Post-manufacturing Testing and Characterization of Materials

A special issue of Designs (ISSN 2411-9660).

Deadline for manuscript submissions: 31 May 2025 | Viewed by 2476

Special Issue Editor


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Guest Editor
School of Mechanical & Manufacturing Engineering, Dublin City University, Dublin, Ireland
Interests: additive manufacturing; laser surface processing; metal surface modification
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Special Issue Information

Dear Colleagues,

Materials science is witnessing a paradigm shift with the advent of advanced manufacturing techniques such as additive manufacturing, precision machining, forging, flow forming, and deep drawing. While these processes bestow unprecedented flexibility and efficiency, they also introduce a myriad of challenges in ensuring the integrity and performance of materials. Post-manufacturing, materials often undergo intricate microstructural and chemical composition changes, including phase transformation and grain size alteration, propelled by diverse cooling rates and mechanical stresses. For this reason, subsequent processing might be necessary in order to mitigate this problem and produce parts with more consistent properties.

These intrinsic alterations to materials post-production necessitate meticulous scrutiny to accurately discern the structural evolution and functional attributes of the materials. Understanding these transformations is pivotal for engineers and researchers to optimize material design and fabrication processes, ensuring superior performance and reliability across diverse applications. However, the journey towards comprehensive material characterization post-manufacturing is riddled with challenges. The multifaceted nature of these transformations demands a multifaceted approach towards testing and analysis. Traditional methods often fall short in capturing the nuances of these changes, necessitating the development and integration of advanced analytical techniques and methodologies. Moreover, the time-sensitive nature of modern manufacturing necessitates expeditious yet precise characterization protocols to facilitate rapid decision-making and process optimization. This urgency underscores the imperative of leveraging cutting-edge technologies, such as advanced microscopy, spectroscopy, and computational modelling, to unravel the intricacies of post-manufacturing material behaviour efficiently. Furthermore, the interdisciplinary nature of materials science underscores the need for collaboration and knowledge exchange across diverse domains. Collaborative efforts between materials scientists, engineers, and manufacturing experts are indispensable in navigating the complexities of post-manufacturing material testing and characterization, fostering innovation and driving progress in materials science and engineering.

In conclusion, the pursuit of excellence in material performance mandates a holistic approach towards post-manufacturing testing and characterization. By embracing innovation, collaboration, and advanced analytical techniques, we can unravel the enigma of material behaviour, paving the way for transformative advancements in manufacturing, engineering, and beyond.

In this Special Issue (SI), we delve into the critical significance of post-manufacturing testing and characterization of materials when trying to comprehend and delineate material properties. We invite authors to publish their original and review articles in this SI and share the results achieved in material properties and inspection.

Dr. Obeidi Muhannad
Guest Editor

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Keywords

  • additive manufacturing
  • 3D printing
  • defect evaluation
  • mechanical stresses
  • deformation
  • simulation
  • material characterization
  • process control
  • post-manufacturing

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Published Papers (3 papers)

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Research

16 pages, 5548 KiB  
Article
Optimizing Selective Laser Melting of Inconel 625 Superalloy through Statistical Analysis of Surface and Volumetric Defects
by Ali Shahrjerdi, Mojtaba Karamimoghadam, Reza Shahrjerdi, Giuseppe Casalino and Mahdi Bodaghi
Designs 2024, 8(5), 87; https://doi.org/10.3390/designs8050087 - 28 Aug 2024
Viewed by 418
Abstract
This article delves into optimizing and modeling the input parameters for the selective laser melting (SLM) process on Inconel 625. The primary aim is to investigate the microstructure within the interlayer regions post-process optimization. For this study, 100 layers with a thickness of [...] Read more.
This article delves into optimizing and modeling the input parameters for the selective laser melting (SLM) process on Inconel 625. The primary aim is to investigate the microstructure within the interlayer regions post-process optimization. For this study, 100 layers with a thickness of 40 µm each were produced. Utilizing the design of experiments (DOE) methodology and employing the Response Surface Method (RSM), the SLM process was optimized. Input parameters such as laser power (LP) and hatch distance (HD) were considered, while changes in microhardness and roughness, Ra, were taken as the responses. Sample microstructure and surface alterations were assessed via scanning electron microscopy (SEM) analysis to ascertain how many defects and properties of Inconel 625 can be controlled using DOE. Porosity and lack of fusion, which were due to rapid post-powder melting solidification, prompted detailed analysis of the flaws both on the surfaces of and in terms of the internal aspects of the samples. An understanding of the formation of these imperfections can help refine the process for enhanced integrity and performance of Inconel 625 printed material. Even slight directional changes in the columnar dendrite structures are discernible within the layers. The microstructural characteristics observed in these samples are directly related to the parameters of the SLM process. In this study, the bulk samples achieved a microhardness of 452 HV, with the minimum surface roughness recorded at 9.9 µm. The objective of this research was to use the Response Surface Method (RSM) to optimize the parameters to result in the minimum surface roughness and maximum microhardness of the samples. Full article
(This article belongs to the Special Issue Post-manufacturing Testing and Characterization of Materials)
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15 pages, 8322 KiB  
Article
Computational Investigation of the Fluidic Properties of Triply Periodic Minimal Surface (TPMS) Structures in Tissue Engineering
by Muhammad Noman Shahid, Muhammad Usman Shahid, Shummaila Rasheed, Muhammad Irfan and Muhannad Ahmed Obeidi
Designs 2024, 8(4), 69; https://doi.org/10.3390/designs8040069 - 10 Jul 2024
Viewed by 777
Abstract
Tissue engineering, a rapidly advancing field in medicine, has made significant strides with the development of artificial tissue substitutes to meet the growing need for organ transplants. Three-dimensional (3D) porous scaffolds are widely utilized in tissue engineering, especially in orthopedic surgery. This study [...] Read more.
Tissue engineering, a rapidly advancing field in medicine, has made significant strides with the development of artificial tissue substitutes to meet the growing need for organ transplants. Three-dimensional (3D) porous scaffolds are widely utilized in tissue engineering, especially in orthopedic surgery. This study investigated the fluidic properties of diamond and gyroid structures with varying porosity levels (50–80%) using Computational Fluid Dynamics (CFD) analysis. The pressure and velocity distributions were analyzed, and it was observed that the pressure decreased gradually, whereas the velocity increased in the central area of the surface structures. Specifically, the pressure drop ranged from 2.079 to 0.984 Pa for the diamond structure and from 1.669 to 0.943 Pa for the gyroid structure as the porosity increased from 50% to 80%. It was also found that the permeability increased as the porosity level increased, with values ranging from 2.424×109 to 5.122×109 m2 for the diamond structure and from 2.966×109 to 5.344×109 m2 for the gyroid structure. The wall shear stress (WSS) was also analyzed, showing a consistent decrease with increased porosity for both types of structures, with WSS values ranging from 9.903×102 to 9.840×101 Pa for the diamond structure and from 1.150×101 to 7.717×102 Pa for the gyroid structure. Overall, this study provides insights into the fluidic properties of diamond and gyroid structures, which can be useful in various applications such as tissue engineering. Full article
(This article belongs to the Special Issue Post-manufacturing Testing and Characterization of Materials)
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15 pages, 16558 KiB  
Article
Investigation on the Microstructure and Micro-Mechanical Properties of Thermal-Sprayed NiCoCrAlY High Entropy Alloy Coating
by Animesh Kumar Basak, Nachimuthu Radhika, Chander Prakash and Alokesh Pramanik
Designs 2024, 8(2), 37; https://doi.org/10.3390/designs8020037 - 20 Apr 2024
Cited by 1 | Viewed by 1006
Abstract
NiCoCrAlY high entropy alloy (HEA) coating (47.1 wt.% Ni, 23 wt.% Co, 17 wt.% Cr, 12.5 wt.% Al, and 0.4 wt.% Y) was deposited on a stainless steel subtract by atmospheric plasma spraying (APS). The as-deposited coating was about 300 μm thickness with [...] Read more.
NiCoCrAlY high entropy alloy (HEA) coating (47.1 wt.% Ni, 23 wt.% Co, 17 wt.% Cr, 12.5 wt.% Al, and 0.4 wt.% Y) was deposited on a stainless steel subtract by atmospheric plasma spraying (APS). The as-deposited coating was about 300 μm thickness with <1% porosity. The microstructure of the coating consisted of dispersed secondary phases/intermetallics in the solid solution. The stress–strain behaviour of this coating was investigated in micro-scale with the help of in situ micro-pillar compression. The experimental results show that yield and compressive stress in the cross-section of the coating was higher (1.27 ± 0.10 MPa and 2.19 ± 0.10 GPa, respectively) than that of the planar direction (0.85 ± 0.09 MPa and 1.20 ± 0.08 GPa, respectively). The various secondary/intermetallic phases (γ′–Ni3Al, β–NiAl) that were present in the coating microstructure hinder the lattice movement during compression, according to Orowan mechanism. In addition to that, the direction of the loading to that of the orientation of the phase/splat boundaries dictate the crack propagation architecture, which results in difference in the micro-mechanical properties. Full article
(This article belongs to the Special Issue Post-manufacturing Testing and Characterization of Materials)
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