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Separations, Volume 11, Issue 3

2024 March - 25 articles

Cover Story: A recent study has made progress in biodiesel production by implementing continuous column extraction. This method utilizes a deep eutectic solvent (DES) to extract glycerol from biodiesel made from waste cooking oils. A focal point of the study was the use of a laboratory Karr column, where variations in mixing intensities and DES to biodiesel mass ratios were explored. The efficiency of this process was influenced by the choice of plate material and geometry, with steel plates exhibiting superior results compared to PETG plates. This was further confirmed through contact angle measurements and an array of analytical techniques. The study's findings provide insights into biodiesel production, emphasizing the importance of process optimization in pursuing environmentally sustainable energy solutions. View this paper
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Articles (25)

  • Brief Report
  • Open Access
3 Citations
3,510 Views
9 Pages

Tofacitinib citrate (RR-isomer) is a janus kinase (JAK) inhibitor approved for the treatment of rheumatoid arthritis (RA) in adults who have had an inadequate response or intolerance to methotrexate. The presence of the enantiomer of tofacitinib citr...

  • Article
  • Open Access
3 Citations
3,084 Views
17 Pages

Chemical composition is a critical factor for determining the efficacy of any traditional Chinese medicine (TCM) and can be used as an indicator of commercial quality. To develop a new strategy for discovering potential quality markers (Q-markers) of...

  • Article
  • Open Access
3 Citations
2,935 Views
12 Pages

Xuetong, the dried stem of Kadsura heteroclita (Roxb.) Craib, is a traditional Tujia medicine extensively used to treat rheumatoid arthritis (RA). All traditional Chinese medicines (TCMs) necessitate a processing stage called “Paozhi” bef...

  • Article
  • Open Access
5 Citations
2,972 Views
17 Pages

The Phosphorus Adsorption and Recovery of Mg/Fe-LDHs Mulberry Rod Biochar Composite

  • Meina Liang,
  • Zimeng Wu,
  • Haiyan Cao,
  • Kun Dong,
  • Shaoyuan Bai and
  • Dunqiu Wang

Mg/Fe layered bimetallic oxide mulberry rod biochar composites (MFBCs) were prepared from mulberry rods and characterized using electron microscopy scanning (SEM), X-ray diffraction (XRD), Fourier infrared spectroscopy (FT-IR), and X-ray photoelectro...

  • Article
  • Open Access
2 Citations
8,072 Views
17 Pages

Chemical Characterization of Human Body Odor Headspace Components

  • A. Celeste Medrano,
  • Ariela Cantu,
  • Edgar O. Aviles-Rosa,
  • Nathaniel J. Hall,
  • Michele N. Maughan,
  • Jenna D. Gadberry and
  • Paola A. Prada-Tiedemann

This study focused on evaluating human body odor volatiles using a chamber approach. Ten participants were asked to sit inside the chamber for 1 h, while using SPME as the extraction technique for vapor sampling. A total of 105 compounds were detecte...

  • Article
  • Open Access
1 Citations
3,722 Views
19 Pages

Evaluation of Carbonized Corncobs for Removal of Microcystins and Nodularin-R from Water

  • Hasaruwani S. Kiridena,
  • Sharmila I. Thenuwara,
  • Manjula M. Kandage,
  • Norman Peiffer,
  • Michal Marszewski and
  • Dragan Isailovic

Microcystins (MCs) and nodularins (NODs) are cyanotoxins that can be found in water bodies during cyanobacterial harmful algal blooms (cyanoHABs). Consumption of water contaminated with cyanotoxins leads to health risks for humans and animals. Herein...

  • Article
  • Open Access
13 Citations
3,520 Views
13 Pages

A sustainable reversed-phase chromatographic method has been developed and validated for the simultaneous determination of three active pharmaceutical ingredients, dorzolamide, brinzolamide, and timolol, used to treat glaucoma. The eco-friendly solve...

  • Article
  • Open Access
3,383 Views
12 Pages

Unveiling Novel Chaotropic Chromatography Method for Determination of Pralidoxime in Nerve Agent Antidote Autoinjectors

  • Bohyun Shin,
  • Hyung-seung Kim,
  • Ji-Youn Lee,
  • Sumin Seo,
  • Cho Hee Jeong,
  • Eunbin Bae,
  • Jiyu Kim,
  • Hyojeong Lee,
  • Donghee Lee and
  • Sang Beom Han
  • + 1 author

Pralidoxime chloride, a highly hydrophilic antidote, cannot be effectively separated by reverse-phase high-performance liquid chromatography (RP-HPLC), unless the mobile-phase composition is varied. However, the use of ion-pairing reagents for pralid...

  • Article
  • Open Access
8 Citations
2,735 Views
14 Pages

A Sustainable Approach for Enhancing Stability and Bioactivity of Allium ursinum Extract for Food Additive Applications

  • Alena Stupar,
  • Senka Vidović,
  • Jelena Vladić,
  • Tanja Radusin and
  • Aleksandra Mišan

Utilizing natural plant extracts as food additives represents a promising strategy for enhancing the quality, nutritional value, and safety of food products, benefiting both consumers and the environment. Therefore, the primary objective of this stud...

  • Review
  • Open Access
16 Citations
5,628 Views
21 Pages

Water pollution poses a global threat to human health, particularly in terms of ensuring a safe supply of drinking water. The accumulation of heavy metals from various water sources is increasing, driving the search for effective and environmentally...

  • Article
  • Open Access
11 Citations
2,918 Views
14 Pages

This study investigates lyocell-based activated carbon fibers (ACFs) for their suitability in adsorbing and electrochemically detecting toxic HCl gas. ACFs were prepared via steam activation, varying temperature (800–900 °C) and time (40&nd...

  • Article
  • Open Access
7 Citations
3,189 Views
15 Pages

Comparison of Acid- and Base-Modified Biochar Derived from Douglas Fir for Removal of Copper (II) from Wastewater

  • Beatrice Arwenyo,
  • Prashan M. Rodrigo,
  • Olalekan A. Olabode,
  • Hashani P. Abeysinghe,
  • Jessie N. Tisdale,
  • Rose C. Azuba and
  • Todd E. Mlsna

Copper is a non-biodegradable heavy metal, and high levels in water bodies cause serious environmental and health issues. Douglas fir biochar has a higher number of carboxylic, phenolic, and lactonic groups, which provide suitable active sites for co...

  • Article
  • Open Access
3 Citations
2,798 Views
17 Pages

Construction of High-Activity Nano-NiTiO3/g-C3N4 Composite Catalysts for Enhanced Photodegradation Activities under Visible Light

  • Da Li,
  • Zhan Yang,
  • Kun Wang,
  • Lan Zhang,
  • Linglong Shi,
  • Abdul Qadeer,
  • Jiao Dong and
  • Haoyu Ren

Nickel titanate (NiTiO3) semiconductors and graphitic carbon nitride (g-C3N4) have attracted great attention as photocatalysts in the degradation of environmental pollutants because of their visible-light-driven activity. But the utilizations of both...

  • Article
  • Open Access
1 Citations
5,047 Views
14 Pages

Pharmaceutical Screening of Bat Feces and Their Applications and Risks in Traditional Chinese Medicine

  • Kou-Toung Chung,
  • Ching-Lung Lin,
  • Wu-Chang Chuang,
  • Ming-Chung Lee,
  • Li-Wen Chen and
  • Chung-Hsin Wu

Bat feces have been reported in traditional Chinese medicine (TCM) books to have the effect of reducing fever and improving eyesight, but the mechanism of vision improvement still needs further research. To this end, we used 2,2-diphenyl-1-picrylhydr...

  • Article
  • Open Access
2 Citations
2,966 Views
15 Pages

A liposome vesicle is an ideal carrier for carbon nanotubes (CNTs) serving as the water channel that allows for the fast transport of water molecules, thus enhancing membrane permeability. However, a low quantity of CNTs inserted into the liposome ve...

  • Article
  • Open Access
1 Citations
3,229 Views
20 Pages

Mechanism of Alleviating Acute Lung Injury in Mice from Serum Metabolomics Analysis of Cordyceps fumosorosea

  • Tahir Khan,
  • Jinna Zhou,
  • Yingqi Guo,
  • Donghai Hou,
  • Na Pi,
  • Yinlong Yang and
  • Hong Yu

Cordyceps fumosorosea is a common species within the Cordyceps genus. In this study, the protective effect of Cordyceps fumosorosea mycelium was investigated to clarify the potential mechanism of alleviating acute lung injury in mice using serum meta...

  • Article
  • Open Access
10 Citations
6,689 Views
10 Pages

Accelerated Development of AAV Purification Process Using a High-Throughput and Automated Crossflow System

  • Sónia Mendes,
  • Tiago Q. Faria,
  • André Nascimento,
  • Marc Noverraz,
  • Franziska Bollmann,
  • Piergiuseppe Nestola,
  • António Roldão,
  • Cristina Peixoto and
  • Ricardo J. S. Silva

Adeno-associated viruses (AAV) are currently predominant viral transfer tools for gene therapy, and efforts are being made to design faster and more efficient methods and technologies for their manufacturing. The early selection of high-performing fi...

  • Article
  • Open Access
2,139 Views
12 Pages

The Effect of Rotation on Gas Storage in Nanoporous Materials

  • Athanasios Ch. Mitropoulos,
  • Ramonna I. Kosheleva,
  • Margaritis Kostoglou and
  • Thodoris D. Karapantsios

Nanoporous materials offer a promising solution for gas storage applications in various scientific and engineering domains. However, several crucial challenges need to be addressed, including adsorptive capacity, rapid loading, and controlled gas del...

  • Article
  • Open Access
4 Citations
2,815 Views
17 Pages

Continuous Purification of Biodiesel with Deep Eutectic Solvent in a Laboratory Karr Column

  • Aleksandra Sander,
  • Ana Petračić,
  • Domagoj Vrsaljko,
  • Jelena Parlov Vuković,
  • Patricija Hršak and
  • Antonija Jelavić

Following the trend of transport decarbonization, biodiesel has become a promising alternative fuel option. Its production includes multiple steps, all of which can be time-consuming and energy intensive. Improving any of these steps could bring cons...

  • Article
  • Open Access
6 Citations
2,831 Views
13 Pages

Camellia oil is a high-value product with rich nutrients. Recently, the adulteration of camellia oil has become an increasingly concerning issue related to human health. In this study, electric soldering iron coupled with rapid evaporative ionization...

  • Article
  • Open Access
4 Citations
3,438 Views
13 Pages

Microfiltration plays an increasingly important role in various fields. Consequently, elucidating the mechanism of membrane fouling has emerged as a pivotal issue that needs to be resolved. In this study, a blocking filtration model was employed to e...

  • Article
  • Open Access
1 Citations
2,474 Views
19 Pages

Background: Recurrent approximation of retention parameters in reversed-phase HPLC is effective for revealing anomalies that are otherwise difficult to detect, namely, the reversible hydration of analytes. This was demonstrated previously for restric...

  • Article
  • Open Access
16 Citations
5,169 Views
21 Pages

Optimized Solid–Liquid Separation of Phenolics from Lavender Waste and Properties of the Dried Extracts

  • Patroklos Vareltzis,
  • Dimitrios Fotiou,
  • Vasiliki Papatheologou,
  • Smaro Kyroglou,
  • Efthymia Tsachouridou and
  • Athanasia M. Goula

Lavender distillation produces huge quantities of solid waste yearly. This waste is usually discarded, resulting in serious environmental issues. However, it still contains residual essential oil and other bioactive compounds. This research reports o...

  • Review
  • Open Access
11 Citations
13,759 Views
13 Pages

Immunochromatographic Detection of Human Blood: A Forensic Review

  • Calogero Cuttaia,
  • Barbara Di Stefano,
  • Solange Sorçaburu Ciglieri,
  • Raffaella Vetrini,
  • Carlo Previderè and
  • Paolo Fattorini

Body fluid identification is fundamental in forensic science as it links a specific biological source to a genetic profile, thus providing critical clues for crime scene reconstruction. Blood is one of the most common body fluids found on the crime s...

  • Article
  • Open Access
2 Citations
5,349 Views
11 Pages

Isolation of Macrocyclic Trichothecene Mycotoxins from the Lethal Toxic Mushroom Podostroma cornu-damae and Their Cytotoxic Activities

  • Bum Soo Lee,
  • Yun Young Lee,
  • Seoung Rak Lee,
  • Yoon Seo Jang,
  • Rhim Ryoo,
  • Wooram Park,
  • Se-Na Kim,
  • Soah Lee,
  • Chun Gwon Park and
  • Ki Hyun Kim

Podostroma cornu-damae, one of the lethal toxic mushrooms, is known to contain macrocyclic trichothecene mycotoxins exhibiting potent cytotoxic effects, attracting attention as an important research subject for scientists interested in natural produc...

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Separations - ISSN 2297-8739