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Metals, Volume 15, Issue 8

2025 August - 109 articles

Cover Story: A porous TiNi3 intermetallic compound has been fabricated through the reactive synthesis of elemental powders, wherein pore formation can be attributed to a combination of the bridging effects of initial powder particles and the Kirkendall effect occurring during the sintering process. This porous TiNi3 intermetallic compound shows favorable corrosion resistance in a 1 M KOH solution, with a corrosion potential of − 0.979 VSCE and a corrosion current density of 1.18 × 10−4 A∙cm−2, reducing the thermodynamic corrosion tendency and corrosion rate. The formation of a more stable passive film with the incorporation of Ti contributes to this improved corrosion resistance performance. View this paper
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Articles (109)

  • Article
  • Open Access
1,035 Views
11 Pages

Effect of Heat Treatment Temperature on the Microstructure and Mechanical Properties of Fe-18Mn-0.6C-xAl

  • Li Xiao,
  • Yuqi Zhang,
  • Huan Huang,
  • Bochao Zhang,
  • Ningning Ji,
  • Shuang Li and
  • Jun Chen

21 August 2025

High-Mn steels are commonly fabricated by hot rolling and on-line cooling for cryogenic applications, because there exists an aging embrittlement zone in most high-Mn steels, and this shortcoming makes it difficult to optimize their mechanical proper...

  • Article
  • Open Access
879 Views
14 Pages

21 August 2025

To enhance the safe service performance of corrosion-resistant tank steel, it is of significant importance to develop novel materials characterized by both high strength-toughness and a low yield ratio. In this study, four experimental steels with a...

  • Communication
  • Open Access
1 Citations
877 Views
9 Pages

Effect of HfC Content on the Elevated-Temperature Ablation Behavior of W-HfC Composites

  • Boyuan Zheng,
  • Chaoqian Song,
  • Yidong Wu,
  • Zhong Du,
  • Liye Du,
  • Baohong Zhang and
  • Xidong Hui

21 August 2025

The effects of HfC content on the ablation resistance of W-HfC composites were systematically studied. The oxy-acetylene flame ablation test was conducted at 2800 °C. Post-ablation samples were characterized via XRD, section morphology, and EDS....

  • Article
  • Open Access
959 Views
16 Pages

21 August 2025

In this study, the feasibility of converting iron-bearing tailings from urban steel scrap recycling to value-added direct reduced iron (DRI) via magnetic separation followed by hydrogen reduction under microwave irradiation was investigated, with an...

  • Article
  • Open Access
1 Citations
1,187 Views
19 Pages

21 August 2025

This study investigated the influence of manganese (Mn) on microstructure evolution and property optimization in Al-0.6Mg-0.58Si-0.24Fe-xMn alloys under both as-cast and hot-extruded conditions. The balance mechanisms of Mn in tensile properties and...

  • Article
  • Open Access
1 Citations
1,029 Views
14 Pages

Investigating the Effect of Calcium Addition on the Microstructural and Mechanical Properties of a Zn-Al-Cu-Mg Alloy via Squeeze Casting

  • Thiyagesan Gopalakrishnan,
  • Sankara Raman Sankaranarayanan and
  • Subramanian Palani Kumaresh Babu

20 August 2025

This study investigates on Zn-Al alloy microstructural characteristics and mechanical properties of a Zn-Al alloy with calcium (Ca) additions ranging from 0.5 to 1.5 wt.%. The base alloy composition is 94.95 wt.% Zn, 4.0 wt.% Al, 1.0 wt.% Cu, and 0.0...

  • Article
  • Open Access
1,108 Views
24 Pages

20 August 2025

This study presents a novel approach to understanding fatigue and crack growth phenomena by benchmarking experimental observations with numerical simulations. We introduced controlled residual stress fields away from notch-induced crack nucleation si...

  • Article
  • Open Access
1 Citations
1,337 Views
14 Pages

20 August 2025

Determining orientation relationships between different grains or phases via electron diffraction typically requires coincident zone axes, but it is difficult to achieve in most cases due to tilting angle limitations. To address this challenge, a str...

  • Article
  • Open Access
2 Citations
1,090 Views
14 Pages

19 August 2025

Boron (B) is widely used as a neutron-absorbing nuclide and has significant applications in the nuclear industry. B4C/Al composites combine the high hardness of B4C with the ductility of Al, making them commonly used neutron-absorbing materials. Unde...

  • Article
  • Open Access
2 Citations
1,088 Views
20 Pages

Electrochemical Characterization of CO2 Corrosion Inhibition of API X100 by a Gemini Surfactant Under Static and Dynamic Conditions

  • Andres Carmona-Hernandez,
  • Rolando Abraham Sánchez-Garrido,
  • Eduardo Palacios-González,
  • Elizabeth America Flores-Frías,
  • Aldo Emelio Landa-Gómez,
  • Edgar Mejía-Sánchez,
  • Araceli Espinoza-Vázquez,
  • Ricardo Orozco-Cruz and
  • Ricardo Galván-Martínez

19 August 2025

In this research work, the electrochemical evaluation of a non-ionic gemini surfactant as a green corrosion inhibitor for X100 pipeline steel in CO2-saturated brine solution was carried out by electrochemical impedance spectroscopy (EIS) and potentio...

  • Article
  • Open Access
824 Views
22 Pages

19 August 2025

Picosecond laser drilling offers high precision and quality, and compared to femtosecond lasers, it also balances processing efficiency, making it widely used across various fields. However, existing drilling processes still face issues such as round...

  • Article
  • Open Access
1 Citations
945 Views
12 Pages

19 August 2025

Welded structures, such as offshore platforms, require robust toughness in their heat-affected zones (HAZ) to withstand low-temperature environments. The coarse-grained HAZ (CGHAZ) adjacent to the fusion boundary often exhibits reduced toughness due...

  • Article
  • Open Access
3 Citations
2,903 Views
19 Pages

Microstructure and Properties of Bi-Sn, Bi-Sn-Sb, and Bi-Sn-Ag Solder Alloys for Electronic Applications

  • Andrei-Alexandru Ilie,
  • Florentina Niculescu,
  • Gheorghe Iacob,
  • Ion Pencea,
  • Florin Miculescu,
  • Robert Bololoi,
  • Dumitru-Valentin Drăguț,
  • Alexandru-Cristian Matei,
  • Mihai Ghiţă and
  • Constantin Ungureanu
  • + 1 author

18 August 2025

The Bi-Sn, Bi-Sn-Ag, and Bi-Sn-Sb solder alloy systems represent lead-free, environmentally friendly alternatives for reliable electronic assembly. These alloys comply with increasingly strict environmental and health regulations, while offering low...

  • Review
  • Open Access
4 Citations
4,286 Views
32 Pages

17 August 2025

The electric arc furnace (EAF) is a key technology in the steel production industry, particularly for recycling scrap iron. It plays a crucial role in the shift to low-carbon metallurgy, responding to the growing demand for more sustainable productio...

  • Article
  • Open Access
1 Citations
1,148 Views
10 Pages

Impact of Surface Preparation on the Quantification of Diffusible Hydrogen Content in Aluminum Alloys

  • Mehrdad Hoseinpoor,
  • Nikola Macháčková,
  • Terezie Košová Altnerová,
  • Sandrine Zanna,
  • Darja Rudomilova and
  • Tomáš Prošek

17 August 2025

The impact of final surface preparation immediately prior to hydrogen content measurements in aluminum alloy samples was investigated using thermal desorption analysis (TDA). Samples ground in water showed an apparent hydrogen signal. Glow-discharge...

  • Article
  • Open Access
1,086 Views
16 Pages

Thermodynamic Modeling of Microstructural Design of Lightweight Ferritic Steels

  • Tamiru Hailu Kori,
  • Adam Skowronek,
  • Jarosław Opara,
  • Ana Paula Domingos Cardoso and
  • Adam Grajcar

16 August 2025

Ferritic lightweight steels are an emerging class of low-density steels (LDSs) with promising mechanical properties. The study aimed to develop two ferritic lightweight steels with different Mn concentrations. Al was incorporated to achieve the light...

  • Article
  • Open Access
2 Citations
1,337 Views
16 Pages

16 August 2025

Heat sinks with thin and tall fins made from pure aluminum using die casting are in demand due to the higher thermal conductivity of pure aluminum compared to aluminum alloys. However, die casting of thin and tall fins using pure aluminum is consider...

  • Article
  • Open Access
2 Citations
1,602 Views
19 Pages

16 August 2025

Stainless steel welding plays a critical role in industrial manufacturing due to its superior corrosion resistance and structural reliability. The keyhole tungsten inert gas (K-TIG) welding, renowned for its high efficiency, high precision, and cost-...

  • Article
  • Open Access
985 Views
11 Pages

16 August 2025

High manganese steel can improve its microstructure after aging treatment, which is beneficial for enhancing strength, toughness, and wear resistance. This study aims to explore the effect of aging treatment on mechanical properties and wear resistan...

  • Article
  • Open Access
1,107 Views
23 Pages

Optimization of Eleven Cross-Roll Straightening Process for 20CrMnTi Bars Based on Combined Hardening Model

  • Shangwu Jia,
  • Longyi Bao,
  • Shijie Wang,
  • Qingdang Meng,
  • Jun Zhao and
  • Ruixue Zhai

15 August 2025

Straightness is one of the important indices to measure the quality of bars; multi-roll straightening is an essential process in bar production. Materials undergo multiple cycles of alternating tensile and compressive loading during multi-roll straig...

  • Article
  • Open Access
1 Citations
891 Views
14 Pages

15 August 2025

In this study, a laboratory-precision four-high micro-rolling mill was employed to investigate the influence of grain size on the deformation behavior and fracture mechanism of a micro-rolled Cu/Al composite ultra-thin sheet. Analytical testing techn...

  • Article
  • Open Access
778 Views
15 Pages

Effect of La/Zn on Microstructural Evolution and Mechanical Properties of Extruded Mg-9Gd-3Y Alloy

  • Xiang Zhang,
  • Yuyang Gao,
  • Ang Zhang,
  • Jing Zhao,
  • Yan Song,
  • Tian Li and
  • Bin Jiang

15 August 2025

This study investigated the impact of La and Zn additions on the microstructure and mechanical properties (at room and high temperatures) of extruded Mg-9Gd-3Y (GW93) alloy. The incorporation of La and Zn induced the precipitation of granular second...

  • Article
  • Open Access
4,552 Views
15 Pages

14 August 2025

The plastic deformation during equal-channel angular pressing (ECAP) can be affected by various material- and processing-related factors. For instance, the initial crystal orientation and grain size play an important role in determining the material...

  • Article
  • Open Access
918 Views
15 Pages

14 August 2025

The critical challenge of achieving precise geometric control in laser directed energy deposition (L-DED) of Inconel 690 for nuclear applications is addressed by this study. We established a data-driven optimization framework that reduces time-consum...

  • Article
  • Open Access
1,031 Views
13 Pages

14 August 2025

MnFe2O4/Fe soft magnetic composites (SMCs) were designed by the surface oxidation method, and the MnFe2O4 layer was utilized as the insulation coating. The microstructure of SMCs and the chemical composition of the insulation layer were observed usin...

  • Article
  • Open Access
1 Citations
885 Views
15 Pages

13 August 2025

This study explores the development of a novel composite coating system combining the high hardness of WC and thermal conductivity of Cu, employing the plasma transfer arc welding method under ambient conditions. Utilizing an advanced welding approac...

  • Article
  • Open Access
983 Views
14 Pages

12 August 2025

The degree of anisotropy and heterogeneity in coarse-grained materials significantly affects ultrasonic propagation behavior and scattering. This paper proposes a vector coherent factor threshold total focusing imaging method (VCF-T-TFM) for austenit...

  • Article
  • Open Access
1 Citations
1,071 Views
11 Pages

12 August 2025

This article investigates the formation of solidification cracks in steel forgings used for bearing rings in gear reducers of robotic arms. The forging and heat treatment processes, conducted under consistent technological conditions, revealed the oc...

  • Article
  • Open Access
1 Citations
956 Views
15 Pages

Effect of Cu and Ag Content on the Electrochemical Performance of Fe40Al Intermetallic Alloy in Artificial Saliva

  • Jesus Porcayo-Calderon,
  • Roberto Ademar Rodriguez-Diaz,
  • Jonathan de la Vega Olivas,
  • Cinthya Dinorah Arrieta-Gonzalez,
  • Jose Gonzalo Gonzalez-Rodriguez,
  • Jose Guadalupe Chacón-Nava and
  • José Luis Reyes-Barragan

11 August 2025

This study investigates the effect of copper (Cu) and silver (Ag) additions on the electrochemical behavior of the Fe40Al intermetallic alloy in artificial saliva, aiming to evaluate its potential for biomedical applications such as dental implants....

  • Article
  • Open Access
801 Views
22 Pages

Experimental Study on the Microscale Milling Process of DD5 Nickel-Based Single-Crystal Superalloy

  • Ying Li,
  • Yadong Gong,
  • Yang Liu,
  • Zhiheng Wang,
  • Junhe Zhao,
  • Zhike Wang and
  • Zelin Xu

11 August 2025

Technological advances have expanded the use of single-crystal in microscale applications—particularly in infrared optics, electronics, and aerospace. Conducting research on the surface quality of micro-milling processes for single-crystal supe...

  • Article
  • Open Access
1,272 Views
34 Pages

Optimization of Process Parameters in Electron Beam Cold Hearth Melting and Casting of Ti-6wt%Al-4wt%V via CFD-ML Approach

  • Yuchen Xin,
  • Jianglu Liu,
  • Yaming Shi,
  • Zina Cheng,
  • Yang Liu,
  • Lei Gao,
  • Huanhuan Zhang,
  • Haohang Ji,
  • Tianrui Han and
  • Qiuni Zhao
  • + 2 authors

11 August 2025

During electron beam cold hearth melting (EBCHM) of Ti-6wt%Al-4wt%V titanium alloy, aluminum volatilization causes compositional segregation in the ingot, significantly degrading material performance. Traditional methods (e.g., the Langmuir equation)...

  • Article
  • Open Access
1,037 Views
21 Pages

Microstructural and Mechanical Characterization of Co-Free AlxTixCrFe2Ni High-Entropy Alloys

  • Róbert Kočiško,
  • Ondrej Milkovič,
  • Patrik Petroušek,
  • Gabriel Sučik,
  • Dávid Csík,
  • Karel Saksl,
  • Ivan Petryshynets,
  • Karol Kovaľ and
  • Pavel Diko

10 August 2025

This study investigates the effect of Alx and Tix content (x = 0.1, 0.2, 0.3, 0.4, 0.5, and 0.6) on the microstructural evolution and mechanical properties of Co-free high-entropy AlxTixCrFe2Ni alloys in both as-cast and homogenized conditions. The r...

  • Article
  • Open Access
1,285 Views
20 Pages

Numerical and Experimental Investigations on the Compressive Properties of the Graded BCC Lattice Cylindrical Shells Made of 316L Stainless Steel

  • Yiting Guan,
  • Wenjie Ma,
  • Miao Cao,
  • Hao Xu,
  • Wenchang Luo,
  • Weidong Cao,
  • Siying Wang,
  • Ying Qin,
  • Xiaoyu Zhang and
  • Xiaofei Cao

10 August 2025

Uniform and graded BCC lattice cylindrical shells were proposed, and the corresponding structural specimens were fabricated with 316L stainless steel material. Experimental testing and numerical simulations were both utilized to investigate the quasi...

  • Article
  • Open Access
3 Citations
1,095 Views
18 Pages

10 August 2025

Picosecond laser trepanning is a key technology for fabricating film cooling holes in aero-engine turbine blades, overcoming the limitations of conventional machining such as severe tool wear and thermal damage. However, optimizing this advanced proc...

  • Article
  • Open Access
773 Views
19 Pages

Combined Influence of Stretch-Bending Straightening and Ageing on the Tensile Properties of Packaging Steels

  • Sebastian Möller,
  • Dimitrios Nouskalis,
  • Björn Ehmke,
  • Holm Altenbach and
  • Christian Dresbach

9 August 2025

Stretch-bending straightening is used to ensure the desired flatness properties of packaging steel in the final stage of semi-finished product manufacturing. Not only is the flatness of the steel affected by the alternating bending load and the tensi...

  • Article
  • Open Access
1,265 Views
18 Pages

Al2O3-Embedded LiNi0.9Mn0.05Al0.05O2 Cathode Engineering for Enhanced Cyclic Stability in Lithium-Ion Batteries

  • Fei Liu,
  • Chenfeng Wang,
  • Ning Yang,
  • Zundong Xiao,
  • Aoxuan Wang and
  • Rijie Wang

8 August 2025

With the rapid advancement of new energy electric vehicles, high-capacity nickel-rich layered oxides have emerged as predominant cathode materials in lithium-ion battery systems. However, their widespread implementation necessitates rigorous investig...

  • Article
  • Open Access
2 Citations
1,490 Views
18 Pages

8 August 2025

Critical metals such as rare earth elements (REEs) are primarily associated with silicates and aluminosilicates in coal fly ash, resulting in poor REE recovery. Silicate bacteria can decompose silicate minerals and release silicon, but their impact o...

  • Article
  • Open Access
1 Citations
1,304 Views
23 Pages

Multi-Scale Mechanical Anisotropy and Heat Treatment Effects in Additively Manufactured AlSi10Mg

  • Aikaterini Argyrou,
  • Leonidas Gargalis,
  • Leonidas Karavias,
  • Evangelia K. Karaxi and
  • Elias P. Koumoulos

8 August 2025

This study investigates the combined effects of build planes and heat treatments on the micro- and nanoscale mechanical properties of additively manufactured AlSi10Mg alloy. The hardness and elastic modulus were examined across two principal planes,...

  • Article
  • Open Access
1 Citations
860 Views
16 Pages

Surface Integrity Evolution and Fretting Wear Improvement of DD6 Single-Crystal Superalloy via Laser Shock Peening and Laser Shock Peening Without Coating

  • Yuliang Li,
  • Linjie Qiao,
  • Xiaofeng Dang,
  • Mo Lang,
  • Sihai Luo,
  • Liucheng Zhou,
  • Xiaoqing Liang and
  • Weifeng He

8 August 2025

In this paper, the different effects of laser shock peening (LSP) and laser shock peening without coating (LSPwC) on the morphology, microhardness and fretting-wear behavior of DD6 Ni-based single-crystal superalloy are investigated. The results show...

  • Article
  • Open Access
895 Views
16 Pages

8 August 2025

This study focuses on the removal of arsenic (As) from contaminated water originating from an abandoned mercury mine landfill. To obtain results that more accurately reflect the material’s behavior under real-world conditions, tests were conduc...

  • Article
  • Open Access
1 Citations
1,214 Views
38 Pages

Development of Technology for Processing Pyrite–Cobalt Concentrates to Obtain Pigments of the Composition Fe2O3 and Fe3O4

  • Tatyana Chepushtanova,
  • Aliya Altmyshbayeva,
  • Yerik Merkibayev,
  • Kulzira Mamyrbayeva,
  • Zhanat Yespenova and
  • Brajendra Mishra

7 August 2025

This paper presents the results of a study on the development of a processing technology for pyrite–cobalt concentrates to obtain iron oxide pigments (Fe2O3 and Fe3O4) via high-temperature hydrolysis. It was found that, in a single operation, t...

  • Article
  • Open Access
969 Views
24 Pages

7 August 2025

This study focuses on realistic modeling of forming load and microstructural evolution during hot metal extrusion, emphasizing the effects of friction models and hydraulic press behavior. Rather than merely predicting load magnitudes, the objective i...

  • Article
  • Open Access
704 Views
24 Pages

7 August 2025

The anisotropic nature of cup ears formed during the deep drawing of sheet metals is governed by the distribution of crystallographic orientation in interaction between earing. In this study, we examined the orientation development of a cube-oriented...

  • Article
  • Open Access
1 Citations
719 Views
17 Pages

7 August 2025

In this study, aluminum single crystals with a {1 0 0} <0 0 1> (Cube) orientation were rolled under two conditions: with external constraints imposed by an external aluminum frame (3DRC) and without external constraints (3DR). The crystal plast...

  • Article
  • Open Access
1,011 Views
14 Pages

7 August 2025

Alloys and metals exhibit high sensitivity to corrosion and aggressive environments. Hence, the development of protective treatments through accessible methods with a high degree of protection has become a necessity. This paper presents a method for...

  • Article
  • Open Access
969 Views
26 Pages

Research on Hydrogen/Deuterium Permeation Behavior and Influencing Factors of X52MS Pipeline Steel

  • Ning Liu,
  • Ke Jin,
  • Junqiang Ren,
  • Jie Sheng,
  • Xuefeng Lu and
  • Xingchang Tang

7 August 2025

The hydrogen/deuterium permeation behavior of X52MS pipeline steel with three thicknesses was investigated using the gas/liquid phase permeation method by changing the current density and regulating the surface roughness. The permeation curves under...

  • Article
  • Open Access
970 Views
20 Pages

Electrochemical Behavior of Thermomechanically Processed UNS S41003 Steel in Acidic Chloride Media: Assessing Martensitic Transformation Effects

  • Carlos H. B. Queiroz,
  • Davi A. Marques,
  • Otílio B. F. Diógenes,
  • Daniel de C. Girão,
  • Roberta B. Vasques,
  • Adolfo K. do N. Viana,
  • Gemma Fargas,
  • Mauro A. C. Florez and
  • Walney S. Araújo

7 August 2025

UNS S41003 is a low-cost, low-carbon ferritic stainless steel that exhibits moderate corrosion resistance but limited mechanical performance. This study evaluates the electrochemical behavior of untreated and thermomechanically treated UNS S41003 sam...

  • Article
  • Open Access
1 Citations
1,005 Views
33 Pages

Constructal Design and Numerical Simulation Applied to Geometric Evaluation of Stiffened Steel Plates Subjected to Elasto-Plastic Buckling Under Biaxial Compressive Loading

  • Andrei Ferreira Lançanova,
  • Raí Lima Vieira,
  • Elizaldo Domingues dos Santos,
  • Luiz Alberto Oliveira Rocha,
  • Thiago da Silveira,
  • João Paulo Silva Lima,
  • Emanuel da Silva Diaz Estrada and
  • Liércio André Isoldi

6 August 2025

Widely employed in diverse engineering applications, stiffened steel plates are often subjected to biaxial compressive loads. Under these conditions, buckling may occur, initially within the elastic range but potentially progressing into the elasto-p...

  • Article
  • Open Access
1 Citations
1,096 Views
15 Pages

Processing of Secondary Raw Materials from Ferrochrome Production via Agglomeration and Study of Their Mechanical Properties

  • Yerlan Zhumagaliyev,
  • Yerbol Shabanov,
  • Maral Almagambetov,
  • Maulen Jundibayev,
  • Nursultan Ulmaganbetov,
  • Salamat Laikhan,
  • Akgul Jundibayeva,
  • Aigerim Abilberikova,
  • Nurbala Ubaidulayeva and
  • Rysgul Adaibayeva

6 August 2025

In the process of producing ferroalloys, a large amount of secondary raw materials is formed, including slag, aspiration dusts and sludge. The recycling of secondary raw materials can create resources and bring environmental and economic benefits. We...

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Metals - ISSN 2075-4701