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Search Results (302)

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Keywords = initiation and propagation mode

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18 pages, 7172 KiB  
Article
Study on the Effect of High Temperature and Cyclic Loading and Unloading Methods on the Mechanical Properties of Granite
by Fan Zhang, Congcong Lv, Kangwen Li, Yiming Zhang, Shengyuan Liu and Man Li
Appl. Sci. 2025, 15(8), 4448; https://doi.org/10.3390/app15084448 - 17 Apr 2025
Viewed by 160
Abstract
During the formation of deep rock bodies, such as hot dry rock, they are frequently exposed to high temperatures and repeated stress perturbations. The prolonged interaction of these two factors is a potential cause of deep underground rock instability. To investigate the effects [...] Read more.
During the formation of deep rock bodies, such as hot dry rock, they are frequently exposed to high temperatures and repeated stress perturbations. The prolonged interaction of these two factors is a potential cause of deep underground rock instability. To investigate the effects of high temperature and cyclic loading–unloading modes on rock mechanical properties, cyclic tests were conducted on granite under real-time high-temperature conditions using a multifunctional high-temperature testing machine. By comparing uniaxial compression test results with scanning electron microscopy (SEM) observations, the following was found: (1) The uniaxial compressive strength and elastic modulus of granite under real-time high-temperature conditions initially increase and then decrease as the temperature rises, while the peak strain consistently increases with temperature. (2) Under both cyclic loading–unloading modes, the mechanical properties of granite first improve and then deteriorate as the temperature increases. (3) As the temperature rises, microcracks in granite under both cyclic loading–unloading methods evolve from intracrystalline to intergranular cracks. The fracture surfaces of granite exhibit a significant increase in fracture severity, along with a noticeable rise in both the number and width of cracks. Crack propagation and crystal integrity degradation are more severe and complex in specimens subjected to variable lower limit cyclic loading–unloading than in those under constant-limit cyclic loading–unloading. These findings are of significant theoretical value for studying rock stability under simultaneous high-temperature and cyclic stress conditions. Full article
(This article belongs to the Special Issue Advances and Challenges in Rock Mechanics and Rock Engineering)
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13 pages, 11300 KiB  
Article
Bond Behavior Between Steel Bar and Reactive Powder Concrete Under Repeated Loading
by Dewen Zhang, Yanming Feng, Ruihui Han, Xiangsheng Kong, Dehong Wang and Chao Ren
Buildings 2025, 15(8), 1305; https://doi.org/10.3390/buildings15081305 - 16 Apr 2025
Viewed by 223
Abstract
To investigate the influence of repeated loading on the bond behavior between steel bars and reactive powder concrete (RPC), this study conducted repeated loading tests on eight beam specimens and one static loading test as a control. The effects of stress levels and [...] Read more.
To investigate the influence of repeated loading on the bond behavior between steel bars and reactive powder concrete (RPC), this study conducted repeated loading tests on eight beam specimens and one static loading test as a control. The effects of stress levels and the number of repeated loading cycles on the bond behavior between steel bars and RPC were examined. The results indicate that the static failure mode was characterized by steel bar pull-out accompanied by significant plastic deformation, with no propagation of cracks in the RPC after their initiation, demonstrating the excellent crack control capability of RPC. After 10,000 cycles of repeated loading at a high stress level (Z = 0.9), the ultimate bond strength decreased by only 3.68%, indicating the superior fatigue resistance of the steel–RPC interface. Based on the analysis of slip accumulation effects, a constitutive model considering stress levels and the number of repeated loading cycles was established. This model can serve as a basis for the design of steel anchorage in RPC structures subjected to cyclic loading. Full article
(This article belongs to the Special Issue Sustainable and Low-Carbon Building Materials and Structures)
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25 pages, 11740 KiB  
Article
Effects of Stress States and Joint Configurations on Dynamic Mechanical Properties of Rock Masses
by Tingting Liu, Zi Wang, Xuyi Wang, Shenghao Yang, Wenxu Huang and Luyang Ding
Materials 2025, 18(8), 1699; https://doi.org/10.3390/ma18081699 - 9 Apr 2025
Viewed by 282
Abstract
In complex geological environments, the discontinuous dynamic response behavior of jointed rock masses under the coupled effects of in situ stress and transient dynamic disturbances significantly exacerbates the risk of surrounding rock instability. This study establishes three-dimensional numerical models of various jointed rocks [...] Read more.
In complex geological environments, the discontinuous dynamic response behavior of jointed rock masses under the coupled effects of in situ stress and transient dynamic disturbances significantly exacerbates the risk of surrounding rock instability. This study establishes three-dimensional numerical models of various jointed rocks under uniaxial–biaxial–triaxial split Hopkinson pressure bar (SHPB) experimental systems through the coupling of the finite difference method (FDM) and discrete element method (DEM). The models adhere to the one-dimensional stress wave propagation assumption and satisfy the dynamic stress equilibrium requirements, demonstrating dynamic mechanical responses consistent with physical experiments. The results reveal that the synergistic–competitive effects between joint configuration and initial pre-compression jointly dominate the dynamic mechanical response of rocks. Multiaxial pre-compression promotes the development of secondary force chain networks, enhances rock impact resistance through multi-path stress transfer mechanisms, significantly improves strain energy storage density during peak stages, and drives failure modes to evolve from macroscopic through-going fractures to localized crushing zones. The spatial heterogeneity of joint configurations induces anisotropic characteristics in principal stress fabric. Single joint systems maintain structural integrity due to restricted weak plane propagation, while cross/parallel joints exhibit geometrically induced synergistic propagation effects, forming differentiated crack propagation paths that intensify frictional and kinetic energy dissipation. Through cross-scale numerical model comparisons, the evolution of force chain fabric, particle displacement distribution, microcrack propagation, and energy dissipation mechanisms were analyzed, unveiling the synergistic regulatory effects of the stress state and joint configuration on the rock dynamic response. This provides a theoretical basis for impact-resistant structure optimization and dynamic instability early warning in deep engineering projects involving jointed surrounding rock. Full article
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19 pages, 4634 KiB  
Article
Tensile Mechanical Properties and Failure Behavior Analysis of Three-Dimensional Woven Composite with Different Apertures and Braiding Angles
by Hailiang Su, Zhe Han, Tengteng Wei, Deng An, Qiulin Qin and Zhenxiao Wei
Coatings 2025, 15(4), 440; https://doi.org/10.3390/coatings15040440 - 8 Apr 2025
Viewed by 339
Abstract
The effects of opening size and braiding angle on the tensile behavior of 3D five-way braided composites were systematically studied, and the mechanical properties, failure modes, and fracture characteristics of the composites were comprehensively analyzed. Initially, a static tensile test was conducted. The [...] Read more.
The effects of opening size and braiding angle on the tensile behavior of 3D five-way braided composites were systematically studied, and the mechanical properties, failure modes, and fracture characteristics of the composites were comprehensively analyzed. Initially, a static tensile test was conducted. The results demonstrated that both the tensile strength and tensile modulus of the three-dimensional (3D) braided composites decreased as the braiding angle increased. The sensitivity of the tensile modulus to the aperture size increased significantly as the aperture increased. For specimens with varying braiding angles, smaller apertures were more effective in withstanding higher stress concentrations around the opening, with minimal impact on the tensile strength. In comparison to the laminate composites, the 3D braided composites, regardless of braiding angle, retained higher tensile strength after hole formation at the same aperture size. The fracture of the samples was observed and captured using an optical microscope. It was observed that the failure mode of the 3D braided composites progressively transitioned from fiber fractures to interface debonding with an increase in the braiding angle. After hole formation, stress concentration at the aperture edge caused crack propagation along the braiding direction. Larger apertures resulted in more severe cracks, ultimately leading to specimen failure. Full article
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15 pages, 10184 KiB  
Article
An Overview of Substrate Copper Trace Crack Through Experiments, Characterization, and Numerical Simulations
by Wei Yu, Faxing Che, Vance Liu, Raymond Chen, Sam Ireland, Yeow Chon Ong, Hong Wan Ng and Gokul Kumar
Micromachines 2025, 16(4), 428; https://doi.org/10.3390/mi16040428 - 2 Apr 2025
Viewed by 331
Abstract
The high input/output demands of memory packages require precise trace width and spacing, posing challenges for contemporary package design. Substrate copper trace cracks are a major reliability issue during temperature cycling tests (TCTs). This study offers a detailed analysis of copper trace crack [...] Read more.
The high input/output demands of memory packages require precise trace width and spacing, posing challenges for contemporary package design. Substrate copper trace cracks are a major reliability issue during temperature cycling tests (TCTs). This study offers a detailed analysis of copper trace crack mechanisms through experimental observations, material characterization, and numerical simulations. Common failure modes of trace cracks are identified from experimental data, pinpointing initiation sites and propagation paths. Young’s modulus of copper foil samples is assessed using four testing methods, revealing consistent trends across samples from different substrate suppliers. Sample A with higher E/H values tested via nanoindentation correlated with lower failure rates in the experiment. Stress–strain testing on copper foil was successfully performed at the lower TCT temperature limit of −65 °C, providing vital input for finite element (FE) models. The simulations show strong alignment with trace crack locations under different failure modes. The impact of copper trace width and material properties is illustrated in numerical models by comparing variations in plastic strain responses, which show differences of up to 40% and 30%, respectively. The simulation design of the experiments (DOE) indicates that high-strength solder resist (SR) can significantly enhance temperature cycling performance by reducing SR and copper trace stress and strain by up to 75%. The accumulation of plastic strain in copper traces is predicted to increase up to four times when SR breaks at the crack location, underscoring the importance of SR in copper trace reliability. Full article
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12 pages, 11545 KiB  
Article
Effect of Notches on Fatigue Crack Initiation and Early Propagation Behaviors of a Ni-Based Superalloy at Elevated Temperatures
by Zuopeng Zhao, Xuteng Hu and Zhiwei Guo
Metals 2025, 15(4), 384; https://doi.org/10.3390/met15040384 - 29 Mar 2025
Viewed by 259
Abstract
The role of notch stress and surface defects on fatigue crack initiation and small-crack propagation behavior has been investigated using groove simulation specimens. The naturally initiated small-crack growth tests have been performed on a FGH4099 superalloy at 500 °C and 700 °C. The [...] Read more.
The role of notch stress and surface defects on fatigue crack initiation and small-crack propagation behavior has been investigated using groove simulation specimens. The naturally initiated small-crack growth tests have been performed on a FGH4099 superalloy at 500 °C and 700 °C. The findings indicate that elevated testing temperature significantly reduced the proportion of fatigue crack initiation life, with a less pronounced effect on the proportion of life for cracks to grow to First Engineering Crack size. Competing crack initiation modes were observed in the fatigue test of groove simulation specimens. The location of maximum principal stress was dominant fatigue crack initiation sites, and for specimens with surface inclusions, the defect location can also serve as a crack initiation site. Furthermore, crack initiation modes were found to have a more pronounced effect on the small-crack growth rate. A turning point observed in the crack growth rate curves for specimens with multi-site crack initiation was attributed to crack shielding and subsequent coalescence. Full article
(This article belongs to the Special Issue Fatigue Assessment of Metals)
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18 pages, 7281 KiB  
Article
Degradation Characteristics and Mechanisms of Steel Fiber-Reinforced Concrete Linings in Subsea Tunnels: Insights from Accelerated Erosion Tests with Applied Electric Fields
by Longhai Wei, Jiguo Liu, Heng Shu, Qinglong Cui, Wenbo Peng, Huimin Gong, Yiguo Xue and Min Han
J. Mar. Sci. Eng. 2025, 13(4), 670; https://doi.org/10.3390/jmse13040670 - 26 Mar 2025
Viewed by 213
Abstract
Understanding the long-term durability and degradation mechanisms of steel fiber-reinforced concrete (SFRC) linings in subsea tunnels is critical for ensuring structural safety, cost effectiveness, and sustainability. This study investigated the degradation characteristics of SFRC with varying fiber contents (0%, 0.35%, 0.55%, and 0.75%) [...] Read more.
Understanding the long-term durability and degradation mechanisms of steel fiber-reinforced concrete (SFRC) linings in subsea tunnels is critical for ensuring structural safety, cost effectiveness, and sustainability. This study investigated the degradation characteristics of SFRC with varying fiber contents (0%, 0.35%, 0.55%, and 0.75%) and different acceleration durations, using the applied electric field acceleration method and X-ray CT tests. The experimental results revealed the characteristics of the surface crack distribution and evolution patterns in the SFRC specimens. Furthermore, the similarity between the non-uniform corrosion patterns observed in regard to accelerated corrosion under the applied electric fields and those occurring due to natural degradation was verified. The pore structure characteristics and internal crack development of the SFRC specimens were compared. The study found that the degradation process of the specimens was closely related to the fiber content. The incorporation of steel fibers altered the crack initiation and propagation modes, leading to a more scattered crack distribution. The accelerated corrosion method, employing an applied electric field, successfully simulated the non-uniform corrosion process of reinforcement in SFRC linings in subsea tunnels under natural conditions. Under the influence of a unidirectional chloride ingress source, the pronounced accumulation of corrosion products was observed only on the side of the reinforcement exposed to chloride penetration. This method effectively visualized the chloride penetration path and its impact on reinforcement corrosion, providing valuable insights for the anti-corrosion design of SFRC linings in subsea tunnels. Full article
(This article belongs to the Section Ocean Engineering)
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25 pages, 8999 KiB  
Article
Multipath-Assisted Ultra-Wideband Vehicle Localization in Underground Parking Environment Using Ray-Tracing
by Shuo Hu, Lixin Guo, Zhongyu Liu and Shuaishuai Gao
Sensors 2025, 25(7), 2082; https://doi.org/10.3390/s25072082 - 26 Mar 2025
Viewed by 253
Abstract
In complex underground parking scenarios, non-line-of-sight (NLOS) obstructions significantly impede positioning signals, presenting substantial challenges for accurate vehicle localization. While traditional positioning approaches primarily focus on mitigating NLOS effects to enhance accuracy, this research adopts an alternative perspective by leveraging NLOS propagation as [...] Read more.
In complex underground parking scenarios, non-line-of-sight (NLOS) obstructions significantly impede positioning signals, presenting substantial challenges for accurate vehicle localization. While traditional positioning approaches primarily focus on mitigating NLOS effects to enhance accuracy, this research adopts an alternative perspective by leveraging NLOS propagation as valuable information, enabling precise positioning in NLOS-dominated environments. We introduce an innovative NLOS positioning framework based on the generalized source (GS) technique, which employs ray-tracing (RT) to transform NLOS paths into equivalent line-of-sight (LOS) paths. A novel GS filtering and weighting strategy to establish initial weights for the nonlinear equation system. To combat significant NLOS noise interference, a robust iterative reweighted least squares (W-IRLS) method synergizes initial weights with optimal position estimation. Integrating ultra-wideband (UWB) delay and angular measurements, four distinct localization modes based on W-IRLS are developed: angle-of-arrival (AOA), time-of-arrival (TOA), AOA/TOA hybrid, and AOA/time-difference-of-arrival (TDOA) hybrid. The comprehensive experimental and simulation results validate the exceptional effectiveness and robustness of the proposed NLOS positioning framework, demonstrating positioning accuracy up to 0.14 m in specific scenarios. This research not only advances the state of the art in NLOS positioning but also establishes a robust foundation for high-precision localization in challenging environments. Full article
(This article belongs to the Special Issue Multi‐sensors for Indoor Localization and Tracking: 2nd Edition)
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15 pages, 11557 KiB  
Article
Revealing the Mechanical Properties and Fracture Mechanism of Ag Paste Sintered Solder by Two Different Preparation Methods
by Jialong Liang, Hao-Kun Yang, Xingming Huang, Li-Yin Gao and Zhi-Quan Liu
Materials 2025, 18(7), 1435; https://doi.org/10.3390/ma18071435 - 24 Mar 2025
Viewed by 235
Abstract
This paper studied the microstructure and mechanical properties of sintered Ag-Cu joints and semi-sintered Ag-Cu joints under tensile and shearing actions. By a comparative analysis of the differences in sintered Ag layer microstructure characteristics, crack propagation directions, and fracture surface characteristics, the differences [...] Read more.
This paper studied the microstructure and mechanical properties of sintered Ag-Cu joints and semi-sintered Ag-Cu joints under tensile and shearing actions. By a comparative analysis of the differences in sintered Ag layer microstructure characteristics, crack propagation directions, and fracture surface characteristics, the differences in the fracture mechanisms of the two types of sintered joints under the influence of tensile and shearing forces were further explained. Research shows that the sintered Ag joints have higher tensile and shearing properties than the semi-sintered Ag joints, but the two show similar fracture modes under the action of tensile force. The same phenomenon also occurs in the fracture mechanism under the action of shearing force. The difference is that under the action of tensile stress, cracks in the joints initiate from the Ag-Cu interface and grow along the interface until fracture occurs, while under the action of shearing force, cracks in the joints still initiate from the Ag-Cu interface, but then turn, and the cracks grow along the silver layer towards another Ag-Cu interface, which is a composite fracture mode. Under the action of tensile stress, the adhesive force of the Ag-Cu interface is shown to be weaker than the cohesive force within the sintered Ag layer itself, and the sintered Ag layer shows better ductile deformation. Under the action of shearing force, the advantage of the cohesive force within the sintered Ag layer is weakened, and the sintered Ag layer begins to fracture. Since sintered Ag joints have a better Ag-Cu interface and lower porosity than semi-sintered Ag joints, the energy required for failure increases correspondingly, showing better mechanical properties. Full article
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28 pages, 7342 KiB  
Article
Development of WHED Method to Study Operational Stability of Typical Transitions in a Hydropower Plant and a Pumped Storage Plant
by Xiuli Mao, Guoqing Wen, Yuchuan Wang, Jiaren Hu, Xuetao Gan and Pengju Zhong
Energies 2025, 18(6), 1549; https://doi.org/10.3390/en18061549 - 20 Mar 2025
Viewed by 270
Abstract
This study proposes the water hammer energy difference (WHED) method based on unsteady flow energy and continuity equations, as well as the propagation laws of water hammer in closed pipes, and verifies its accuracy. Additionally, the parameter evolution patterns of typical transient conditions [...] Read more.
This study proposes the water hammer energy difference (WHED) method based on unsteady flow energy and continuity equations, as well as the propagation laws of water hammer in closed pipes, and verifies its accuracy. Additionally, the parameter evolution patterns of typical transient conditions in pumped storage power plants are investigated based on WHED. The application of WHED in the transient processes of hydropower plants (HPs) is validated by experiments, showing a maximum error of about 7% between numerical and experimental results under conditions of initial load increase followed by decrease (HR = 184 m). Additionally, WHED was validated under two critical conditions in pumped storage plants (PSPs): 90% load rejection in generating mode and emergency power-off in pumping mode. In PSPs, the results of WHED are consistent with those obtained using the method of characteristics (MOC), with a maximum fault tolerance rate Δ < 3%. Notably, WHED offers superior time efficiency when analyzing hydraulic transitions in complex pipe networks, as it directly considers boundary conditions at both ends of the pipeline and hydraulic machinery, whereas MOC requires dividing the pipeline into multiple segments with a series of boundary points. Lastly, WHED’s energy parameters are used to describe flow stability from a physics perspective, explaining the causes of pressure fluctuations during transient periods in HPs and PSPs. These findings offer valuable references and guidance for the safe operation of PSPs and HPs. Full article
(This article belongs to the Special Issue Optimization Design and Simulation Analysis of Hydraulic Turbine)
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25 pages, 9613 KiB  
Article
A New Root and Trunk Rot Disease of Grapevine Plantlets Caused by Fusarium in Four Species Complexes
by José Manoel Ferreira de Lima Cruz, Otília Ricardo de Farias, Brunno Cassiano Lemos Araújo, Alejandra Valencia Rivera, Cláudia Rita de Souza and Jorge Teodoro de Souza
J. Fungi 2025, 11(3), 230; https://doi.org/10.3390/jof11030230 - 17 Mar 2025
Viewed by 496
Abstract
Grapevines are propagated by grafting, but the rootstocks used in commercial plantations are susceptible to several diseases. In this study, we focused on a novel root and trunk rot disease of grapevine plantlets that show symptoms during cold storage, before field establishment. Our [...] Read more.
Grapevines are propagated by grafting, but the rootstocks used in commercial plantations are susceptible to several diseases. In this study, we focused on a novel root and trunk rot disease of grapevine plantlets that show symptoms during cold storage, before field establishment. Our objectives were to study the aetiology, symptomatology, plant resistance responses, and mode of action of the pathogen that was initially identified as Fusarium. The characterisation of this pathosystem was performed by isolation, pathogenicity assays, genetic diversity studies with BOX-PCR, and identification by sequencing a fragment of the tef1 gene. Scanning electron microscopy and X-ray spectroscopy were used to study the mode of action and plant resistance responses. The results showed that 12 species of Fusarium, initially isolated from both healthy and diseased plantlets, and classified into 4 species complexes, were pathogenic to grapevines. Comparative analyses between diseased and healthy roots showed typical resistance responses in diseased plantlets, including tyloses formation, translocation of Ca, and accumulation of Si. Field experiments confirmed that 100% of the diseased plantlets died within 90 days of transplantation. This study contributes to a better understanding of root and trunk rot disease under cold storage and provides insights for the development of management strategies. Full article
(This article belongs to the Section Fungal Pathogenesis and Disease Control)
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14 pages, 5399 KiB  
Article
Fracture Modeling of QP980 Steel: Evaluating the Rice–Tracey and DF2016 Criteria Under Diverse Loading States
by Hammad Akhtar, Thamer Sami Alhalaybeh, Xucheng Fang, Salah Ud Din Asbah, Shuaijun Chao and Yanshan Lou
Materials 2025, 18(6), 1303; https://doi.org/10.3390/ma18061303 - 15 Mar 2025
Viewed by 636
Abstract
The ductile fracture behavior of QP980 steel was studied under various loading conditions, including shear (SS), equibiaxial tension (EBT), plane strain tension (PST), and uniaxial tension (UT). The experimental results are compared to the predictions from the Rice–Tracey and DF2016 criteria. Excluding the [...] Read more.
The ductile fracture behavior of QP980 steel was studied under various loading conditions, including shear (SS), equibiaxial tension (EBT), plane strain tension (PST), and uniaxial tension (UT). The experimental results are compared to the predictions from the Rice–Tracey and DF2016 criteria. Excluding the Lode parameter restricts the Rice–Tracey criteria, which considers stress triaxiality only, from making reasonable predictions of fracture behavior under complicated loading conditions of PST and SS. However, it yields reasonable predictions for simple stress states, UT, and EBT. The DF2016 criteria take both the Lode parameter and stress triaxiality into account and lead to a reasonable prediction over the maximum range of stress states. Experimental findings verify that the DF2016 model adequately describes the fracture initiation and propagation mode under conditions of moderate and high triaxiality. The findings show that the DF2016 criterion presents a more robust and versatile approach toward modeling ductile fracture behavior in QP980 steel for applications in structural engineering and the automobile industry, where accurate failure modeling is important. Full article
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18 pages, 3803 KiB  
Article
A High-Throughput Biosensing Approach for Rapid Screening of Compounds Targeting the hNav1.1 Channel: Marine Toxins as a Case Study
by Huijing Shen, Yuxia Cui, Shiyuan Liang, Shuang Zhou, Yingji Li, Yongning Wu and Junxian Song
Mar. Drugs 2025, 23(3), 119; https://doi.org/10.3390/md23030119 - 9 Mar 2025
Viewed by 948
Abstract
Voltage-gated sodium (Nav) channels play a crucial role in initiating and propagating action potentials throughout the heart, muscles and nervous systems, making them targets for a number of drugs and toxins. While patch-clamp electrophysiology is considered the gold standard for measuring ion channel [...] Read more.
Voltage-gated sodium (Nav) channels play a crucial role in initiating and propagating action potentials throughout the heart, muscles and nervous systems, making them targets for a number of drugs and toxins. While patch-clamp electrophysiology is considered the gold standard for measuring ion channel activity, its labor-intensive and time-consuming nature highlights the need for fast screening strategies to facilitate a preliminary selection of potential drugs or hazards. In this study, a high-throughput and cost-effective biosensing method was developed to rapidly identify specific agonists and inhibitors targeting the human Nav1.1 (hNav1.1) channel. It combines a red fluorescent dye sensitive to transmembrane potentials with CHO cells stably expressing the hNav1.1 α-subunit (hNav1.1-CHO). In the initial screening mode, the tested compounds were mixed with pre-equilibrated hNav1.1-CHO cells and dye to detect potential agonist effects via fluorescence enhancement. In cases where no fluorescence enhancement was observed, the addition of a known agonist veratridine allowed the indication of inhibitor candidates by fluorescence reduction, relative to the veratridine control without test compounds. Potential agonists or inhibitors identified in the initial screening were further evaluated by measuring concentration–response curves to determine EC50/IC50 values, providing semi-quantitative estimates of their binding strength to hNav1.1. This robust, high-throughput biosensing assay was validated through comparisons with the patch-clamp results and tested with 12 marine toxins, yielding consistent results. It holds promise as a low-cost, rapid, and long-term stable approach for drug discovery and non-target screening of neurotoxins. Full article
(This article belongs to the Special Issue Toxins as Marine-Based Drug Discovery, 2nd Edition)
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13 pages, 2195 KiB  
Article
Experimental Study on the Acid Fracturing Fracture Propagation Law of a Fractured Carbonate Reservoir in the Majiagou Formation
by Yongchun Zhang, Jianchao Kuang, Hao Zhang, Ying Zhong and Shijie Dong
Processes 2025, 13(3), 695; https://doi.org/10.3390/pr13030695 - 28 Feb 2025
Viewed by 484
Abstract
Acid fracturing is a crucial method for reservoir reconstruction in carbonate reservoirs, and the propagation pattern of acid-etched fractures plays a key role in determining the scope of reservoir enhancement and post-fracturing productivity. However, large-scale physical simulations directly using acid solutions in fracturing [...] Read more.
Acid fracturing is a crucial method for reservoir reconstruction in carbonate reservoirs, and the propagation pattern of acid-etched fractures plays a key role in determining the scope of reservoir enhancement and post-fracturing productivity. However, large-scale physical simulations directly using acid solutions in fracturing experiments are limited, and the fracture propagation patterns under acid fracturing remain unclear. To address this gap, in this study, we collected carbonate rock samples from the Majiagou Formation in the Daniudi area, preparing large-scale fracturing specimens with side lengths of 30 cm. The propagation of acid fracturing fractures was investigated using self-developed true-triaxial acid fracturing equipment. Based on post-fracturing fracture morphology and pressure curves, the effects of fracturing fluid type, injection rate, injection mode, and natural fractures (NFs) on acid fracturing fracture propagation were analyzed. The experimental results showed that the acid solution effectively weakens the mechanical properties of the open-hole section, creating multiple mechanical weak points and promoting the initiation of fractures. Pre-fracturing treatment with low-viscosity acid can significantly enhance fracture complexity near the wellbore and expand the near-well stimulation zone. Lowering the injection rate increases the acid solution’s filtration loss into natural fractures, weakening the cementation strength of these fractures and encouraging the formation of complex fracture networks. Furthermore, employing a multi-stage alternating injection of high-viscosity and low-viscosity acids can reduce fracture temperature and acid filtration loss while also enhancing differential etching through viscous fingering. This approach improves the conductivity and conductivity retention of the acid-etched fractures. The results of this study can provide a reference for the acid fracturing stimulation of fractured carbonate reservoirs. Full article
(This article belongs to the Special Issue Recent Advances in Hydrocarbon Production Processes from Geoenergy)
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19 pages, 8309 KiB  
Article
Experimental Study on Factors Influencing the Propagation of Hydraulic Fractures in Shale Reservoirs with Developed Natural Weak Planes
by Yitao Huang, Juhui Zhu, Yongming Li, Le He, Zeben Fang and Xiyu Chen
Energies 2025, 18(5), 1100; https://doi.org/10.3390/en18051100 - 24 Feb 2025
Viewed by 329
Abstract
Hydraulic fracturing is a key technology to build productivity in shale reservoirs; however, the evolution mechanism of fractures is extremely complex, especially in reservoirs with natural weak-planes development. There is an urgent need to conduct systematic research on the influence of natural weak [...] Read more.
Hydraulic fracturing is a key technology to build productivity in shale reservoirs; however, the evolution mechanism of fractures is extremely complex, especially in reservoirs with natural weak-planes development. There is an urgent need to conduct systematic research on the influence of natural weak planes on the vertical propagation of hydraulic fractures. This article takes the deep shale gas block of Luzhou in Southern Sichuan as the research basis and conducts different conditions of true triaxial large-scale hydraulic fracturing physical simulation experiments as well as the characteristics of natural weak-plane reservoir development and reservoir geological characteristics. This study clarifies the interaction mechanism between hydraulic fractures and natural weak planes and identifies the influence of parameters such as vertical stress difference, natural fracture strength, and approach angle on the propagation path of hydraulic fractures in reservoirs with developed natural weak planes, which help us gain a deeper insight into the interaction mechanism between fracture and weak plane. This study indicates that the widely developed natural weak planes in shale reservoirs significantly affect the initiation, propagation, and final distribution of hydraulic fractures. Based on pressure response characteristics, the fracture initiation types can be categorized into two scenarios: initiation along the direction of the maximum principal stress and initiation along natural weak planes. The propagation modes of fractures can be divided into three types: propagation perpendicular to natural weak planes, propagation parallel to natural weak planes, and multi-fracture propagation. The post-pressure fracture distribution patterns can be classified into four types: through-going fractures, T-shaped fractures, compound fractures, and complex fracture networks. The absence of developed natural weak planes, high vertical stress differences, high natural weak-plane cementation strength, and large intersection angles are favorable conditions for the vertical propagation of hydraulic fractures. The research findings enrich the fundamental theory of vertical propagation of hydraulic fractures in shale reservoirs with developed natural weak planes and provide a scientific basis for the formulation and optimization of stimulation schemes for deep shale reservoirs, contributing to better stimulation effects in the Southern Sichuan shale gas block. Full article
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