 20 May 2010 / Published: 25 May 2010
PDF Full-text (191 KB) | Supplementary Files
Abstract 9-Methyl-3,5-dioxo-4-azatricyclo[5.2.2.02,6]undec-8-ene-1,8-diyl diacetatewas synthesized from 2-methylcyclohexane-1,3-dione and 1H-pyrrole-2,5-dione. The title compound was characterized by 1H NMR, 13C NMR, elemental analysis and MS. Full article
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Open AccessShort Note 3-Hydroxy-4-{[(4-methoxyphenyl)imino]methyl}phenyl Octadecanoate
Molbank 2010, 2010(2), M686; doi:10.3390/M686
Received: 2 April 2010 / Accepted: 4 June 2010 / Published: 8 June 2010
PDF Full-text (149 KB) | Supplementary Files
Abstract A new Schiff base ester, 3-hydroxy-4-{[(4-methoxyphenyl)imino]methyl}phenyl octadecanoate, was synthesized and its IR, 1H NMR, 13C NMR and MS spectroscopic data are presented. Full article
Figures

Open AccessShort Note (2E)-3-(3,5-Dimethyl-1-phenyl-1H-pyrazol-4-yl)-1-(2,5-dimethyl-3-furanyl)prop-2-en-1-one
Molbank 2010, 2010(2), M687; doi:10.3390/M687
Received: 8 May 2010 / Accepted: 27 May 2010 / Published: 8 June 2010
Cited by 1 | PDF Full-text (85 KB) | Supplementary Files
Abstract The title compound, (2E)-3-(3,5-dimethyl-1-phenyl-1H-pyrazol-4-yl)-1-(2,5-dimethyl-3-furanyl)prop-2-en-1-one (3) was synthesized in high yield by an aldol condensation between 3-acetyl-2,5-dimethylfuran and 3,5-dimethyl-1-phenylpyrazole-4-carboxaldehyde in ethanolic NaOH at room temperature. Its structure was fully characterized by elemental analysis, IR, 1H NMR, 13C NMR and EI-MS spectral analysis. Full article
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Open AccessShort Note (8-Chloro-3-methyl-1H-pyrazolo[4,3-c]cinnolin-1-yl) (pyridin-4-yl)methanone
Molbank 2010, 2010(2), M688; doi:10.3390/M688
Received: 14 July 2010 / Accepted: 21 July 2010 / Published: 23 July 2010
PDF Full-text (75 KB) | Supplementary Files
Abstract (8-Chloro-3-methyl-1H-pyrazolo[4,3-c]cinnolin-1-yl) (pyridin-4-yl)methanone 2 has been synthesized through condensation of 3-acetyl-6-chloro-1H-cinnolin-4-one 1 with isonicotinic acid hydrazide (INH) in absolute ethanol. The structure of the title compound 2 was established on the basis of IR, 1H-NMR, 13C-NMR and mass spectral data. Full article
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