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Keywords = enamel abrasion

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10 pages, 2820 KiB  
Article
Clinical and Technological Evaluation of the Remineralising Effect of Biomimetic Hydroxyapatite in a Population Aged 6 to 18 Years: A Randomized Clinical Trial
by Andrea Scribante, Saverio Cosola, Maurizio Pascadopoli, Annamaria Genovesi, Rebecca Andrea Battisti and Andrea Butera
Bioengineering 2025, 12(2), 152; https://doi.org/10.3390/bioengineering12020152 - 5 Feb 2025
Cited by 3 | Viewed by 2253
Abstract
The aim of this randomized clinical trial was to evaluate the efficacy of two different remineralising toothpastes in preventing dental caries and promoting oral health. Patients aged 6–18 years old with healthy and fully erupted first permanent molars (C1 and C2 DIAGNOdent scores) [...] Read more.
The aim of this randomized clinical trial was to evaluate the efficacy of two different remineralising toothpastes in preventing dental caries and promoting oral health. Patients aged 6–18 years old with healthy and fully erupted first permanent molars (C1 and C2 DIAGNOdent scores) were enrolled and randomized into two groups according to the home-hydroxyapatite-based remineralising treatment used: the Trial group used zinc carbonate hydroxyapatite-based treatment (Biorepair Total Protective Repair), while the Control group used magnesium strontium carbonate hydroxyapatite conjugated with chitosan toothpaste (Curasept Biosmalto Caries Abrasion & Erosion). Dental and periodontal parameters were measured over a six-month period, including the DIAGNOdent Pen Index (primary outcome), BEWE Index, Plaque Index, Bleeding Score, Schiff Air Index, and ICDAS assessed with DIAGNOcam. A total of 40 patients were equally allocated in the two groups and finally analyzed. A significant reduction in the DIAGNOdent Pen score was reported in the Trial group after 1 month of treatment, while in the Control group, no significant change was found. The Trial group also showed a significant reduction in plaque levels after 3 months of treatment, while in the Control group, it occurred after 1 month. However, the Bleeding Score and Schiff Air Index showed no significant differences between the groups, suggesting that additional measures may be required to address gingival inflammation and hypersensitivity. The ICDAS index also showed no statistically significant changes, due to the limited duration of this study. Overall, zinc-hydroxyapatite-based toothpaste was more effective than magnesium strontium carbonate hydroxyapatite toothpaste in enhancing enamel remineralisation in the short-term period. The assigned treatments did not result in significant improvements in the oral indexes assessed in this study. Full article
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18 pages, 4114 KiB  
Article
Effects of Five Different Toothpastes on Remineralization and Surface Roughness of Primary Tooth Enamel with Artificial Initial Caries
by Gokce Ozcan Altinsoy and Derya Ceyhan
Appl. Sci. 2024, 14(16), 7232; https://doi.org/10.3390/app14167232 - 16 Aug 2024
Cited by 1 | Viewed by 2765
Abstract
There are only a few studies about the effects of toothpastes for children on remineralization and surface roughness of primary teeth. The aim of this study was to examine the remineralization capacity of five different toothpastes for children on primary tooth enamels with [...] Read more.
There are only a few studies about the effects of toothpastes for children on remineralization and surface roughness of primary teeth. The aim of this study was to examine the remineralization capacity of five different toothpastes for children on primary tooth enamels with artificial initial caries, their effects on enamel surface roughness, and the relationship between their abrasive effects and remineralization. Sixty of 74 samples were allocated for microhardness and AFM analyses (after initialization, demineralization, and pH cycling), and 14 samples were evaluated by SEM. Sixty samples were divided into five groups, with each group representing a different toothpaste brand, as follows: Group 1: Splat; Group 2: Logodent; Group 3: Eyup Sabri Tuncer; Group 4: Naturalive; and Group 5: Buccotherm. Fourteen samples were divided into seven groups, each representing a different processing stage, with two samples in each group, for the initial (sound enamel surface) stage, post demineralization, and after applying the five remineralizing toothpastes. Toothpastes were applied to samples in a 7-day pH cycle. Data were analyzed statistically. Each toothpaste showed increased microhardness values; however, this increase was significant only for Group 4 (Naturalive) and Group 5 (Buccotherm). The highest surface roughness values were obtained after demineralization. The toothpastes reduced surface roughness, but these reductions were not statistically significant among the different types of toothpastes. The correlation analysis revealed that the toothpastes affected surface roughness according to their remineralization potential. The results were supported by SEM images. All toothpastes recovered primary tooth enamels with artificial initial caries, but only two had significant values. Full article
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18 pages, 9203 KiB  
Article
A Comparative Analysis of Enamel Surface Roughness Following Various Interproximal Reduction Techniques: An Examination Using Scanning Electron Microscopy and Atomic Force Microscopy
by Dan-Cosmin Serbanoiu, Aurel-Claudiu Vartolomei, Dana-Valentina Ghiga, Marioara Moldovan, Codruta Sarosi, Ioan Petean, Marie-Jose Boileau and Mariana Pacurar
Biomedicines 2024, 12(8), 1629; https://doi.org/10.3390/biomedicines12081629 - 23 Jul 2024
Cited by 2 | Viewed by 1830
Abstract
Interproximal enamel reduction (IER) is a minimally invasive therapeutic procedure commonly used in orthodontics to address both functional and aesthetic issues. Its mechanical effects on enamel surfaces induce the formation of grooves, furrows, scratches, depressions, and valleys. The aim of this study was [...] Read more.
Interproximal enamel reduction (IER) is a minimally invasive therapeutic procedure commonly used in orthodontics to address both functional and aesthetic issues. Its mechanical effects on enamel surfaces induce the formation of grooves, furrows, scratches, depressions, and valleys. The aim of this study was to assess the enamel surface roughness resulting after the application of currently available methods for interproximal reduction. Ninety freshly extracted human teeth were divided into six groups and subjected to the stripping procedure, using a different method for each group (diamond burs, abrasive strips of 90 μm, 60 μm, 40 μm, 15 μm, and abrasive discs). A single individual performed stripping according to the manufacturer’s recommendations, involving interproximal reduction on one tooth’s proximal face and leaving the other side untreated. Qualitative and quantitative assessment of the enamel surfaces was carried out using Scanning Electron Microscopy (SEM) and Atomic Force Microscopy (AFM), obtaining 2D and volumetric 3D images of the enamel surface microstructure and nanostructure. The study found that diamond burs and abrasive strips of 60 μm and 90 μm increased enamel roughness due to intense de-structuring effects, while the 40 μm polisher had a gentler effect and 15 μm abrasive strips and polishing discs preserved enamel surface quality and removed natural wear traces. Full article
(This article belongs to the Section Molecular and Translational Medicine)
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12 pages, 905 KiB  
Article
Comparative Evaluation of Dental Enamel Microhardness Following Various Methods of Interproximal Reduction: A Vickers Hardness Tester Investigation
by Dan-Cosmin Serbanoiu, Aurel-Claudiu Vartolomei, Dana-Valentina Ghiga, Silvia Izabella Pop, Irinel Panainte, Marioara Moldovan, Codruta Sarosi, Ioan Petean, Marie-Jose Boileau and Mariana Pacurar
Biomedicines 2024, 12(5), 1132; https://doi.org/10.3390/biomedicines12051132 - 20 May 2024
Cited by 3 | Viewed by 2610
Abstract
Interproximal enamel reduction, also known as stripping, is a common orthodontic procedure that reduces the mesiodistal diameter of teeth, allowing for a balance of available space in dental arches. The aim of this study was to assess the enamel surface microhardness resulting from [...] Read more.
Interproximal enamel reduction, also known as stripping, is a common orthodontic procedure that reduces the mesiodistal diameter of teeth, allowing for a balance of available space in dental arches. The aim of this study was to assess the enamel surface microhardness resulting from the application of currently available methods for interproximal reduction. Forty-two extracted human permanent teeth were divided into six different groups, each subjected to a therapeutic stripping procedure using various methods (i.e., diamond burs, abrasive strips of 90 μm, 60 μm, 40 μm, and 15 μm, and abrasive discs). Stripping was performed by a single individual in accordance with the manufacturers’ recommendations for the various systems used. One of the proximal faces of the tooth underwent IPR, while the other side remained untreated for control. The hardness of the enamel surface was measured using a Vickers hardness tester. The control group achieved the hardest enamel surface (354.4 ± 41.02 HV1), while the lowest was observed for enamel surfaces treated with 90 µm abrasive strips (213.7 ± 118.6). The only statistically significant difference was identified in comparisons between the values measured for the control group and those obtained after stripping with diamond burs (p = 0.0159). Enamel microhardness varied depending on the stripping instrument used, but no statistically significant differences were found (p > 0.05). Optimal microhardness values, close to those of healthy enamel, were achieved after mechanical treatment with 15 µm abrasive strips and abrasive discs. Dental stripping is a safe therapeutic procedure that has a relatively minor influence on the microhardness of surface enamel. Full article
(This article belongs to the Section Molecular and Translational Medicine)
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18 pages, 3453 KiB  
Article
Dynamics of Dental Enamel Surface Remineralization under the Action of Toothpastes with Substituted Hydroxyapatite and Birch Extract
by Cristina Teodora Dobrota, Alexandra-Diana Florea, Csaba-Pal Racz, Gheorghe Tomoaia, Olga Soritau, Alexandra Avram, Horea-Rares-Ciprian Benea, Cristina Lavinia Rosoiu, Aurora Mocanu, Sorin Riga, Attila-Zsolt Kun and Maria Tomoaia-Cotisel
Materials 2024, 17(9), 2038; https://doi.org/10.3390/ma17092038 - 26 Apr 2024
Viewed by 1596
Abstract
To address tooth enamel demineralization resulting from factors such as acid erosion, abrasion, and chronic illness treatments, it is important to develop effective daily dental care products promoting enamel preservation and surface remineralization. This study focused on formulating four toothpastes, each containing calcined [...] Read more.
To address tooth enamel demineralization resulting from factors such as acid erosion, abrasion, and chronic illness treatments, it is important to develop effective daily dental care products promoting enamel preservation and surface remineralization. This study focused on formulating four toothpastes, each containing calcined synthetic hydroxyapatite (HAP) in distinct compositions, each at 4%, along with 1.3% birch extract. Substitution elements were introduced within the HAP structure to enhance enamel remineralization. The efficacy of each toothpaste formulation was evaluated for repairing enamel and for establishing the dynamic of the remineralization. This was performed by using an in vitro assessment of artificially demineralized enamel slices. The structural HAP features explored by XRD and enamel surface quality by AFM revealed notable restorative properties of these toothpastes. Topographic images and the self-assembly of HAP nanoparticles into thin films on enamel surfaces showcased the formulations’ effectiveness. Surface roughness was evaluated through statistical analysis using one-way ANOVA followed by post-test Bonferroni’s multiple comparison test with a p value < 0.05 significance setting. Remarkably, enamel nanostructure normalization was observed within a short 10-day period of toothpaste treatment. Optimal remineralization for all toothpastes was reached after about 30 days of treatment. These toothpastes containing birch extract also have a dual function of mineralizing enamel while simultaneously promoting enamel health and restoration. Full article
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15 pages, 3463 KiB  
Article
Effects of Different Toothpastes on the Nanomechanical Properties and Chemical Composition of Resin-Modified Glass Ionomer Cement and Composite Resin Restorations
by Mariana Dias Moda, Paulo Henrique Dos Santos, Nubia Inocencya Pavesi Pini, Leonardo Negri Furini, André Luiz Fraga Briso, André Assmann and Ticiane Cestari Fagundes
Dent. J. 2023, 11(7), 173; https://doi.org/10.3390/dj11070173 - 17 Jul 2023
Cited by 3 | Viewed by 2153
Abstract
Purpose: This study evaluates the effects of different toothpastes on the nanohardness and chemical compositions of restorative materials and dental surfaces. Methods: Bovine enamel (n = 72) and dentin (n = 72) blocks were obtained and restored using RMGIC (n [...] Read more.
Purpose: This study evaluates the effects of different toothpastes on the nanohardness and chemical compositions of restorative materials and dental surfaces. Methods: Bovine enamel (n = 72) and dentin (n = 72) blocks were obtained and restored using RMGIC (n = 36) or CR (n = 36) to create the following surfaces: dentin adjacent to RMGIC (DRMGIC), enamel adjacent to RMGIC (ERMGIC), dentin adjacent to CR (DCR), and enamel adjacent to CR (ECR). After restoration, one hemiface of each specimen was coated with an acid-resistant varnish to facilitate the creation of control (C) and eroded (E) sides; the latter were achieved by erosion–abrasion cycles as follows: erosion with 1% citric acid: 5 days, four times for 2 min each day; 1% citric acid/abrasion, two times for 15 s, followed by immersion in a toothpaste slurry for 2 min. Toothpastes without fluoride (WF; n = 12), with sodium fluoride (NaF; n = 12), and with stannous fluoride (SnF2; n = 12) were used for RMGIC or CR. The specimens were analyzed for nanohardness (H), and chemical composition using energy-dispersive X-ray spectroscopy and Raman microscopy. The data were statistically analyzed using two-way repeated measures ANOVA and Tukey’s test (α = 0.05). Results: Lower H values were obtained with NaF for DRMGIC-C, with a statistically significant difference from the H value obtained with WF (p < 0.05). The calcium and phosphorus concentrations in DCR-E were significantly lower with WF than with the other types of toothpaste (p < 0.05). Fluoride-containing toothpastes are capable of preserving the main chemical components of the dentin adjacent to the restorative materials under erosive–abrasive conditions. Full article
(This article belongs to the Special Issue Preventive Dental Care, Chairside and Beyond)
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13 pages, 932 KiB  
Review
Conservative Treatment of Dental Non-Carious Cervical Lesions: A Scoping Review
by Assunta Patano, Giuseppina Malcangi, Matteo De Santis, Roberta Morolla, Vito Settanni, Fabio Piras, Alessio Danilo Inchingolo, Antonio Mancini, Francesco Inchingolo, Gianna Dipalma and Angelo Michele Inchingolo
Biomedicines 2023, 11(6), 1530; https://doi.org/10.3390/biomedicines11061530 - 25 May 2023
Cited by 24 | Viewed by 6701
Abstract
This scoping review aims to evaluate methods of conservative reconstruction of dental enamel lesions resulting from abrasions and evaluate the effect of diode laser in reducing the symptoms of tooth sensitivity. The cementoenamel junction is more prone to substance loss because the enamel [...] Read more.
This scoping review aims to evaluate methods of conservative reconstruction of dental enamel lesions resulting from abrasions and evaluate the effect of diode laser in reducing the symptoms of tooth sensitivity. The cementoenamel junction is more prone to substance loss because the enamel thickness is substantially decreased, resulting in a much weaker enamel–dentin bond. Methods: Dental abrasion was examined in the mechanical cause alone. Pubmed, Scopus, and Web of Science were used to discover publications that matched our topic from 1 January 2018 to 20 March 2023. A comparison of various non-carious cervical lesion (NCCL) restoration treatments was generated mostly by mechanical considerations. Results: A final number of 11 clinical trials and randomized controlled trials were included in the review for qualitative analysis. Composite resins performed well in clinical trials for the restoration of NCCLs. Conclusions: Composite, in its different forms of filling and consistency, preceded by the use of adhesives, is an efficient and effective material for the treatment of NCCLs. Diode laser use prior to NCCL restoration of teeth does not diminish restoration retention rate, may lessen hypersensitivity, and may affect restoration success. Full article
(This article belongs to the Section Biomedical Engineering and Materials)
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14 pages, 7286 KiB  
Article
Tribological Behaviour of Enamel Coatings Created by a Prototype Device for Local Repair of Inorganic Surfaces
by Miroslav Müller, Monika Hromasová, Petr Valášek, Iva Nováková, Jaromír Moravec and Milan Jelínek
Materials 2023, 16(3), 1224; https://doi.org/10.3390/ma16031224 - 31 Jan 2023
Cited by 2 | Viewed by 1587
Abstract
The ability of materials to withstand environmental influences is a frequent necessity in many industries. Special requirements are imposed by such industries where surfaces are affected by acidity during the processing or storage of products. In such cases, when the basic surface is [...] Read more.
The ability of materials to withstand environmental influences is a frequent necessity in many industries. Special requirements are imposed by such industries where surfaces are affected by acidity during the processing or storage of products. In such cases, when the basic surface is exposed to chemical influences, it is possible to use enamel coatings, which, with their properties, guarantee the protection of the surface and achieve the required service life of the material. This article deals mainly with the interaction between the base material and the enamel and its resistance to wear between the original and the renovated surface caused by local heating. The article presents a methodical procedure for the preparation of test specimens with an enamel layer prepared by AWJ cutting, eliminating its damage. There are minimal differences in the microstructure between the original and the renovated surface due to the production technique. The renovated enamel surface had more bubbles of a larger size than the original surface. Good adhesion between the base metal material (substrate) and the ground coat was demonstrated. The tested surfaces demonstrated high resistance to intensive abrasion conditions with low linear wear increments. Full article
(This article belongs to the Special Issue Organic Matrix Composites and Multifunctional Materials)
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12 pages, 4233 KiB  
Article
Glass-Ceramic Protective Coatings Based on Metallurgical Slag
by Alexander V. Gorokhovsky, Gleb Yu. Yurkov, Igor N. Burmistrov, Angel F. Villalpando-Reyna, Denis V. Kuznetsov, Alexander A. Gusev, Bekzod B. Khaidarov, Yuri V. Konyukhov, Olga V. Zakharova and Nikolay V. Kiselev
Coatings 2023, 13(2), 269; https://doi.org/10.3390/coatings13020269 - 24 Jan 2023
Cited by 5 | Viewed by 3338
Abstract
Pyroxene glass-ceramic enamels based on combinations of blast furnace slag and some additives were produced and investigated. The batch compositions and technological regimes of enameling were developed to produce high temperature protective coatings for carbon steel (ASTM 1010/1008). The composition of raw materials [...] Read more.
Pyroxene glass-ceramic enamels based on combinations of blast furnace slag and some additives were produced and investigated. The batch compositions and technological regimes of enameling were developed to produce high temperature protective coatings for carbon steel (ASTM 1010/1008). The composition of raw materials was selected to match the values of the thermal expansion coefficients of the glass-ceramic coating (~11∙10−6 K−1) and metal substrate (~12∙10−6 K−1) taking into account the temperatures of fluidization (Tf ~ 800°) and crystallization (Tc = 850−1020 °C) of the corresponding glasses. The covered and thermally treated samples of carbon steel were produced using single-layer enameling technology and investigated to specify structure, phase composition and properties of the coating and coating-steel interface. The obtained coatings were characterized with excellent adhesion to the steel (impact energy ~3 J) and protective properties. The closed porous structure of the coatings promoted low thermal conductivity (~1 W/(m·K)) and high (up to 1000 °C) thermal resistance, whereas the pyroxene-like crystalline phases supported high wear and chemical resistance as well as micro-hardness (~480 MPa) and thermal shock resistance (>30 cycles of 23–700 °C). The obtained cheap coatings and effective protective coatings could be used at the temperatures up to 1100 °C in the corrosive atmosphere and under the action of abrasive particles. Full article
(This article belongs to the Special Issue Ceramic Films and Coatings: Properties and Applications)
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10 pages, 2705 KiB  
Article
Excessive Dental Bleaching with 22% Carbamide Peroxide Combined with Erosive and Abrasive Challenges: New Insights into the Morphology and Surface Properties of Enamel
by Edson de Sousa Barros Júnior, Mara Eliane Soares Ribeiro, Rafael Rodrigues Lima, Mário Honorato da Silva e Souza Júnior and Sandro Cordeiro Loretto
Materials 2022, 15(21), 7496; https://doi.org/10.3390/ma15217496 - 26 Oct 2022
Cited by 9 | Viewed by 2187
Abstract
This study aimed to evaluate the effects of 22% carbamide peroxide combined with an erosive challenge and simulated brushing on enamel. Bovine incisor teeth were divided into G1, tooth bleaching; G2, tooth bleaching + erosive challenge; and G3, tooth bleaching + erosive challenge [...] Read more.
This study aimed to evaluate the effects of 22% carbamide peroxide combined with an erosive challenge and simulated brushing on enamel. Bovine incisor teeth were divided into G1, tooth bleaching; G2, tooth bleaching + erosive challenge; and G3, tooth bleaching + erosive challenge + simulated brushing, and evaluated at T0, before any intervention; T1, 14 days after the proposed treatments; and T2, 28 days after the proposed treatments. Tooth bleaching was performed daily for 1 h for 28 days. The microhardness, surface roughness, mass variation, and ultrastructure were analyzed at T0, T1, and T2. Two-way analysis of variance for repeated measures was performed and Tukey’s post hoc test (α = 5%) was used. The surface roughness increased in groups G2 and G3 as a function of time, whereas microhardness and mass measurements demonstrated a significant reduction for groups associated with challenges. Ultrastructural evaluation indicated a loss of the aprismatic layer and exposure of the enamel prisms in all groups after 14 days of bleaching, with more pronounced results in G2 and G3 after 28 days. In conclusion, abrasive and erosive challenges potentiated the deleterious effects of tooth whitening on microhardness, ultramorphology, and mass, without affecting the roughness of dental enamel. Full article
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11 pages, 3026 KiB  
Article
Evaluation of Bioactive Glass and Low Viscosity Resin as Orthodontic Enamel Sealer: An In Vitro Study
by Abdullah Al Shehab, Ahmed Samir Bakry, Robert Hill, Fahad Faiz Alsulaimani and Mona Aly Abbassy
J. Funct. Biomater. 2022, 13(4), 191; https://doi.org/10.3390/jfb13040191 - 17 Oct 2022
Cited by 7 | Viewed by 2206
Abstract
The study aimed to evaluate the effect of applying fluoride bioactive glass (FBAG) and Alpha-Glaze® (resin sealer) on the shear bond strength of orthodontic brackets to enamel bonded by Transbond XT, brushing–abrasion durability, and their protective effect against simulated cariogenic acidic attack. [...] Read more.
The study aimed to evaluate the effect of applying fluoride bioactive glass (FBAG) and Alpha-Glaze® (resin sealer) on the shear bond strength of orthodontic brackets to enamel bonded by Transbond XT, brushing–abrasion durability, and their protective effect against simulated cariogenic acidic attack. Materials include 135 extracted premolars that were divided into three groups—FBAG, Alpha-Glaze, and control. The shear bond strength test was measured using an Instron Universal Testing Machine. The brushing abrasion challenge took place with a tooth-brushing simulator. Transmitted light microscopy examinations were performed after the specimens were demineralized for 4 days. The results show that the shear bond strength values of the three groups did not report any statistically significant differences: FBAG (28.1 ± 5.5 Mpa), Alpha-Glaze (32.5 ± 7.4 Mpa), and control (30.7 ± 6.5 Mpa) p < 0.05. The Adhesive Remenant Index (ARI) study showed chipping of enamel in 6.6% of Alpha-Glaze and control specimens and 40% of specimens had their enamel surface covered with resin. Furthermore, 30% of the FBAG and 100% of the Alpha-Glaze sealer specimens resisted the abrasion test. In conclusion, FBAG can serve as an orthodontic-sealer capable of protecting the enamel surface surrounding orthodontic brackets. However, the Alpha-Glaze sealer did not offer the capability of protecting the enamel. Full article
(This article belongs to the Section Dental Biomaterials)
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13 pages, 2997 KiB  
Article
Effect of Whitening Toothpaste on Surface Roughness and Colour Alteration of Artificially Extrinsic Stained Human Enamel: In Vitro Study
by Sarat Suriyasangpetch, Pimduean Sivavong, Boondarick Niyatiwatchanchai, Thanaphum Osathanon, Puliwan Gorwong, Chawalid Pianmee and Dusit Nantanapiboon
Dent. J. 2022, 10(10), 191; https://doi.org/10.3390/dj10100191 - 13 Oct 2022
Cited by 15 | Viewed by 5243
Abstract
Objective: The aim of this study was to compare five toothpastes in terms of alteration of surface roughness and colour of red-wine-stained human enamel over time after brushing simulation. Methods: Stained specimens were randomly divided into five groups (n = 8): Oral-B [...] Read more.
Objective: The aim of this study was to compare five toothpastes in terms of alteration of surface roughness and colour of red-wine-stained human enamel over time after brushing simulation. Methods: Stained specimens were randomly divided into five groups (n = 8): Oral-B Gum and Enamel (C), ZACT Stain Fighter (ZW), Colgate Optic White Volcanic Mineral (CW), Oral-B 3D White Luxe Fresh Breath (3DW), and Thepthai (TW). The colour and surface roughness of the specimens were measured after brushing simulation for four durations; two weeks, one month, six months, and twelve months. Abrasive particles in toothpaste were inspected under a scanning electron microscope. Results: Surface roughness was increased in the specimens that underwent brushing simulation in all groups (p < 0.05). ZW (6.33 ± 0.98 μm) exerted the most changes in surface roughness for all durations. Other groups showed similar surface roughness at each time point. ΔE00 and ΔL were increased in all groups until twelve months; however, there were no significant differences between C (ΔE00 = 30.17 ± 4.16, ΔL = 38.19 ± 4.34), CW (ΔE00 = 24.25 ± 10.52, ΔL = 31.12 ± 11.00), and TW (ΔE00 = 29.00 ± 3.96, ΔL = 36.68 ± 4.53) at any time period. Moreover, ZW (ΔE00 = 45.6 ± 8.01, ΔL = 53.03 ± 6.71) and 3DW (ΔE00 = 43.6 ± 7.33, ΔL = 51.03 ± 6.47) exhibited a substantial change and were statistically differed from the other groups after four-weeks. Various characteristics of abrasive particles were inspected under SEM. Conclusion: All five toothpastes increased the surface roughness altered the colour of red wine-stained human enamel over time. Full article
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12 pages, 5592 KiB  
Article
Xylitol Fluoride Varnish: In Vitro Effect Analysis on Enamel by Atomic Force Microscopy
by Catalina Iulia Saveanu, Oana Dragos, Daniela Anistoroaei, Livia Ionela Bobu, Alexandra Ecaterina Saveanu, Adina Armencia, Sorina Mihaela Solomon and Oana Tanculescu
Biomedicines 2022, 10(8), 1900; https://doi.org/10.3390/biomedicines10081900 - 5 Aug 2022
Cited by 2 | Viewed by 2564
Abstract
(1) Background: Numerous studies have shown the beneficial role of fluoride in the primary prevention of dental caries. The aim of the present study was to put into evidence the change in the enamel structure immediately after the application of a fluoride varnish. [...] Read more.
(1) Background: Numerous studies have shown the beneficial role of fluoride in the primary prevention of dental caries. The aim of the present study was to put into evidence the change in the enamel structure immediately after the application of a fluoride varnish. (2) Methods: A xylitol–fluoride varnish was evaluated. The enamel specimens (n = 10) were analyzed by atomic force microscopy on enamel surface and treatment with fluoride varnish applied. The dimensional topographic analysis was performed by 2D and 3D analysis software. Statistical analysis was performed using SPSS Version 26.00 (IBM, Armonk, NY, USA). A one-sample statistics test was used to identify significant differences (p < 0.05). (3) Results: Surface roughness (Ra) measurements ranged from Ra = 0.039 μm (±0.048), to Ra = 0.049 μm (±0.031), respectively (p < 0.05), with an increase in the surface roughness passing from the intact enamel to the enamel exposed to fluoride varnish. When comparing Ra values of the nonfluorinated enamel and fluorinated enamel, significant differences (p < 0.05) were found, suggesting that the varnish had a protective effect on the enamel surface. (4) Conclusions: Xylitol–fluoride varnish, even in one single short-time application, is effective in reducing the surface roughness of enamel structure exposed to abrasion, thus increasing resistance to dental caries. Full article
(This article belongs to the Section Biomedical Engineering and Materials)
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16 pages, 4426 KiB  
Article
Human Enamel Fluorination Enhancement by Photodynamic Laser Treatment
by Corina Elena Tisler, Marioara Moldovan, Ioan Petean, Smaranda Dana Buduru, Doina Prodan, Codruta Sarosi, Daniel-Corneliu Leucuţa, Radu Chifor, Mîndra Eugenia Badea and Razvan Ene
Polymers 2022, 14(14), 2969; https://doi.org/10.3390/polym14142969 - 21 Jul 2022
Cited by 14 | Viewed by 2191
Abstract
Poor oral hygiene leads to serious damages of theteeth’s surface enamel such as micro-abrasions and acid erosion. These alterations combined with bacterial plaque result in cavity appearance. Prophylactic measures include various techniques for enamel surface restoration. Fluorination is one of the most important [...] Read more.
Poor oral hygiene leads to serious damages of theteeth’s surface enamel such as micro-abrasions and acid erosion. These alterations combined with bacterial plaque result in cavity appearance. Prophylactic measures include various techniques for enamel surface restoration. Fluorination is one of the most important treatments for this purpose. Therefore, in the present research, we investigated the classical fluorination treatment compared with laser photodynamic fluorination performed on human enamel samples with poor surface quality. Three sample groups were investigated: veneer (F), inlay (I), and crowns (C). The general morphologic aspect was investigated by scanning electron microscopy (SEM), and the specific details such as the fine microstructure and nanostructure were investigated by atomic force microscopy (AFM) of the surface roughness. The samples were also investigated by Fourier transformed infrared attenuated total reflectance (FTIR-ATR) to evidence the fluorination effect on the enamel surface. Results showed that all initial samples had an altered state with micro-abrasions and erosion with mineral loss, which increase the surface roughness. The F group was the most damaged, having a higher roughness, and the I group was less damaged. Classic fluorination treatment partially restored the enamel by local re-mineralization, but did not obtain the parameters of healthy enamel. However, a significant decrease of the roughness was observed (statistical relevance p = 0.001 with the Breusch–Pagan Test). This fact was supported by the presence of newly formed fluorides in the FTIR-ATR spectra. The photodynamic laser fluorination restores the enamel in an enhanced manner by a strong re-mineralization, which implies a significant roughness value decrease comparable to healthy enamel. The Breusch–Pagan Test confirmed the relevance with p = 0.001. This is due to an extended re-mineralization abundant in fluoride crystals as observed by AFM and FTIR. Statistical p-values regarding laser application were in the range of 0.02–0.06, supporting its relevance in the fluorination effect. The final conclusion is that the photodynamic effect is able to favor the newly formed fluoride deposition onto the affected sites of the enamel surface. Full article
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12 pages, 841 KiB  
Article
Fractographic and Microhardness Evaluation of All-Ceramic Hot-Pressed and CAD/CAM Restorations after Hydrothermal Aging
by Roxana Diana Vasiliu, Ion-Dragoș Uțu, Lucian Rusu, Adrian Boloș and Liliana Porojan
Materials 2022, 15(11), 3987; https://doi.org/10.3390/ma15113987 - 3 Jun 2022
Cited by 6 | Viewed by 1848
Abstract
All-ceramic dental restorations have great advantages, such as highly esthetical properties, a less complex fabrication, and a similar abrasion resistance to enamel. Despite these advantages, ceramic materials are more prone to fracture due to their brittle microstructure. The main aim of this in [...] Read more.
All-ceramic dental restorations have great advantages, such as highly esthetical properties, a less complex fabrication, and a similar abrasion resistance to enamel. Despite these advantages, ceramic materials are more prone to fracture due to their brittle microstructure. The main aim of this in vitro study was to determine the difference in hot-pressed and milled glass-ceramic mechanical properties such as fracture resistance and microhardness (VHN). Four types of ceramics, two hot-pressed and two milled, feldspathic glass-ceramics and zirconia-reinforced glass-ceramics were selected in this study and tested using the static loading test and Vicker’s testing. Hydrothermal aging, consisting of different baths with temperatures between 5 degrees Celsius and 55 degrees Celsius, was chosen as the in vitro aging method. Statistical analyses are performed using SPSS Statistics software at a significance level of p < 0.05. Micro-hardness values decrease after hydrothermal aging. The static loading test reveals a significant difference between the feldspathic hot-pressed glass-ceramic, which fractures at lower forces, and milled zirconia-reinforced lithium silicate glass-ceramic, which fractures at greater forces (N). Fractographic analysis of the fractured fragments resulted in the static loading test revealing different surface features about the crack origins and propagations under a stereomicroscope. Full article
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