Search Results (79)

Sheet metal forming is a widely used manufacturing process, but the high cost and long production time of traditional forming tools limit its flexibility, especially for prototyping and small-batch production. Additive manufacturing offers a promising alternative, enabling the rapid and cost-effective fabrication of customized tools. In this study, bending tools were produced using Fused Filament Fabrication and optimized through a topology optimization approach. A combined experimental and numerical approach was applied to validate standard tool geometries and extract load conditions for use in a topology optimization process. The resulting optimized punch and die achieved a mass reduction of approximately 50% while maintaining structural integrity and safety factors well above critical thresholds. Finite Element Analysis revealed an increase in elastic deformation and stress concentration in non-critical regions, without compromising tool functionality. Experimental tests with the optimized tools confirmed their suitability for sheet metal bending, although a decrease of about 2° in the bending angle and an increase in variability were observed, consistent with simulation results. The study demonstrates the feasibility of using topology-optimized polymer tools for low-volume forming applications, offering a lightweight, cost-effective, and sustainable alternative to traditional metal tooling. Full article

Degradation of power engineering steel structures requires constant monitoring of their mechanical properties to estimate remaining service life. Therefore, the current study aimed to develop a methodology that will enable for accurate determination of changes in mechanical properties of 10CrMo9-10 steel after long-term exploitation involving the Small Punch Test (SPT). Firstly, the as-received 10CrMo9-10 steel was annealed at 770 °C for different periods (1.5, 6 and 24 h) to deteriorate its strength to a level similar to its exploited counterpart. Then, mechanical properties were characterized by uniaxial tensile tests and the SPT method using miniaturized discs with a diameter of 8 mm and a thickness of 0.5 mm as recommended by the EN 10371:2021 standard. It allowed to determine a formula correlating the SPT results (i.e., elastic–plastic transition force and maximum force) with the yield and ultimate tensile strength. The β_Rp0.2 and β_Rm correlation factors were equal to 0.437 and 0.255, respectively. Finally, the exploited 10CrMo9-10 steel was tested by the SPT method. Based on the SPT results, the values of R_p0.2 = 236 ± 27 MPa and R_m = 459 ± 17 MPa were estimated, which were close to those assessed during the uniaxial tensile tests (R_p0.2 = 218 ± 3 MPa and R_m = 454 ± 4 MPa). It was shown that the application of such a relatively simple method is a promising way for determining the changes in mechanical properties of structural steels after long-term service at elevated temperature. Full article

Laser powder bed fusion (LPBF) can fabricate hydraulic components with significant weight reduction, and in this study, small punch tests (SPTs) evaluated the tensile and fracture properties of four stainless steels (30Cr13, 316L, 15-5PH, 17-4PH), alongside metallographic, scanning electron microscope (SEM), and Electron Backscatter Diffraction (EBSD) analyses which examined their fracture modes, grain orientation, phase distribution, and grain boundary distribution. The tensile property results showed ductility rankings as 316L > 17-4PH > 15-5PH > 30Cr13, with correlations between R_p0.2 and R_m from SPT and uniaxial tensile tests for all four, while high-magnification SEM fractographs revealed ductile dimples on 15-5PH, 17-4PH, and 316L SPT specimens versus distinct cleavage fracture in 30Cr13. EBSD analysis indicated austenite content order as 316L > 17-4PH > 30Cr13 > 15-5PH, grain size order as 316L > 17-4PH > 15-5PH > 30Cr13, and high-angle grain boundaries ranking as 15-5PH > 30Cr13 > 17-4PH > 316L; additionally, notched SPT specimens inspected per EN 10371 for fracture toughness showed J-integral (J_IC) values in the order 316L > 17-4PH > 15-5PH > 30Cr13, consistent with ductility and grain size results. Full article

The microstructural evolution and mechanical properties of WWER 440 steam generator steel GOST 22K after long-term operation were thoroughly examined in this study. The samples were taken directly from a steam generator using the small punch test method. The uniqueness of these samples lies in the fact that they were real operating materials used in a nuclear power plant with different years of operation. The microstructure was characterized using optical microscopy and transmission electron microscopy supplemented by selective electron diffraction and semi-quantitative chemical microanalysis. It was found that with the prolongation of the operation time of the steam generator, the density of carbides increased slightly, which was reflected in a decrease in the mean distance between particles, but these differences were very small, which indicates the microstructural stability of GOST 22K steel. The stability of this steel was also confirmed by measuring its mechanical properties, which changed only minimally depending on the years of operation. The tensile strength values were in the range of 508 to 579 MPa. In the case of the ductile-to-brittle transition temperature (DBTT), a slight increase was found after 6 years of operation. The DBTT did not change significantly with subsequent operation. Full article

The present work is a relevant advance in the validation of the incremental step loading technique (ASTM F1624 standard) when applied to Small Punch tests (SPT) for the threshold load determination of medium- and high-strength steels in aggressive environments, as a novel alternative to conventional time-consuming tests under constant load. It completes previous works by the authors on this topic, extending a methodology to estimate the threshold stress from SPT tests in aggressive environments, covering the whole range of hardness marked by ASTM F1624 as the main goal. This is achieved by calibrating a model of the material’s hardness by the use of a coefficient in function of it. For this purpose, four medium- and high-strength steels of 33, 35, 50 and 60 HRC (Hardness Rockwell C) are exposed to three different cathodic polarization hydrogen embrittlement environments of 1, 5 and 10 mA/cm² in 1N H₂SO₄ acid electrolyte connected to a platinum anode. Threshold stresses in these circumstances are obtained by uniaxial specimens following ASTM F1624 and compared to their homologous threshold loads obtained by Small Punch tests according to the authors’ original methodology proposal. Finally, the aforementioned model, consisting of a correlation based on composing an elastic and a plastic part, is calibrated for a hardness ranging 33–60 HRC, this being the main original contribution of this work; the elastic part is dependent just on the elastic-to-plastic transition SPT load, while the plastic part is ruled by a material hardness-dependent coefficient. This technique supposes an advance in engineering tools, due to its applicability in situations of material shortage, such as in-service components, welded joints, local areas, complex geometries, small thicknesses, etc., often present in aerospace, automotive or oil–gas, among others. Full article

The utilization of micro-sample testing has demonstrated its effectiveness in conducting quantitative research on mechanical properties, damage evolutions and fracture features. For in-service equipment, millimicron sampling allows for non-destructive testing and analysis of mechanical performance evolution during operation. This paper presents a comparative study of the miniature uniaxial tensile test (MUTT) and small punch test (SPT) by experimental and finite element methods. As a comparison, the standard conventional-size tensile tests were also carried out. Detailed analyses of the elastoplastic behaviors and damage evolutions of MUTT and SPT were presented, followed by an application case illustrating the characterization of hydrogen embrittlement sensitivity based on MUTT and SPT. An inverse finite element modeling method of load–displacement curve reproduction was used to calibrate the variations of damage parameters of hydrogen-charged MUTT and SPT specimens. Hydrogen embrittlement (HE) indexes were determined by using different calculation methods. The results reveal that the HE sensitivity estimated by MUTT is higher than that measured by SPT, which is related to the different deformation processes and strain rates of the two testing methods. Full article

The mechanical properties of local materials subjected to various stress triaxialities were investigated via self-designed small punch tests and corresponding simulations, which were tailored to the geometry and notch forms of the samples. The finite element model was developed on the basis of the actual test method. After verifying the accuracy of the simulation, the stress, strain, and void volume fraction distributions of the Ti6Al4V titanium alloy under different stress states were compared and analyzed. The results indicate that the mechanical properties of the local material significantly differ during downward pressing depending on the geometric shape. A three-dimensional tensile stress state was observed in the center area, where the void volume fraction was greater than the fracture void volume fraction. The fracture morphology of the samples further confirmed the presence of different stress states. Specifically, the fracture morphology of the globular head samples (with or without U-shaped notches) predominantly featured dimples. Modifying the specimen’s geometry effectively increased stress triaxiality, facilitating the determination of the material’s constitutive relationship under varying stress states. Full article

This research used end-of-use cotton apparel to develop mulch mats, a type of agrotextiles. The researchers collected and sorted end-of-use garments to obtain cotton textile waste. These end-of-use garments were deconstructed to obtain shredded textiles and big pieces of textiles. Using the textiles from deconstructed end-of-use garments, together with a small amount of new cotton fibers, the researchers used a Feltloom to develop needle-punched nonwoven fabrics that can be used as mulch mats. The researchers tested textile properties of these mulch mats and conducted agricultural field tests for weed control and pot tests for biodegradation. The researchers also tested the mulch mats’ soil moisture infiltration, and impact on water evaporation. The nonwoven mulch mats made from end-of-use garments have excellent weed inhibition capability and biodegradability. Compared to plastic mulch sheet, the nonwoven mulch mats are better for water utilization in rainfall watering and sprinkle irrigation but poorer in water conservation in drip irrigation. Considering durability, biodegradability, and soil temperature regulation, it is recommended to use 100% cotton and felt four times to produce mulch mats from end-of-use garments. Full article

This comprehensive review examines the phenomena of stress corrosion cracking (SCC) and chloride-induced stress corrosion cracking (Cl-SCC) in materials commonly used in the oil and gas industry, with a focus on austenitic stainless steels. The study reveals that SCC initiation can occur at temperatures as low as 20 °C, while Cl-SCC propagation rates significantly increase above 60 °C, reaching up to 0.1 mm/day in environments with high chloride concentrations. Experimental methods such as Slow Strain Rate Tests (SSRTs), Small Punch Tests (SPTs), and Constant-Load Tests (CLTs) were employed to quantify the impacts of temperature, chloride concentration, and pH on SCC susceptibility. The results highlight the critical role of these factors in determining the susceptibility of materials to SCC. The review emphasizes the importance of implementing various mitigation strategies to prevent SCC, including the use of corrosion-resistant alloys, protective coatings, cathodic protection, and corrosion inhibitors. Additionally, regular monitoring using advanced sensor technologies capable of detecting early signs of SCC is crucial for preventing the onset of SCC. The study concludes with practical recommendations for enhancing infrastructure resilience through meticulous material selection, comprehensive environmental monitoring, and proactive maintenance strategies, aimed at safeguarding operational integrity and ensuring environmental compliance. The review underscores the significance of considering the interplay between mechanical stresses and corrosive environments in the selection and application of materials in the oil and gas industry. Low pH levels and high temperatures facilitate the rapid progression of SCC, with experimental results indicating that stainless steel forms passive films with more defects under these conditions, reducing corrosion resistance. This interplay highlights the need for a comprehensive understanding of the complex interactions between materials, environments, and mechanical stresses to ensure the long-term integrity of critical infrastructure. Full article

Threshold stress in aggressive environments is usually determined by tests under constant load, which are very time-consuming, so the incremental loading technique published in the ASTM F1624 standard was created to solve this issue. This approach has been recently applied to Small Punch tests, but it requires an optimization of the incremental step times, which is carried out in this work. Three medium- and high-strength quenched and tempered steels of 35, 50 and 60 HRC are exposed to three different cathodic polarization environments of 1, 5 and 10 mA/cm² in 1N H₂SO₄ acid electrolyte with a Platinum anode, studying in each case three different step durations of one-quarter, one-sixth and one-eighth of the ones indicated in ASTM F1624. Optimal step times for Small Punch tests are derived from this work as one-sixth of the ones recommended in ASTM F1624 for tensile specimens, which are 20 min and 40 min for steps 1–10 and 11–20, respectively, in the case of 33 ≤ HRC < 45 steels, 10 min and 20 min for steps 1–10, 11–20 in the case of 45 ≤ HRC < 55 steels, and 10 min for steps 1–20 in the case of HRC ≥ 55 steels. Full article

The combination of wrought materials and laser-based directed energy deposition (DED-LB) is being increasingly used for manufacturing new and repairing old or damaged components in several industries. Aerospace components made of Inconel 718 featuring small-thickness DED-LB buildups are a remarkable example of such a combination due to the high added value it brings. Despite that these are usually critical components, the miniature testing methods to assess the local mechanical properties in the buildup area are not fully developed. This work contributes to this miniature testing development with an improvement of the small punch testing (SPT) technique for measuring the mechanical properties of the weld line between the DED-LB and the wrought substrate. A new criterion for weld line positioning in the SPT specimens is proposed and applied on samples of hybrid wrought/DED-LB Inconel 718. The results of positioning the weld line at the necking site of the SPT specimen show that the proposed approach is valid for assessing the properties of the transition zone between the wrought and additive states. For the specific conditions tested and taking the wrought material as a reference, the strength of the Inconel 718 drops 10% in the weld line and 20% in the buildup. Full article

In this investigation, 0.19–1.8 wt.% of Ge was introduced into a ternary Zn-Mg-Al alloy. The introduction of Ge had a significant impact on the microstructure, leading to the formation of Mg₂Ge. The area fraction of the eutectic phase diminished with increasing Ge additions. Small-scale test techniques were utilised to evaluate the mechanical properties due to the changes in microstructure. Zn-Mg-Al alloys were found to be inherently harder compared to standard hot-dip Zn-containing 0.2 wt.% Al. The hardness and strength of the Zn-Mg-Al alloys decreased with the increase in Ge additions. Full article

The effects of the secondary processes of Hot Isostatic Pressing (HIP) at 920 °C and Heat Treatment (HT) at 1000 °C of Electron Beam-Melted (EBM) Ti–6Al–4V alloy on the microstructure and hydrogen embrittlement (HE) after electrochemical hydrogen charging (EC) were investigated. Comprehensive characterization, including microstructural analysis, X-ray diffraction (XRD), thermal desorption analysis, and mechanical testing, was conducted. After HIP, the β-phase morphology changed from discontinuous Widmanstätten to a more continuous structure, 10 times and ~1.5 times larger in length and width, respectively. Following HT, the β-phase morphology changed to a continuous “web-like” structure, ~4.5 times larger in width. Despite similar mechanical behavior in their non-hydrogenated state, the post-treated alloys exhibit increased susceptibility to HE due to enhanced hydrogen penetration into the bulk. It is shown that hydrogen content in the samples’ bulk is inversely dependent on surface hydride content. It is therefore concluded that the formed hydride surface layer is crucial for inhibiting further hydrogen penetration and adsorption into the bulk and thus for reducing HE susceptibility. The lack of a hydride surface layer in the samples subject to HIP and HT highlights the importance of choosing secondary treatment process parameters that will not increase the continuous β-phase morphology of EBM Ti–6Al–4V alloys in applications that involve electrochemical hydrogen environments. Full article

Reinforced concrete slabs are widely used in building structures due to their economic, durable, and aesthetic advantages. The determination of their ultimate strength often hinges on punching shear strength. Presently, methods such as closed hoops, steel bending, and fiber reinforcement are employed to enhance punching shear strength, with fiber reinforcement gaining popularity due to its ease of implementation and efficacy in improving concrete durability. This study introduces a novel approach employing six machine learning algorithms rooted in decision trees and decision tree-based ensemble learning to predict punching shear strength in steel fiber-reinforced concrete slabs. To overcome experimental data limitations, a data augmentation approach based on the Gaussian mixture model is employed. The validation of the data augmentation is conducted through “synthetic training—real testing” and “real training—real testing”. Additionally, the best machine learning model is analyzed for explainability using Shapley Additive exPlanation (SHAP). Results demonstrate that the proposed data augmentation method effectively captures the original data distribution, enhancing the robustness and accuracy of the machine learning model. Moreover, SHAP provides better insights into the features influencing punching shear strength. Thus, the proposed data enhancement model offers a reliable approach for modeling small experimental datasets in structural engineering. Full article

As a commonly used material in the petrochemical, nuclear and aerospace fields, Inconel 625 has excellent strength and corrosion resistance. The accurate evaluation of material properties with small specimen volume is of great significance to ensure in-service equipment safety. To realize reasonable estimations of tensile strength based on the small punch test, load–displacement and slope–displacement curves of Inconel 625 were discussed in this study. The results prove that the first inflexion point can be used in the yield strength analysis based on the empirical correlation method and plate bend theory. Meanwhile, the lowest point of the elastic and plastic deformation stages in the slope–displacement curves were compared. A new deformation energy method was established to realize yield strength estimations. To analyze the ultimate tensile strength, a small punch deformation feature was discussed based on the geometric deformation model and microstructure analysis. The relationship between stress and displacement was obtained. F_m/d_mt₀ was proven to be a more appropriate parameter in ultimate tensile strength estimations. Full article